Water-soluble gold nanoparticles

Water-soluble gold nanoparticles (Au NPs) stabilized by a nitrogen-rich PEG-tagged substrate have been prepared by reduction of HAuCl₄ with NaBH₄ in water at room temperature. The morphology and size of the nanoparticles can be controlled by simply varying the gold/stabilizer ratio. The nanoparticle...

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Detalles Bibliográficos
Autores: Guo, Wusheng|||0000-0002-9988-8497, Pleixats, Roser|||0000-0003-2544-732X, Shafir, Alexandr|||0000-0002-8127-2299
Tipo de recurso: artículo
Fecha de publicación:2015
País:España
Institución:Universitat Autònoma de Barcelona
Repositorio:Dipòsit Digital de Documents de la UAB
Idioma:inglés
OAI Identifier:oai:ddd.uab.cat:157784
Acceso en línea:https://ddd.uab.cat/record/157784
https://dx.doi.org/urn:doi:10.1002/asia.201500290
Access Level:acceso abierto
Palabra clave:Water-soluble Au NPs
Reduction
Nitroarenes
Anilines
Descripción
Sumario:Water-soluble gold nanoparticles (Au NPs) stabilized by a nitrogen-rich PEG-tagged substrate have been prepared by reduction of HAuCl₄ with NaBH₄ in water at room temperature. The morphology and size of the nanoparticles can be controlled by simply varying the gold/stabilizer ratio. The nanoparticles have been fully characterized by TEM, HRTEM, ED, EDS, UV-vis, p-XRD and elemental analysis. The material is efficient as a recyclable catalyst for the selective reduction of nitroarenes with NaBH₄ to yield the corresponding anilines in water at room temperature. Furthermore, the potential ability of the Au NPs as a refractive index sensor due to their localized surface plasmon resonance (LSPR) effect has also been assessed.