Evidence for helical microstructure of aragonite fibers in pteropod shells

Abstract: Planktonic gastropods of the suborder Euthecosomata (order Pteropoda) secrete a unique microstructure made of tightly interlocked, space-filling helically coiled aragonite fibers. This material has a high degree of ordering because all fibers are in phase at a given growth plane. The recog...

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Detalles Bibliográficos
Autores: Checa, Antonio G., Pimentel, Carlos, Berent, K., Ramos-Silva, Paula, Rodríguez-Navarro, Alejandro B., Cartwright, Julyan H. E., Sainz-Díaz, C. Ignacio
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2023
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/343590
Acceso en línea:http://hdl.handle.net/10261/343590
Access Level:acceso abierto
Palabra clave:3D modeling
Biomimetic processes
Carbonate minerals
Functional materials
Microstructure
Molluscs
Scanning electron microscopy
All fiber
Aragonite
Aragonite fiber
Degree of ordering
Helical fiber
In-phase
Pteropod
Scanning electron micrographs
Space filling
Theoretical modeling
Fibers
Descripción
Sumario:Abstract: Planktonic gastropods of the suborder Euthecosomata (order Pteropoda) secrete a unique microstructure made of tightly interlocked, space-filling helically coiled aragonite fibers. This material has a high degree of ordering because all fibers are in phase at a given growth plane. The recognition of the helical nature from mere scanning electron micrographs is somewhat uncertain. In addition, three-dimensional (3D) reconstructions of individual helices are hindered by the small dimensions of fibers, and the virtual absence of intervening organic interphases. Here, we (1) reexamine the morphological characteristics of the fibers in fracture and find them compatible with a helical model, (2) provide direct evidence of the helical mode of coiling in the form of anaglyphs, and (3) develop a 3D model, which is fully consistent with the patterns observed in fractures and polished sections. Proposals based on motifs different from helices are not congruent with the observations. Graphical abstract: [Figure not available: see fulltext.] Impact statement: Some planktonic gastropods of the order Pteropoda secrete a unique microstructure that was originally described as made of tightly interlocked helically coiled continuous aragonite fibers. Despite this material having been described 50 years ago, there is still debate as to the helical design of such fibers. We provide additional unambiguous evidence that fibers describe true helical trajectories during growth. Establishing their true nature is essential in order to know the spectrum of calcified biomaterials produced by molluscs. This is also a prerequisite for future biomimetic studies aiming at producing bioinspired highly functional materials.