Assessing Si-based anodes for Ca-ion batteries: Electrochemical decalciation of CaSi2

Density functional theory (DFT) calculations are used to investigate the basic electrochemical characteristics of Si-based anodes in calcium ion batteries (CIBs). The calculated average voltage of Ca alloying with fcc-Si to form the intermetallic CaxSi phases (0.5 b x ≤ 2) is of 0.4 V, with a volume...

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Detalles Bibliográficos
Autores: Ponrouch, Alexandre, Tchitchekova , Deyana S., Frontera, Carlos, Bardé, Fanny, Arroyo-de Dompablo, M. Elena, Palacín, M. Rosa
Tipo de recurso: artículo
Estado:Versión aceptada para publicación
Fecha de publicación:2016
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/147984
Acceso en línea:http://hdl.handle.net/10261/147984
Access Level:acceso abierto
Palabra clave:Ca-ion batteries
Si anode
CaSi alloys
CaSi2
Descripción
Sumario:Density functional theory (DFT) calculations are used to investigate the basic electrochemical characteristics of Si-based anodes in calcium ion batteries (CIBs). The calculated average voltage of Ca alloying with fcc-Si to form the intermetallic CaxSi phases (0.5 b x ≤ 2) is of 0.4 V, with a volume variation of 306%. Decalciation of the lower Ca content phase, CaSi2, is predicted at an average voltage between 0.57 V (formation of Si-fcc, 65% volume variation) and 1.2 V (formation of metastable deinserted-Si phase, 29% volume variation). Experiments carried out in conventional alkyl carbonate electrolytes show evidence that electrochemical “decalciation” of CaSi2 is possible at moderate temperatures. The decalciation of CaSi2 is confirmed by different characterization techniques.