Rapid determination of malondialdehyde in serum samples using a porphyrin‑functionalized magnetic graphene oxide electrochemical sensor.

An electrochemical sensor based on a screen-printed carbon electrode (SPCE) modified with porphyrin-functionalized magnetic graphene oxide (TCPP-MGO) was developed for the sensitive and selective determination of malondialdehyde (MDA), an important biomarker of oxidative damage, in serum samples. Th...

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Detalles Bibliográficos
Autores: Ben Attig Fayac, Jihane, Latrous, Latifa, Galván, Ismael, Zougagh Zariouh, Mohammed, Ríos Castro, Ángel
Tipo de recurso: artículo
Fecha de publicación:2023
País:España
Institución:Universidad de Castilla-La Mancha
Repositorio:RUIdeRA. Repositorio Institucional de la UCLM
OAI Identifier:oai:ruidera.uclm.es:10578/36638
Acceso en línea:https://hdl.handle.net/10578/36638
Access Level:acceso abierto
Palabra clave:Porphyrin-functionalized magnetic graphene oxide
Screen-printed carbon electrode
Electrochemical sensor
Malondialdehyde
Serum samples
Descripción
Sumario:An electrochemical sensor based on a screen-printed carbon electrode (SPCE) modified with porphyrin-functionalized magnetic graphene oxide (TCPP-MGO) was developed for the sensitive and selective determination of malondialdehyde (MDA), an important biomarker of oxidative damage, in serum samples. The coupling of TCPP with MGO allows the exploitation of the magnetic properties of the material for separation, preconcentration, and manipulation of analyte, which is selectively captured onto the TCPPMGO surface. The electron-transfer capability in the SPCE was improved through derivatization of MDA with diaminonaphthalene (DAN) (MDA-DAN). TCPP-MGO-SPCEs have been employed to monitor the differential pulse voltammetry (DVP) levels of the whole material, which is related to the amount of the captured analyte.