Engineering pH-Sensitive Stable Nanovesicles for Delivery of MicroRNA Therapeutics

MicroRNAs (miRNAs) are small non-coding endogenous RNAs, which are attracting a growing interest as therapeutic molecules due to their central role in major diseases. However, the transformation of these biomolecules into drugs is limited due to their unstability in the bloodstream, caused by nuclea...

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Autores: Boloix, Ariadna, Feiner-Gracia, Natalia, Köber, Mariana, Repetto, Javier, Pascarella, Rosa, Soriano, Aroa, Masanas, Marc, Segovia, Nathaly, Vargas Nadal, Guillem, Merlo Mas, Josep, Danino, Dganit, Abutbul-Ionita, Inbal, Foradada, Laia, Roma, Josep, Córdoba, Alba, Sala Vergés, Santiago, Toledo, Josep Sánchez de, Gallego, Soledad, Veciana, Jaume, Albertazzi, Lorenzo, Segura, Miguel F., Ventosa, Nora
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2022
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/264232
Acceso en línea:http://hdl.handle.net/10261/264232
https://api.elsevier.com/content/abstract/scopus_id/85119046061
Access Level:acceso abierto
Palabra clave:Cancer therapy
miRNAs delivery
Nanocarriers
Nanovesicles
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dc.title.none.fl_str_mv Engineering pH-Sensitive Stable Nanovesicles for Delivery of MicroRNA Therapeutics
title Engineering pH-Sensitive Stable Nanovesicles for Delivery of MicroRNA Therapeutics
spellingShingle Engineering pH-Sensitive Stable Nanovesicles for Delivery of MicroRNA Therapeutics
Boloix, Ariadna
Cancer therapy
miRNAs delivery
Nanocarriers
Nanovesicles
title_short Engineering pH-Sensitive Stable Nanovesicles for Delivery of MicroRNA Therapeutics
title_full Engineering pH-Sensitive Stable Nanovesicles for Delivery of MicroRNA Therapeutics
title_fullStr Engineering pH-Sensitive Stable Nanovesicles for Delivery of MicroRNA Therapeutics
title_full_unstemmed Engineering pH-Sensitive Stable Nanovesicles for Delivery of MicroRNA Therapeutics
title_sort Engineering pH-Sensitive Stable Nanovesicles for Delivery of MicroRNA Therapeutics
dc.creator.none.fl_str_mv Boloix, Ariadna
Feiner-Gracia, Natalia
Köber, Mariana
Repetto, Javier
Pascarella, Rosa
Soriano, Aroa
Masanas, Marc
Segovia, Nathaly
Vargas Nadal, Guillem
Merlo Mas, Josep
Danino, Dganit
Abutbul-Ionita, Inbal
Foradada, Laia
Roma, Josep
Córdoba, Alba
Sala Vergés, Santiago
Toledo, Josep Sánchez de
Gallego, Soledad
Veciana, Jaume
Albertazzi, Lorenzo
Segura, Miguel F.
Ventosa, Nora
author Boloix, Ariadna
author_facet Boloix, Ariadna
Feiner-Gracia, Natalia
Köber, Mariana
Repetto, Javier
Pascarella, Rosa
Soriano, Aroa
Masanas, Marc
Segovia, Nathaly
Vargas Nadal, Guillem
Merlo Mas, Josep
Danino, Dganit
Abutbul-Ionita, Inbal
Foradada, Laia
Roma, Josep
Córdoba, Alba
Sala Vergés, Santiago
Toledo, Josep Sánchez de
Gallego, Soledad
Veciana, Jaume
Albertazzi, Lorenzo
Segura, Miguel F.
Ventosa, Nora
author_role author
author2 Feiner-Gracia, Natalia
Köber, Mariana
Repetto, Javier
Pascarella, Rosa
Soriano, Aroa
Masanas, Marc
Segovia, Nathaly
Vargas Nadal, Guillem
Merlo Mas, Josep
Danino, Dganit
Abutbul-Ionita, Inbal
Foradada, Laia
Roma, Josep
Córdoba, Alba
Sala Vergés, Santiago
Toledo, Josep Sánchez de
Gallego, Soledad
Veciana, Jaume
Albertazzi, Lorenzo
Segura, Miguel F.
Ventosa, Nora
author2_role author
author
author
author
author
author
author
author
author
author
author
author
author
author
author
author
author
author
author
author
author
dc.contributor.none.fl_str_mv Ministerio de Educación, Cultura y Deporte (España)
Ministerio de Economía y Competitividad (España)
Ministerio de Ciencia, Innovación y Universidades (España)
Instituto de Salud Carlos III
Centro de Investigación Biomédica en Red Bioingeniería, Biomateriales y Nanomedicina (España)
Matem lo Bitxo
Asociación Española Contra el Cáncer
Generalitat de Catalunya
Boloix, Ariadna [0000-0002-1648-5589]
Köber, Mariana [0000-0001-9962-7900]
Soriano, Aroa [0000-0001-9659-1471]
Masanas, Marc [0000-0002-2249-8554]
Segovia, Nathaly [0000-0001-8814-6095]
Vargas Nadal, Guillem [0000-0003-4383-1325]
Merlo Mas, Josep [0000-0002-3698-6655]
Danino, Dganit [0000-0002-9782-4940]
Foradada, Laia [0000-0002-0589-4360]
Roma, Josep [0000-0001-7692-6123]
Toledo, Josep Sánchez de [0000-0002-1034-1920]
Gallego, Soledad [0000-0002-4712-9624]
Veciana, Jaume [0000-0003-1023-9923]
Albertazzi, Lorenzo [0000-0002-6837-0812]
Segura, Miguel F. [0000-0003-0916-3618]
Ventosa, Nora [0000-0002-8008-4974]
Consejo Superior de Investigaciones Científicas [https://ror.org/02gfc7t72]
dc.subject.none.fl_str_mv Cancer therapy
miRNAs delivery
Nanocarriers
Nanovesicles
topic Cancer therapy
miRNAs delivery
Nanocarriers
Nanovesicles
description MicroRNAs (miRNAs) are small non-coding endogenous RNAs, which are attracting a growing interest as therapeutic molecules due to their central role in major diseases. However, the transformation of these biomolecules into drugs is limited due to their unstability in the bloodstream, caused by nucleases abundantly present in the blood, and poor capacity to enter cells. The conjugation of miRNAs to nanoparticles (NPs) could be an effective strategy for their clinical delivery. Herein, the engineering of non-liposomal lipid nanovesicles, named quatsomes (QS), for the delivery of miRNAs and other small RNAs into the cytosol of tumor cells, triggering a tumor-suppressive response is reported. The engineered pH-sensitive nanovesicles have controlled structure (unilamellar), size (<150 nm) and composition. These nanovesicles are colloidal stable (>24 weeks), and are prepared by a green, GMP compliant, and scalable one-step procedure, which are all unavoidable requirements for the arrival to the clinical practice of NP based miRNA therapeutics. Furthermore, QS protect miRNAs from RNAses and when injected intravenously, deliver them into liver, lung, and neuroblastoma xenografts tumors. These stable nanovesicles with tunable pH sensitiveness constitute an attractive platform for the efficient delivery of miRNAs and other small RNAs with therapeutic activity and their exploitation in the clinics.
publishDate 2022
dc.date.none.fl_str_mv 2022
2022
2022
dc.type.none.fl_str_mv info:eu-repo/semantics/article
http://purl.org/coar/resource_type/c_6501
Publisher's version
info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/10261/264232
https://api.elsevier.com/content/abstract/scopus_id/85119046061
url http://hdl.handle.net/10261/264232
https://api.elsevier.com/content/abstract/scopus_id/85119046061
dc.language.none.fl_str_mv Inglés
language_invalid_str_mv Inglés
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info:eu-repo/grantAgreement/MINECO/Plan Estatal de Investigación Científica y Técnica y de Innovación 2013-2016/MAT2016-80826-R
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Small (Weinheim an der Bergstrasse, Germany)
http://dx.doi.org/10.1002/smll.202101959

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eu_rights_str_mv openAccess
dc.publisher.none.fl_str_mv Wiley-VCH
publisher.none.fl_str_mv Wiley-VCH
dc.source.none.fl_str_mv reponame:DIGITAL.CSIC. Repositorio Institucional del CSIC
instname:Consejo Superior de Investigaciones Científicas (CSIC)
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spelling Engineering pH-Sensitive Stable Nanovesicles for Delivery of MicroRNA TherapeuticsBoloix, AriadnaFeiner-Gracia, NataliaKöber, MarianaRepetto, JavierPascarella, RosaSoriano, AroaMasanas, MarcSegovia, NathalyVargas Nadal, GuillemMerlo Mas, JosepDanino, DganitAbutbul-Ionita, InbalForadada, LaiaRoma, JosepCórdoba, AlbaSala Vergés, SantiagoToledo, Josep Sánchez deGallego, SoledadVeciana, JaumeAlbertazzi, LorenzoSegura, Miguel F.Ventosa, NoraCancer therapymiRNAs deliveryNanocarriersNanovesiclesMicroRNAs (miRNAs) are small non-coding endogenous RNAs, which are attracting a growing interest as therapeutic molecules due to their central role in major diseases. However, the transformation of these biomolecules into drugs is limited due to their unstability in the bloodstream, caused by nucleases abundantly present in the blood, and poor capacity to enter cells. The conjugation of miRNAs to nanoparticles (NPs) could be an effective strategy for their clinical delivery. Herein, the engineering of non-liposomal lipid nanovesicles, named quatsomes (QS), for the delivery of miRNAs and other small RNAs into the cytosol of tumor cells, triggering a tumor-suppressive response is reported. The engineered pH-sensitive nanovesicles have controlled structure (unilamellar), size (<150 nm) and composition. These nanovesicles are colloidal stable (>24 weeks), and are prepared by a green, GMP compliant, and scalable one-step procedure, which are all unavoidable requirements for the arrival to the clinical practice of NP based miRNA therapeutics. Furthermore, QS protect miRNAs from RNAses and when injected intravenously, deliver them into liver, lung, and neuroblastoma xenografts tumors. These stable nanovesicles with tunable pH sensitiveness constitute an attractive platform for the efficient delivery of miRNAs and other small RNAs with therapeutic activity and their exploitation in the clinics.The funding was received by Ministerio de Educación, Cultura y Deporte (Grant no. FPU16/01099), Ministerio de Economía, Industria y Competividad (Grants MAT2016-80820-R, MAT2016-80826-R and SAF2016-75241-R), the Ministry of Science and Innovation (MINECO) of Spain through grant PID2019-105622RB-I00, from Instituto de Salud Carlos III (Grant no. CP16/00006, PI17/00564, PI20/00530, DTS20/00018) (Co-funded by European Regional Development Fund/European Social Fund) “Investing in your future”), from the EuroNanoMed II platform through the NanoVax project, from CIBER-BBN through grant TAG-SMARTLY, Joan Petit Foundation, Asociación Matem Lo Bitxo and Asociación Española Contra el Cáncer (Grant no. LABAE18009SEGU), as well as, Generalitat de Catalunya through the Centres de Recerca de Catalunya (CERCA) programme and grant no. 2017-SGR-918, and from Agency for Management of University and Research Grants (AGAUR) (Grant no 2018LLAV0064 and SIFECAT IU68-010017). Furthermore, ICMAB-CSIC acknowledges support from the MINECO through the Severo Ochoa Programme for Centres of Excellence in R&D (SEV-2015-0496 and CEX2019-000917-S). Quatsome production and their physicochemical characterization was performed by the ICTS “NANBIOSIS,” more specifically in the Biomaterial Processing and Nanostructuring Unit (U6), Unit of the CIBER in Bioengineering, Biomaterials & Nanomedicne (CIBER-BBN) located at the Institute of Materials Science of Barcelona (ICMAB-CSIC). The authors thank the UAB Microscopy service for their help in recording cryo-TEM images. The authors also thank Mr. Adolfo de Hoyos-Limon for pKa measurements, Ms. Patricia Pérez for her help in in vitro experiments, the members of Laboratory Animal Service Unit of Vall d'Hebron Research Institute for their help in the in vivo experiment. The authors thank Editage (www.editage.com) and Ms. Christine O'Hara for English language correction. The authors acknowledge Biorender.com for allowing the adaptation of their templates. Retrieved from https://app.biorender.com/biorender-templates.With funding from the Spanish government through the ‘Severo Ochoa Centre of Excellence’ accreditation (CEX2019-000917-S).Peer reviewedWiley-VCHMinisterio de Educación, Cultura y Deporte (España)Ministerio de Economía y Competitividad (España)Ministerio de Ciencia, Innovación y Universidades (España)Instituto de Salud Carlos IIICentro de Investigación Biomédica en Red Bioingeniería, Biomateriales y Nanomedicina (España)Matem lo BitxoAsociación Española Contra el CáncerGeneralitat de CatalunyaBoloix, Ariadna [0000-0002-1648-5589]Köber, Mariana [0000-0001-9962-7900]Soriano, Aroa [0000-0001-9659-1471]Masanas, Marc [0000-0002-2249-8554]Segovia, Nathaly [0000-0001-8814-6095]Vargas Nadal, Guillem [0000-0003-4383-1325]Merlo Mas, Josep [0000-0002-3698-6655]Danino, Dganit [0000-0002-9782-4940]Foradada, Laia [0000-0002-0589-4360]Roma, Josep [0000-0001-7692-6123]Toledo, Josep Sánchez de [0000-0002-1034-1920]Gallego, Soledad [0000-0002-4712-9624]Veciana, Jaume [0000-0003-1023-9923]Albertazzi, Lorenzo [0000-0002-6837-0812]Segura, Miguel F. [0000-0003-0916-3618]Ventosa, Nora [0000-0002-8008-4974]Consejo Superior de Investigaciones Científicas [https://ror.org/02gfc7t72]202220222022info:eu-repo/semantics/articlehttp://purl.org/coar/resource_type/c_6501Publisher's versioninfo:eu-repo/semantics/publishedVersionhttp://hdl.handle.net/10261/264232https://api.elsevier.com/content/abstract/scopus_id/85119046061reponame:DIGITAL.CSIC. 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