Control of the Microstructure in a Al5Co15Cr30Fe25Ni25 High Entropy Alloy through Thermo-Mechanical and Thermal Treatments

The effect of thermos-mechanical processing and thermal treatments on the microstructure of a single phase fcc-based AlCoCrFeNi high entropy alloy is evaluated in this study. As-cast ingots of the high entropy alloy were thermo-mechanically processed following different routes involving forging, col...

Descripción completa

Detalles Bibliográficos
Autores: Pérez Zubiaur, Pablo, Medina, Judit, Vega González, María Fernanda, Garcés, Gerardo, Adeva, Paloma
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2023
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/340453
Acceso en línea:http://hdl.handle.net/10261/340453
Access Level:acceso abierto
Palabra clave:High-entropy alloys
Processing routes
Annealing
Microstructural evolution
Hardness
Descripción
Sumario:The effect of thermos-mechanical processing and thermal treatments on the microstructure of a single phase fcc-based AlCoCrFeNi high entropy alloy is evaluated in this study. As-cast ingots of the high entropy alloy were thermo-mechanically processed following different routes involving forging, cold rolling, warm rolling or hot rolling. In addition, the microstructural evolution of highly deformed cold rolled sheets with the annealing temperature was analyzed. The data reveal that a high-volume fraction of the microstructure commences to recrystallize from 600 °C. In the absence of recrystallization, i.e., below 600 °C, the hardness of thermo-mechanically processed and annealed samples was very close. When recrystallization takes place, the thermo-mechanically treated alloys exhibit higher hardness than the annealed alloys because the recrystallized grains are strengthened by dislocations generated in further steps of the processing while the alloys in the annealed condition are free of dislocations. Maximum hardening is found for the alloy warm-rolled at 450 °C and the alloy cold-rolled plus annealing at 500 °C for 1 h. Diffusion of solute atoms to the core of dislocations, pinning its movement, accounts for the additional hardening.