Synthesis and characterization of a new nano lead(II) 0-D coordination supramolecular compound
Nano-structure of a new 0D Pb(II) coordination supramolecular compound, [Pb(8-Quin)](ClO)(1), L = 8-HQuin = 8-hydroxyquinolin ligand has been synthesized by use of a sonochemical process and characterized by scanning electron microscopy (SEM), X-ray powder diffraction (XRPD), Fourier transform infra...
| Autores: | , , , |
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| Tipo de recurso: | artículo |
| Fecha de publicación: | 2017 |
| País: | España |
| Institución: | Universitat Autònoma de Barcelona |
| Repositorio: | Dipòsit Digital de Documents de la UAB |
| Idioma: | inglés |
| OAI Identifier: | oai:ddd.uab.cat:225299 |
| Acceso en línea: | https://ddd.uab.cat/record/225299 https://dx.doi.org/urn:doi:10.1016/j.ultsonch.2017.04.023 |
| Access Level: | acceso abierto |
| Palabra clave: | Nanoparticles Lead(II) oxide Coordination supramolecular Ultrasonic |
| Sumario: | Nano-structure of a new 0D Pb(II) coordination supramolecular compound, [Pb(8-Quin)](ClO)(1), L = 8-HQuin = 8-hydroxyquinolin ligand has been synthesized by use of a sonochemical process and characterized by scanning electron microscopy (SEM), X-ray powder diffraction (XRPD), Fourier transform infrared spectroscopy (FTIR) and elemental analyses. The structure of compound 1 was determined by single-crystal X-ray diffraction. The single crystal X-ray data of compound 1 implies that the Pb ions are five coordinated. Each lead atom is coordinated to nitrogen and oxygen atoms of 8-hydroxyquinolin ligand. Topological analysis shows that the compound 1 is 1,2,3,4,4M12-1net. Nanoparticles of lead(II) oxide have been prepared by calcination of lead(II) coordination polymer at 500 °C that were characterized by scanning electron microscopy (SEM), X-ray powder diffraction (XRPD) and IR spectroscopy. |
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