A potential C-S-H nucleation mechanism: atomistic simulations of the portlandite to C-S-H transformation

The nucleation of the C-S-H gel is a complex process, key to controlling the hydration kinetics and microstructure development of cement. In this paper, a mechanism for the crystallization step during the C-S-H gel non-classical nucleation is proposed and explored by atomistic simulation methods. In...

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Detalles Bibliográficos
Autores: Méndez Aretxabaleta, Xabier, López Zorrilla, Jon, Labbez, Christophe, Etxebarria Altzaga, Iñigo, Manzano Moro, Hegoi
Tipo de recurso: artículo
Fecha de publicación:2022
País:España
Institución:Universidad del País Vasco
Repositorio:Addi. Archivo Digital para la Docencia y la Investigación
OAI Identifier:oai:addi.ehu.eus:10810/58880
Acceso en línea:http://hdl.handle.net/10810/58880
Access Level:acceso abierto
Palabra clave:calcium silicate hydrate
Portlandite
atomistic simulation
nucleation
free energy of reaction
Descripción
Sumario:The nucleation of the C-S-H gel is a complex process, key to controlling the hydration kinetics and microstructure development of cement. In this paper, a mechanism for the crystallization step during the C-S-H gel non-classical nucleation is proposed and explored by atomistic simulation methods. In the proposed mechanism portlandite precursor monolayers undergo a chemically induced transformation by condensation of silicate dimmers, forming C-S-H monolayers. We studied by DFT and nudged elastic band the structural transformation from bulk portlandite to a tobermorite-like calcium hydroxide polymorph, and the silicate condensation reaction at portlandite surface. Then, both processes are studied together, investigating the topochemical transformation from a portlandite monolayer to a C-S-H monolayer at room conditions using targeted molecular dynamics and umbrella sampling methods. Comparing the free energy of the process with thermodynamic data we conclude that the proposed mechanism is a potential path for C-S-H formation.