Decay study of pesticide residues in apple samples

A method for monitoring pesticides in apple samples, including Soxhlet extraction, an evaporation step and capillary gas chromatography with nitrogen-phosphorus detection, is applied to a decay study of the carbamate pesticide ethiofencarb. The evaporation step is carried out by a surface nitrogen f...

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Detalhes bibliográficos
Autores: Pérez Clavijo, M., Plaza Medina, M., Sanz Asensio, J., Galbán Bernal, J. [0000-0002-8973-5104]
Formato: artículo
Estado:Versión publicada
Fecha de publicación:1996
País:España
Recursos:Universidad de La Rioja (UR)
Repositorio:RIUR. Repositorio Institucional de la Universidad de La Rioja
OAI Identifier:oai:portal.dialnet.es:doc/5bbc69deb750603269e822da
Acesso em linha:https://investigacion.unirioja.es/documentos/5bbc69deb750603269e822da
Access Level:acceso abierto
Palavra-chave:apples
carbamates
food analysis
organophosphorus compounds
pesticides
Descrição
Resumo:A method for monitoring pesticides in apple samples, including Soxhlet extraction, an evaporation step and capillary gas chromatography with nitrogen-phosphorus detection, is applied to a decay study of the carbamate pesticide ethiofencarb. The evaporation step is carried out by a surface nitrogen flow and the recoveries of ethiofencarb measured in standard solutions of ethyl acetate and apple extracts. The results of the decay studies show that ethiofencarb is degraded in the apple peel faster than in the interior of the fruit. The methodology is then applied to decay studies in the laboratory of the organophosphorus pesticides, diclofluanid, fenitrothion and malathion.