The molecular structure of Me3TiCp* in the gas phase

The thermal average molecular structure of Me3TiCp★ has been determined by gas phase electron diffraction (GED). The GED data are consistent with a molecular model in which the TiMe3 fragment has C3v symmetry and the TiCp★ fragment has C5v symmetry. No static tilt of the methyl groups attached to ti...

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Detalles Bibliográficos
Autores: Blom, R., Rypdal, K., Mena Montoro, Miguel|||0000-0001-7456-1212, Royo Gracia, Pascual, Serrano Roche, Ricardo
Tipo de recurso: artículo
Fecha de publicación:1990
País:España
Institución:Universidad de Alcalá (UAH)
Repositorio:e_Buah Biblioteca Digital Universidad de Alcalá
Idioma:inglés
OAI Identifier:oai:ebuah.uah.es:10017/4633
Acceso en línea:http://hdl.handle.net/10017/4633
https://dx.doi.org/10.1016/0022-328X(90)80155-S
Access Level:acceso abierto
Palabra clave:Gas phase electron diffraction
GED
Methyl groups
Ciencia
Química inorgánica
Science
Chemistry, inorganic
Descripción
Sumario:The thermal average molecular structure of Me3TiCp★ has been determined by gas phase electron diffraction (GED). The GED data are consistent with a molecular model in which the TiMe3 fragment has C3v symmetry and the TiCp★ fragment has C5v symmetry. No static tilt of the methyl groups attached to titanium can be detected, although a flattening of the methyl groups with Ti-C-H 103.8(1.2)° is obtained. The Ti-C(Me) bond distance is 210.7(5) pm, and the Ti-C(Cp★) distance 238.0(5) pm.