Presence of Ceramidase Activity in Electronegative LDL

Electronegative low-density lipoprotein (LDL(-)) is a minor modified fraction of human plasma LDL with several atherogenic properties. Among them is increased bioactive lipid mediator content, such as lysophosphatidylcholine (LPC), non-esterified fatty acids (NEFA), ceramide (Cer), and sphingosine (...

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Autores: Puig Calvó, Núria|||0000-0001-8235-4934, Rives Jimenez, Jose|||0009-0001-5725-9270, Estruch, Montserrat|||0000-0002-7162-4158, Aguilera-Simón, Ana|||0000-0003-1428-8212, Rotllan, Noemi|||0000-0002-0587-8045, Camacho, Mercedes|||0000-0001-5970-3294, Colomé, Núria, Canals, Francesc|||0000-0002-0650-1135, Sánchez Quesada, José Luis|||0000-0003-0224-591X, Benitez, Sonia|||0000-0003-3565-0743
Tipo de recurso: artículo
Fecha de publicación:2022
País:España
Institución:Universitat Autònoma de Barcelona
Repositorio:Dipòsit Digital de Documents de la UAB
Idioma:inglés
OAI Identifier:oai:ddd.uab.cat:280926
Acceso en línea:https://ddd.uab.cat/record/280926
https://dx.doi.org/urn:doi:10.3390/ijms24010165
Access Level:acceso abierto
Palabra clave:Ceramidase
Ceramide
Electronegative LDL
Sphingomyelinase
Sphingosine
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spelling Presence of Ceramidase Activity in Electronegative LDLPuig Calvó, Núria|||0000-0001-8235-4934Rives Jimenez, Jose|||0009-0001-5725-9270Estruch, Montserrat|||0000-0002-7162-4158Aguilera-Simón, Ana|||0000-0003-1428-8212Rotllan, Noemi|||0000-0002-0587-8045Camacho, Mercedes|||0000-0001-5970-3294Colomé, NúriaCanals, Francesc|||0000-0002-0650-1135Sánchez Quesada, José Luis|||0000-0003-0224-591XBenitez, Sonia|||0000-0003-3565-0743CeramidaseCeramideElectronegative LDLSphingomyelinaseSphingosineElectronegative low-density lipoprotein (LDL(-)) is a minor modified fraction of human plasma LDL with several atherogenic properties. Among them is increased bioactive lipid mediator content, such as lysophosphatidylcholine (LPC), non-esterified fatty acids (NEFA), ceramide (Cer), and sphingosine (Sph), which are related to the presence of some phospholipolytic activities, including platelet-activating factor acetylhydrolase (PAF-AH), phospholipase C (PLC), and sphingomyelinase (SMase), in LDL(-). However, these enzymes' activities do not explain the increased Sph content, which typically derives from Cer degradation. In the present study, we analyzed the putative presence of ceramidase (CDase) activity, which could explain the increased Sph content. Thin layer chromatography (TLC) and lipidomic analysis showed that Cer, Sph, and NEFA spontaneously increased in LDL(-) incubated alone at 37 °C, in contrast with native LDL(+). An inhibitor of neutral CDase prevented the formation of Sph and, in turn, increased Cer content in LDL(-). In addition, LDL(-) efficiently degraded fluorescently labeled Cer (NBD-Cer) to form Sph and NEFA. These observations defend the existence of the CDase-like activity's association with LDL(-). However, neither the proteomic analysis nor the Western blot detected the presence of an enzyme with known CDase activity. Further studies are thus warranted to define the origin of the CDase-like activity detected in LDL(-).Universitat Autònoma de Barcelona 22022-01-0120222022-01-01Articlehttp://purl.org/coar/resource_type/c_6501VoRhttp://purl.org/coar/version/c_970fb48d4fbd8a85info:eu-repo/semantics/articleapplication/pdfhttps://ddd.uab.cat/record/280926https://dx.doi.org/urn:doi:10.3390/ijms24010165reponame:Dipòsit Digital de Documents de la UABinstname:Universitat Autònoma de BarcelonaInglésengMinisterio de Economía y Competitividad https://doi.org/10.13039/501100003329 PI13/00364Ministerio de Economía y Competitividad https://doi.org/10.13039/501100003329 PI16/00471Instituto de Salud Carlos III https://doi.org/10.13039/501100004587 PI20/00334Ministerio de Economía y Competitividad https://doi.org/10.13039/501100003329 CB16/11/00257Ministerio de Economía y Competitividad https://doi.org/10.13039/501100003329 RD16/0019/0010open accesshttp://purl.org/coar/access_right/c_abf2Aquest document està subjecte a una llicència d'ús Creative Commons. Es permet la reproducció total o parcial, la distribució, la comunicació pública de l'obra i la creació d'obres derivades, fins i tot amb finalitats comercials, sempre i quan es reconegui l'autoria de l'obra original.https://creativecommons.org/licenses/by/4.0/info:eu-repo/semantics/openAccessoai:ddd.uab.cat:2809262026-06-06T12:50:31Z
dc.title.none.fl_str_mv Presence of Ceramidase Activity in Electronegative LDL
title Presence of Ceramidase Activity in Electronegative LDL
spellingShingle Presence of Ceramidase Activity in Electronegative LDL
Puig Calvó, Núria|||0000-0001-8235-4934
Ceramidase
Ceramide
Electronegative LDL
Sphingomyelinase
Sphingosine
title_short Presence of Ceramidase Activity in Electronegative LDL
title_full Presence of Ceramidase Activity in Electronegative LDL
title_fullStr Presence of Ceramidase Activity in Electronegative LDL
title_full_unstemmed Presence of Ceramidase Activity in Electronegative LDL
title_sort Presence of Ceramidase Activity in Electronegative LDL
dc.creator.none.fl_str_mv Puig Calvó, Núria|||0000-0001-8235-4934
Rives Jimenez, Jose|||0009-0001-5725-9270
Estruch, Montserrat|||0000-0002-7162-4158
Aguilera-Simón, Ana|||0000-0003-1428-8212
Rotllan, Noemi|||0000-0002-0587-8045
Camacho, Mercedes|||0000-0001-5970-3294
Colomé, Núria
Canals, Francesc|||0000-0002-0650-1135
Sánchez Quesada, José Luis|||0000-0003-0224-591X
Benitez, Sonia|||0000-0003-3565-0743
author Puig Calvó, Núria|||0000-0001-8235-4934
author_facet Puig Calvó, Núria|||0000-0001-8235-4934
Rives Jimenez, Jose|||0009-0001-5725-9270
Estruch, Montserrat|||0000-0002-7162-4158
Aguilera-Simón, Ana|||0000-0003-1428-8212
Rotllan, Noemi|||0000-0002-0587-8045
Camacho, Mercedes|||0000-0001-5970-3294
Colomé, Núria
Canals, Francesc|||0000-0002-0650-1135
Sánchez Quesada, José Luis|||0000-0003-0224-591X
Benitez, Sonia|||0000-0003-3565-0743
author_role author
author2 Rives Jimenez, Jose|||0009-0001-5725-9270
Estruch, Montserrat|||0000-0002-7162-4158
Aguilera-Simón, Ana|||0000-0003-1428-8212
Rotllan, Noemi|||0000-0002-0587-8045
Camacho, Mercedes|||0000-0001-5970-3294
Colomé, Núria
Canals, Francesc|||0000-0002-0650-1135
Sánchez Quesada, José Luis|||0000-0003-0224-591X
Benitez, Sonia|||0000-0003-3565-0743
author2_role author
author
author
author
author
author
author
author
author
dc.contributor.none.fl_str_mv Universitat Autònoma de Barcelona
dc.subject.none.fl_str_mv Ceramidase
Ceramide
Electronegative LDL
Sphingomyelinase
Sphingosine
topic Ceramidase
Ceramide
Electronegative LDL
Sphingomyelinase
Sphingosine
description Electronegative low-density lipoprotein (LDL(-)) is a minor modified fraction of human plasma LDL with several atherogenic properties. Among them is increased bioactive lipid mediator content, such as lysophosphatidylcholine (LPC), non-esterified fatty acids (NEFA), ceramide (Cer), and sphingosine (Sph), which are related to the presence of some phospholipolytic activities, including platelet-activating factor acetylhydrolase (PAF-AH), phospholipase C (PLC), and sphingomyelinase (SMase), in LDL(-). However, these enzymes' activities do not explain the increased Sph content, which typically derives from Cer degradation. In the present study, we analyzed the putative presence of ceramidase (CDase) activity, which could explain the increased Sph content. Thin layer chromatography (TLC) and lipidomic analysis showed that Cer, Sph, and NEFA spontaneously increased in LDL(-) incubated alone at 37 °C, in contrast with native LDL(+). An inhibitor of neutral CDase prevented the formation of Sph and, in turn, increased Cer content in LDL(-). In addition, LDL(-) efficiently degraded fluorescently labeled Cer (NBD-Cer) to form Sph and NEFA. These observations defend the existence of the CDase-like activity's association with LDL(-). However, neither the proteomic analysis nor the Western blot detected the presence of an enzyme with known CDase activity. Further studies are thus warranted to define the origin of the CDase-like activity detected in LDL(-).
publishDate 2022
dc.date.none.fl_str_mv 2
2022-01-01
2022
2022-01-01
dc.type.none.fl_str_mv Article
http://purl.org/coar/resource_type/c_6501
VoR
http://purl.org/coar/version/c_970fb48d4fbd8a85
dc.type.openaire.fl_str_mv info:eu-repo/semantics/article
format article
dc.identifier.none.fl_str_mv https://ddd.uab.cat/record/280926
https://dx.doi.org/urn:doi:10.3390/ijms24010165
url https://ddd.uab.cat/record/280926
https://dx.doi.org/urn:doi:10.3390/ijms24010165
dc.language.none.fl_str_mv Inglés
eng
language_invalid_str_mv Inglés
language eng
dc.relation.none.fl_str_mv Ministerio de Economía y Competitividad https://doi.org/10.13039/501100003329 PI13/00364
Ministerio de Economía y Competitividad https://doi.org/10.13039/501100003329 PI16/00471
Instituto de Salud Carlos III https://doi.org/10.13039/501100004587 PI20/00334
Ministerio de Economía y Competitividad https://doi.org/10.13039/501100003329 CB16/11/00257
Ministerio de Economía y Competitividad https://doi.org/10.13039/501100003329 RD16/0019/0010
dc.rights.none.fl_str_mv open access
http://purl.org/coar/access_right/c_abf2
https://creativecommons.org/licenses/by/4.0/
dc.rights.openaire.fl_str_mv info:eu-repo/semantics/openAccess
rights_invalid_str_mv open access
http://purl.org/coar/access_right/c_abf2
https://creativecommons.org/licenses/by/4.0/
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.source.none.fl_str_mv reponame:Dipòsit Digital de Documents de la UAB
instname:Universitat Autònoma de Barcelona
instname_str Universitat Autònoma de Barcelona
reponame_str Dipòsit Digital de Documents de la UAB
collection Dipòsit Digital de Documents de la UAB
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repository.mail.fl_str_mv
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