Determination of solubility parameters and thermodynamic properties in hydrocarbon-solvent systems by gas chromatography

Gas chromatography used to calculate the specific retention volume of several hydrocarbons in different chromatographic liquid phases (Squalane, Carbowax-400, Carbowax-1500, Carbowax-4000, Amine-220, Dinonyl phthalate, Tributyl phosphate and Trixylenyl phosphate). Some thermodynamic parameters, such...

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Detalles Bibliográficos
Autores: Díaz Fernández, Eva|||0000-0002-6955-4971, Cazurro, A., Ordóñez García, Salvador|||0000-0002-6529-7066, Vega Granda, Aurelio Balbino|||0000-0002-8207-9925, Coca Prados, José
Tipo de recurso: artículo
Fecha de publicación:2007
País:España
Institución:Universidad de Oviedo (UNIOVI)
Repositorio:RUO. Repositorio Institucional de la Universidad de Oviedo
Idioma:inglés
OAI Identifier:oai:digibuo.uniovi.es:10651/29242
Acceso en línea:http://hdl.handle.net/10651/29242
https://dx.doi.org/10.1590/S0104-66322007000200014
Access Level:acceso abierto
Palabra clave:Flory-Huggins interaction parameters
Gas chromatography
Polar component
Solubility parameter
Specific retention volume
Descripción
Sumario:Gas chromatography used to calculate the specific retention volume of several hydrocarbons in different chromatographic liquid phases (Squalane, Carbowax-400, Carbowax-1500, Carbowax-4000, Amine-220, Dinonyl phthalate, Tributyl phosphate and Trixylenyl phosphate). Some thermodynamic parameters, such as enthalpy of sorption and Flory-Huggins parameters relating the interaction between liquid phases and solutes, were also calculated from the determined retention volumes. Liquid phase solubility parameters of Squalane, Carbowax-400, Carbowax-1500 and Carbowax-4000 at 80 °C as well as the polar and apolar components were calculated too. A new model was proposed to correlate polar contribution to the solubility parameter of a liquid phase with the specific retention volume of a solute in this liquid phase