Innovative insights in a plug flow microreactor for operando X-ray studies

© 2013 International Union of Crystallography

Detalles Bibliográficos
Autores: Figueroa, Santiago J. A., Gibson, Dean, Mairs, Trevor, Pasternak, Sebastien, Newton, Mark A., Michiel, Marco Di, Andrieux, Jerome, Christoforidis, Konstantinos, Iglesias Juez, Ana, Prestipino, Carmelo, Fernández, M.
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2013
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/181873
Acceso en línea:http://hdl.handle.net/10261/181873
Access Level:acceso abierto
Palabra clave:In situ X-ray studies
Catalysis
Plug flow microreactors
Operando X-ray studies
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spelling Innovative insights in a plug flow microreactor for operando X-ray studiesFigueroa, Santiago J. A.Gibson, DeanMairs, TrevorPasternak, SebastienNewton, Mark A.Michiel, Marco DiAndrieux, JeromeChristoforidis, KonstantinosIglesias Juez, AnaPrestipino, CarmeloFernández, M.In situ X-ray studiesCatalysisPlug flow microreactorsOperando X-ray studies© 2013 International Union of CrystallographyDifferent solutions have been proposed over the years to optimize control of the temperature and atmosphere over a catalyst in order to reach an ideal reactor behavior. Here, a new innovative solution which aims to minimize temperature gradients along the catalyst bed is demonstrated. This was attained by focusing the infrared radiation generated from the heating elements onto the catalyst bed with the aid of an aluminium shield. This method yields a ∼0.13Kmm-1 axial temperature gradient ranging from 960 to 1173K. With the selection of appropriate capillaries, pressures of 20bar (2MPa) can be attained.The research leading to these results has been funded by the Spanish CICYT (CTQ2010-14872/BQU) and the European Union's Seventh Framework Programme (FP7/2007–2013) under grant agreement No. 253445. KCC acknowledges Marie Curie Action – Intra-European Fellowship (FP7-PEOPLE-2009-IEF-253445) for a postdoctoral fellowship.Peer ReviewedInternational Union of CrystallographyComisión Interministerial de Ciencia y Tecnología, CICYT (España)European CommissionConsejo Superior de Investigaciones Científicas [https://ror.org/02gfc7t72]2019201920132019info:eu-repo/semantics/articlehttp://purl.org/coar/resource_type/c_6501Publisher's versioninfo:eu-repo/semantics/publishedVersionhttp://hdl.handle.net/10261/181873reponame:DIGITAL.CSIC. Repositorio Institucional del CSICinstname:Consejo Superior de Investigaciones Científicas (CSIC)Inglés#PLACEHOLDER_PARENT_METADATA_VALUE#info:eu-repo/grantAgreement/EC/FP7/253445https://doi.org/10.1107/S0021889813018839Síinfo:eu-repo/semantics/openAccessoai:digital.csic.es:10261/1818732026-05-22T06:33:51Z
dc.title.none.fl_str_mv Innovative insights in a plug flow microreactor for operando X-ray studies
title Innovative insights in a plug flow microreactor for operando X-ray studies
spellingShingle Innovative insights in a plug flow microreactor for operando X-ray studies
Figueroa, Santiago J. A.
In situ X-ray studies
Catalysis
Plug flow microreactors
Operando X-ray studies
title_short Innovative insights in a plug flow microreactor for operando X-ray studies
title_full Innovative insights in a plug flow microreactor for operando X-ray studies
title_fullStr Innovative insights in a plug flow microreactor for operando X-ray studies
title_full_unstemmed Innovative insights in a plug flow microreactor for operando X-ray studies
title_sort Innovative insights in a plug flow microreactor for operando X-ray studies
dc.creator.none.fl_str_mv Figueroa, Santiago J. A.
Gibson, Dean
Mairs, Trevor
Pasternak, Sebastien
Newton, Mark A.
Michiel, Marco Di
Andrieux, Jerome
Christoforidis, Konstantinos
Iglesias Juez, Ana
Prestipino, Carmelo
Fernández, M.
author Figueroa, Santiago J. A.
author_facet Figueroa, Santiago J. A.
Gibson, Dean
Mairs, Trevor
Pasternak, Sebastien
Newton, Mark A.
Michiel, Marco Di
Andrieux, Jerome
Christoforidis, Konstantinos
Iglesias Juez, Ana
Prestipino, Carmelo
Fernández, M.
author_role author
author2 Gibson, Dean
Mairs, Trevor
Pasternak, Sebastien
Newton, Mark A.
Michiel, Marco Di
Andrieux, Jerome
Christoforidis, Konstantinos
Iglesias Juez, Ana
Prestipino, Carmelo
Fernández, M.
author2_role author
author
author
author
author
author
author
author
author
author
dc.contributor.none.fl_str_mv Comisión Interministerial de Ciencia y Tecnología, CICYT (España)
European Commission
Consejo Superior de Investigaciones Científicas [https://ror.org/02gfc7t72]
dc.subject.none.fl_str_mv In situ X-ray studies
Catalysis
Plug flow microreactors
Operando X-ray studies
topic In situ X-ray studies
Catalysis
Plug flow microreactors
Operando X-ray studies
description © 2013 International Union of Crystallography
publishDate 2013
dc.date.none.fl_str_mv 2013
2019
2019
2019
dc.type.none.fl_str_mv info:eu-repo/semantics/article
http://purl.org/coar/resource_type/c_6501
Publisher's version
info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/10261/181873
url http://hdl.handle.net/10261/181873
dc.language.none.fl_str_mv Inglés
language_invalid_str_mv Inglés
dc.relation.none.fl_str_mv #PLACEHOLDER_PARENT_METADATA_VALUE#
info:eu-repo/grantAgreement/EC/FP7/253445
https://doi.org/10.1107/S0021889813018839
Sí
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.publisher.none.fl_str_mv International Union of Crystallography
publisher.none.fl_str_mv International Union of Crystallography
dc.source.none.fl_str_mv reponame:DIGITAL.CSIC. Repositorio Institucional del CSIC
instname:Consejo Superior de Investigaciones Científicas (CSIC)
instname_str Consejo Superior de Investigaciones Científicas (CSIC)
reponame_str DIGITAL.CSIC. Repositorio Institucional del CSIC
collection DIGITAL.CSIC. Repositorio Institucional del CSIC
repository.name.fl_str_mv
repository.mail.fl_str_mv
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score 15,811543

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