Sonochemical synthesis of a novel nanoscale 1D lead(II) [Pb2(L)2(I)4]n coordination Polymer, survey of temperature, reaction time parameters

One new lead(II) coordination supramolecular complex (CSC) (1D), [Pb(L)(I)], L = CHN (1-methyl imidazole), has been synthesized under different experimental conditions. Micrometric crystals (bulk) or nano-sized materials have been obtained depending on using the branch tube method or sonochemical ir...

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Autores: Hayati, Payam|||0000-0002-9312-3143, Suárez García, Salvio|||0000-0002-4156-0579, Gutiérrez Alonso, Ángel, Ruiz-Molina, Daniel|||0000-0002-6844-8421, Morsali, Ali|||0000-0002-1828-7287, Rezvani, Ali Reza
Formato: artículo
Fecha de publicación:2018
País:España
Recursos:Universitat Autònoma de Barcelona
Repositorio:Dipòsit Digital de Documents de la UAB
Idioma:inglés
OAI Identifier:oai:ddd.uab.cat:220658
Acesso em linha:https://ddd.uab.cat/record/220658
https://dx.doi.org/urn:doi:10.1016/j.ultsonch.2017.11.033
Access Level:acceso abierto
Palavra-chave:Coordination polymer
Sonochemical process
Ultrasound irradiation
Morphology
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spelling Sonochemical synthesis of a novel nanoscale 1D lead(II) [Pb2(L)2(I)4]n coordination Polymer, survey of temperature, reaction time parametersHayati, Payam|||0000-0002-9312-3143Suárez García, Salvio|||0000-0002-4156-0579Gutiérrez Alonso, ÁngelRuiz-Molina, Daniel|||0000-0002-6844-8421Morsali, Ali|||0000-0002-1828-7287Rezvani, Ali RezaCoordination polymerSonochemical processUltrasound irradiationMorphologyOne new lead(II) coordination supramolecular complex (CSC) (1D), [Pb(L)(I)], L = CHN (1-methyl imidazole), has been synthesized under different experimental conditions. Micrometric crystals (bulk) or nano-sized materials have been obtained depending on using the branch tube method or sonochemical irradiation. All materials have been characterized by scanning electron microscopy (SEM), powder X-ray diffraction (PXRD) and FT-IR spectroscopy. Single crystal X-ray analyses on complex 1 showed that Pb ion is 4-coordinated. Topological analysis shows that the complex 1 is 2,3,5C2 net. Finally, the role of reaction time and temperature on the growth and final morphology of the structures obtained by sonochemical irradiation have been studied. 22018-01-0120182018-01-01Articlehttp://purl.org/coar/resource_type/c_6501SMURhttp://purl.org/coar/version/c_71e4c1898caa6e32info:eu-repo/semantics/articleapplication/pdfhttps://ddd.uab.cat/record/220658https://dx.doi.org/urn:doi:10.1016/j.ultsonch.2017.11.033reponame:Dipòsit Digital de Documents de la UABinstname:Universitat Autònoma de BarcelonaInglésengMinisterio de Economía y Competitividad https://doi.org/10.13039/501100003329 MAT2015-70615-RMinisterio de Economía y Competitividad https://doi.org/10.13039/501100003329 SEV-2013-0295open accesshttp://purl.org/coar/access_right/c_abf2Aquest document està subjecte a una llicència d'ús Creative Commons. Es permet la reproducció total o parcial, la distribució, i la comunicació pública de l'obra, sempre que no sigui amb finalitats comercials, i sempre que es reconegui l'autoria de l'obra original. No es permet la creació d'obres derivades.https://creativecommons.org/licenses/by-nc-nd/4.0/info:eu-repo/semantics/openAccessoai:ddd.uab.cat:2206582026-06-06T12:50:31Z
dc.title.none.fl_str_mv Sonochemical synthesis of a novel nanoscale 1D lead(II) [Pb2(L)2(I)4]n coordination Polymer, survey of temperature, reaction time parameters
title Sonochemical synthesis of a novel nanoscale 1D lead(II) [Pb2(L)2(I)4]n coordination Polymer, survey of temperature, reaction time parameters
spellingShingle Sonochemical synthesis of a novel nanoscale 1D lead(II) [Pb2(L)2(I)4]n coordination Polymer, survey of temperature, reaction time parameters
Hayati, Payam|||0000-0002-9312-3143
Coordination polymer
Sonochemical process
Ultrasound irradiation
Morphology
title_short Sonochemical synthesis of a novel nanoscale 1D lead(II) [Pb2(L)2(I)4]n coordination Polymer, survey of temperature, reaction time parameters
title_full Sonochemical synthesis of a novel nanoscale 1D lead(II) [Pb2(L)2(I)4]n coordination Polymer, survey of temperature, reaction time parameters
title_fullStr Sonochemical synthesis of a novel nanoscale 1D lead(II) [Pb2(L)2(I)4]n coordination Polymer, survey of temperature, reaction time parameters
title_full_unstemmed Sonochemical synthesis of a novel nanoscale 1D lead(II) [Pb2(L)2(I)4]n coordination Polymer, survey of temperature, reaction time parameters
title_sort Sonochemical synthesis of a novel nanoscale 1D lead(II) [Pb2(L)2(I)4]n coordination Polymer, survey of temperature, reaction time parameters
dc.creator.none.fl_str_mv Hayati, Payam|||0000-0002-9312-3143
Suárez García, Salvio|||0000-0002-4156-0579
Gutiérrez Alonso, Ángel
Ruiz-Molina, Daniel|||0000-0002-6844-8421
Morsali, Ali|||0000-0002-1828-7287
Rezvani, Ali Reza
author Hayati, Payam|||0000-0002-9312-3143
author_facet Hayati, Payam|||0000-0002-9312-3143
Suárez García, Salvio|||0000-0002-4156-0579
Gutiérrez Alonso, Ángel
Ruiz-Molina, Daniel|||0000-0002-6844-8421
Morsali, Ali|||0000-0002-1828-7287
Rezvani, Ali Reza
author_role author
author2 Suárez García, Salvio|||0000-0002-4156-0579
Gutiérrez Alonso, Ángel
Ruiz-Molina, Daniel|||0000-0002-6844-8421
Morsali, Ali|||0000-0002-1828-7287
Rezvani, Ali Reza
author2_role author
author
author
author
author
dc.subject.none.fl_str_mv Coordination polymer
Sonochemical process
Ultrasound irradiation
Morphology
topic Coordination polymer
Sonochemical process
Ultrasound irradiation
Morphology
description One new lead(II) coordination supramolecular complex (CSC) (1D), [Pb(L)(I)], L = CHN (1-methyl imidazole), has been synthesized under different experimental conditions. Micrometric crystals (bulk) or nano-sized materials have been obtained depending on using the branch tube method or sonochemical irradiation. All materials have been characterized by scanning electron microscopy (SEM), powder X-ray diffraction (PXRD) and FT-IR spectroscopy. Single crystal X-ray analyses on complex 1 showed that Pb ion is 4-coordinated. Topological analysis shows that the complex 1 is 2,3,5C2 net. Finally, the role of reaction time and temperature on the growth and final morphology of the structures obtained by sonochemical irradiation have been studied.
publishDate 2018
dc.date.none.fl_str_mv 2
2018-01-01
2018
2018-01-01
dc.type.none.fl_str_mv Article
http://purl.org/coar/resource_type/c_6501
SMUR
http://purl.org/coar/version/c_71e4c1898caa6e32
dc.type.openaire.fl_str_mv info:eu-repo/semantics/article
format article
dc.identifier.none.fl_str_mv https://ddd.uab.cat/record/220658
https://dx.doi.org/urn:doi:10.1016/j.ultsonch.2017.11.033
url https://ddd.uab.cat/record/220658
https://dx.doi.org/urn:doi:10.1016/j.ultsonch.2017.11.033
dc.language.none.fl_str_mv Inglés
eng
language_invalid_str_mv Inglés
language eng
dc.relation.none.fl_str_mv Ministerio de Economía y Competitividad https://doi.org/10.13039/501100003329 MAT2015-70615-R
Ministerio de Economía y Competitividad https://doi.org/10.13039/501100003329 SEV-2013-0295
dc.rights.none.fl_str_mv open access
http://purl.org/coar/access_right/c_abf2
https://creativecommons.org/licenses/by-nc-nd/4.0/
dc.rights.openaire.fl_str_mv info:eu-repo/semantics/openAccess
rights_invalid_str_mv open access
http://purl.org/coar/access_right/c_abf2
https://creativecommons.org/licenses/by-nc-nd/4.0/
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.source.none.fl_str_mv reponame:Dipòsit Digital de Documents de la UAB
instname:Universitat Autònoma de Barcelona
instname_str Universitat Autònoma de Barcelona
reponame_str Dipòsit Digital de Documents de la UAB
collection Dipòsit Digital de Documents de la UAB
repository.name.fl_str_mv
repository.mail.fl_str_mv
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