Study of the Critical Points and the Role of the Pores and Viscosity in Carbamazepine Hydrophilic Matrix Tablets

Percolation theory has been applied to estimate the Hypromellose (HPMC) percolation thresholds and the influence of the polymer viscosity and the initial porosity on these thresholds in carbamazepine multicomponent matrix formulations. Different batches containing two viscosity grades of HPMC as hyd...

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Detalles Bibliográficos
Autores: Aguilar de Leyva, Mercedes Ángela, Cifuentes, Celia, Rajabi-Siahboomi, Ali R., Caraballo Rodríguez, Isidoro
Tipo de recurso: artículo
Estado:Versión aceptada para publicación
Fecha de publicación:2012
País:España
Institución:Universidad de Sevilla (US)
Repositorio:idUS. Depósito de Investigación de la Universidad de Sevilla
OAI Identifier:oai:idus.us.es:11441/162854
Acceso en línea:https://hdl.handle.net/11441/162854
https://doi.org/10.1016/j.ejpb.2011.09.007
Access Level:acceso abierto
Palabra clave:Hydroxypropylmethyl cellulose
Hydrophilic matrices
Carbamazepine
Tablet porosity
Percolation threshold
Critical points
Extended release
Descripción
Sumario:Percolation theory has been applied to estimate the Hypromellose (HPMC) percolation thresholds and the influence of the polymer viscosity and the initial porosity on these thresholds in carbamazepine multicomponent matrix formulations. Different batches containing two viscosity grades of HPMC as hydrophilic matrix forming polymer, MCC and lactose as fillers, and a lubricant mixture have been manufactured varying the compression pressure in order to obtain matrices with three levels of initial porosity. The results suggested the existence of an excipient percolation threshold between 13 and 15% v/v of HPMC for the different batches prepared. It has been found that the percolation threshold for this polymer is independent on the formulation factors studied in this paper: polymer viscosity and initial porosity of the matrices.