Long-lasting low fluorinated stainless steel hierarchical surfaces for omniphobic, anti-fouling and anti-icing applications

Stainless steel (SS) alloys are prevalent in many industries, household appliances or other commodities, where a strict control of surface properties is required to tailor their interaction with the environment. In this work we report a new procedure of stainless steel surface processing that provid...

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Autores: Montes, Laura, Rico, Víctor, Núñez-Gálvez, Fernando, Arenas, María Ángeles, Conde del Campo, Ana, López Flores, Víctor, Espinós, Juan P., Borrás, Ana, González-Elipe, Agustín R., López Santos, Carmen
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2024
País:España
Institución:Universidad de Sevilla (US)
Repositorio:idUS. Depósito de Investigación de la Universidad de Sevilla
OAI Identifier:oai:idus.us.es:11441/160603
Acceso en línea:https://hdl.handle.net/11441/160603
https://doi.org/10.1016/j.surfin.2024.104167
Access Level:acceso abierto
Palabra clave:Stainless steel
Nanostructures
Fluorination
Anti-fouling
Anti-icing
Superhydrophobicity
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spelling Long-lasting low fluorinated stainless steel hierarchical surfaces for omniphobic, anti-fouling and anti-icing applicationsMontes, LauraRico, VíctorNúñez-Gálvez, FernandoArenas, María ÁngelesConde del Campo, AnaLópez Flores, VíctorEspinós, Juan P.Borrás, AnaGonzález-Elipe, Agustín R.López Santos, CarmenStainless steelNanostructuresFluorinationAnti-foulingAnti-icingSuperhydrophobicityStainless steel (SS) alloys are prevalent in many industries, household appliances or other commodities, where a strict control of surface properties is required to tailor their interaction with the environment. In this work we report a new procedure of stainless steel surface processing that provides a multifunctional response including superhydrophobicity, omniphobicity, self-cleaning, anti-fouling and effective anti-icing capacity, while still preserving a corrosion resistance similar to that of this material in compact form. The method consists of a first nanostructuration step followed by a low fluorination. The nanostructured surfaces presented a dual scale roughness of hierarchical character. The liquid free approach developed in this work to get this singular surface nanostructuration entails a first laser treatment of stainless steel flat substrates, followed by the deposition of a nanostructured thin layer of this material by electron beam evaporation in an oblique angle configuration. The resulting hierarchical surfaces were subjected to fluorination by: (i) the plasma-assisted deposition of a thin Teflon-like coating or (ii) the grafting of fluorinated molecules. The self-cleanable, anti-adherent and ice repellent character of the resulting low fluorinated surfaces outperformed the behaviour of classical slippery surfaces obtained by the infusion of high amounts of fluorinated liquids. These hierarchical SS surfaces withstood mild abrasion tests and the effect of water jets. Moreover, the corrosion behaviour of the fluorinated surfaces determined through their potentiodynamic analysis revealed a similar corrosion resistance than the flat SS substrates. Outstandingly, after these corrosion tests, the fluorinated samples obtained by grafting preserved their surface functionalities without significant degradation. The high mechanical and chemical stability of these low fluorinated samples support their usage for a large variety of applications.Institute of Materials Science of Seville (Spain)ElsevierFísica Aplicada IFQM196: Nanotecnología en Superficies y PlasmaEuropean Union (UE). H2020Ministerio de Ciencia e Innovación (MICIN). EspañaEuropean Commission (EC). Fondo Europeo de Desarrollo Regional (FEDER)Universidad de Sevilla2024info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionapplication/pdfapplication/pdfhttps://hdl.handle.net/11441/160603https://doi.org/10.1016/j.surfin.2024.104167reponame:idUS. Depósito de Investigación de la Universidad de Sevillainstname:Universidad de Sevilla (US)InglésEU H2020 899352TED2021-130916B-I00PID2022-143120OB-I00VII Plan Propio de Investigación y Transferenciahttps://www.sciencedirect.com/science/article/pii/S2468023024003262?via%3Dihubinfo:eu-repo/semantics/openAccessoai:idus.us.es:11441/1606032026-06-17T12:51:07Z
dc.title.none.fl_str_mv Long-lasting low fluorinated stainless steel hierarchical surfaces for omniphobic, anti-fouling and anti-icing applications
title Long-lasting low fluorinated stainless steel hierarchical surfaces for omniphobic, anti-fouling and anti-icing applications
spellingShingle Long-lasting low fluorinated stainless steel hierarchical surfaces for omniphobic, anti-fouling and anti-icing applications
Montes, Laura
Stainless steel
Nanostructures
Fluorination
Anti-fouling
Anti-icing
Superhydrophobicity
title_short Long-lasting low fluorinated stainless steel hierarchical surfaces for omniphobic, anti-fouling and anti-icing applications
title_full Long-lasting low fluorinated stainless steel hierarchical surfaces for omniphobic, anti-fouling and anti-icing applications
title_fullStr Long-lasting low fluorinated stainless steel hierarchical surfaces for omniphobic, anti-fouling and anti-icing applications
title_full_unstemmed Long-lasting low fluorinated stainless steel hierarchical surfaces for omniphobic, anti-fouling and anti-icing applications
title_sort Long-lasting low fluorinated stainless steel hierarchical surfaces for omniphobic, anti-fouling and anti-icing applications
dc.creator.none.fl_str_mv Montes, Laura
Rico, Víctor
Núñez-Gálvez, Fernando
Arenas, María Ángeles
Conde del Campo, Ana
López Flores, Víctor
Espinós, Juan P.
Borrás, Ana
González-Elipe, Agustín R.
López Santos, Carmen
author Montes, Laura
author_facet Montes, Laura
Rico, Víctor
Núñez-Gálvez, Fernando
Arenas, María Ángeles
Conde del Campo, Ana
López Flores, Víctor
Espinós, Juan P.
Borrás, Ana
González-Elipe, Agustín R.
López Santos, Carmen
author_role author
author2 Rico, Víctor
Núñez-Gálvez, Fernando
Arenas, María Ángeles
Conde del Campo, Ana
López Flores, Víctor
Espinós, Juan P.
Borrás, Ana
González-Elipe, Agustín R.
López Santos, Carmen
author2_role author
author
author
author
author
author
author
author
author
dc.contributor.none.fl_str_mv Física Aplicada I
FQM196: Nanotecnología en Superficies y Plasma
European Union (UE). H2020
Ministerio de Ciencia e Innovación (MICIN). España
European Commission (EC). Fondo Europeo de Desarrollo Regional (FEDER)
Universidad de Sevilla
dc.subject.none.fl_str_mv Stainless steel
Nanostructures
Fluorination
Anti-fouling
Anti-icing
Superhydrophobicity
topic Stainless steel
Nanostructures
Fluorination
Anti-fouling
Anti-icing
Superhydrophobicity
description Stainless steel (SS) alloys are prevalent in many industries, household appliances or other commodities, where a strict control of surface properties is required to tailor their interaction with the environment. In this work we report a new procedure of stainless steel surface processing that provides a multifunctional response including superhydrophobicity, omniphobicity, self-cleaning, anti-fouling and effective anti-icing capacity, while still preserving a corrosion resistance similar to that of this material in compact form. The method consists of a first nanostructuration step followed by a low fluorination. The nanostructured surfaces presented a dual scale roughness of hierarchical character. The liquid free approach developed in this work to get this singular surface nanostructuration entails a first laser treatment of stainless steel flat substrates, followed by the deposition of a nanostructured thin layer of this material by electron beam evaporation in an oblique angle configuration. The resulting hierarchical surfaces were subjected to fluorination by: (i) the plasma-assisted deposition of a thin Teflon-like coating or (ii) the grafting of fluorinated molecules. The self-cleanable, anti-adherent and ice repellent character of the resulting low fluorinated surfaces outperformed the behaviour of classical slippery surfaces obtained by the infusion of high amounts of fluorinated liquids. These hierarchical SS surfaces withstood mild abrasion tests and the effect of water jets. Moreover, the corrosion behaviour of the fluorinated surfaces determined through their potentiodynamic analysis revealed a similar corrosion resistance than the flat SS substrates. Outstandingly, after these corrosion tests, the fluorinated samples obtained by grafting preserved their surface functionalities without significant degradation. The high mechanical and chemical stability of these low fluorinated samples support their usage for a large variety of applications.
publishDate 2024
dc.date.none.fl_str_mv 2024
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv https://hdl.handle.net/11441/160603
https://doi.org/10.1016/j.surfin.2024.104167
url https://hdl.handle.net/11441/160603
https://doi.org/10.1016/j.surfin.2024.104167
dc.language.none.fl_str_mv Inglés
language_invalid_str_mv Inglés
dc.relation.none.fl_str_mv EU H2020 899352
TED2021-130916B-I00
PID2022-143120OB-I00
VII Plan Propio de Investigación y Transferencia
https://www.sciencedirect.com/science/article/pii/S2468023024003262?via%3Dihub
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
application/pdf
dc.publisher.none.fl_str_mv Elsevier
publisher.none.fl_str_mv Elsevier
dc.source.none.fl_str_mv reponame:idUS. Depósito de Investigación de la Universidad de Sevilla
instname:Universidad de Sevilla (US)
instname_str Universidad de Sevilla (US)
reponame_str idUS. Depósito de Investigación de la Universidad de Sevilla
collection idUS. Depósito de Investigación de la Universidad de Sevilla
repository.name.fl_str_mv
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