Cryoconcentration in block assisted by centrifugation-vacuum to pomegranate juice: A new improved method

Cryoconcentration is a technique in which the concentrate fraction preserves the thermolabile bioactive compounds of fruit juices. Separation of the concentrated juice fraction is a critical step that depends on the concentrate’s operating temperature and freezing point. Some systems use gravity for...

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Autores: Vásquez Castillo, Flor de María|||0000-0002-4665-8938, Hernández Yáñez, Eduard|||0000-0002-5337-6947, Achaerandio Puente, María Isabel|||0000-0002-0387-6118
Tipo de recurso: artículo
Fecha de publicación:2024
País:España
Institución:Universitat Politècnica de Catalunya (UPC)
Repositorio:UPCommons. Portal del coneixement obert de la UPC
Idioma:inglés
OAI Identifier:oai:upcommons.upc.edu:2117/426858
Acceso en línea:https://hdl.handle.net/2117/426858
https://dx.doi.org/10.1007/s11947-024-03472-3
Access Level:acceso abierto
Palabra clave:Block freeze concentration
Fruit juice
Non-thermal treatment
Bioactive compounds
Punica granatum
Àrees temàtiques de la UPC::Enginyeria agroalimentària::Indústries agroalimentàries::Begudes
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repository_id_str
spelling Cryoconcentration in block assisted by centrifugation-vacuum to pomegranate juice: A new improved methodVásquez Castillo, Flor de María|||0000-0002-4665-8938Hernández Yáñez, Eduard|||0000-0002-5337-6947Achaerandio Puente, María Isabel|||0000-0002-0387-6118Block freeze concentrationFruit juiceNon-thermal treatmentBioactive compoundsPunica granatumÀrees temàtiques de la UPC::Enginyeria agroalimentària::Indústries agroalimentàries::BegudesCryoconcentration is a technique in which the concentrate fraction preserves the thermolabile bioactive compounds of fruit juices. Separation of the concentrated juice fraction is a critical step that depends on the concentrate’s operating temperature and freezing point. Some systems use gravity forces for separation, resulting in low efciency. Centrifugation force is also used to separate the concentrate and ice fraction in the frozen juice to improve the process yield. This work aims to investigate a new system where centrifugation and vacuum are combined in successive stages, cryoconcentration in block assisted by centrifugation-vacuum (V-CABC), and compare it with centrifugation-assisted block cryoconcentration (CABC). The conditions evaluated were for CABC: centrifugation speed 40, 750, and 2360 RCF (relative centrifugal force), time of 10 min, 35 min, and 60 min, and for V-CABC: same as for CABC and 20 kPa (absolute pressure) for 10 min. With the CABC, the best concentration index (CI) is obtained with shorter times, while the solute yield (SY) increases with time and centrifugation speed. With the application of additional vacuum (V-CABC) the parameters improved obtaining a concentrated juice with 50.4–54.9°Brix, 3.5–3.8 of CI; 39.3–66.7% of SY, 81.5–90.2% of efciency (Ef, %) and 4763–5665 mg GAE/L of total phenolic compounds (TPC). The best conditions were 2360 RCF for 10 min with 20 kPa for 10 min. V-CABC might be a promising technique for obtaining high-quality concentrated pomegranate juice.Objectius de Desenvolupament Sostenible::12 - Producció i Consum ResponsablesObjectius de Desenvolupament Sostenible::9 - Indústria, Innovació i InfraestructuraSpringer20242024-06-1820252025-03-21journal articlehttp://purl.org/coar/resource_type/c_6501AMhttp://purl.org/coar/version/c_ab4af688f83e57aainfo:eu-repo/semantics/articleapplication/pdfhttps://hdl.handle.net/2117/426858https://dx.doi.org/10.1007/s11947-024-03472-3reponame:UPCommons. Portal del coneixement obert de la UPCinstname:Universitat Politècnica de Catalunya (UPC)Inglésengopen accesshttp://purl.org/coar/access_right/c_abf2info:eu-repo/semantics/openAccessoai:upcommons.upc.edu:2117/4268582026-05-27T15:37:01Z
dc.title.none.fl_str_mv Cryoconcentration in block assisted by centrifugation-vacuum to pomegranate juice: A new improved method
title Cryoconcentration in block assisted by centrifugation-vacuum to pomegranate juice: A new improved method
spellingShingle Cryoconcentration in block assisted by centrifugation-vacuum to pomegranate juice: A new improved method
Vásquez Castillo, Flor de María|||0000-0002-4665-8938
Block freeze concentration
Fruit juice
Non-thermal treatment
Bioactive compounds
Punica granatum
Àrees temàtiques de la UPC::Enginyeria agroalimentària::Indústries agroalimentàries::Begudes
title_short Cryoconcentration in block assisted by centrifugation-vacuum to pomegranate juice: A new improved method
title_full Cryoconcentration in block assisted by centrifugation-vacuum to pomegranate juice: A new improved method
title_fullStr Cryoconcentration in block assisted by centrifugation-vacuum to pomegranate juice: A new improved method
title_full_unstemmed Cryoconcentration in block assisted by centrifugation-vacuum to pomegranate juice: A new improved method
title_sort Cryoconcentration in block assisted by centrifugation-vacuum to pomegranate juice: A new improved method
dc.creator.none.fl_str_mv Vásquez Castillo, Flor de María|||0000-0002-4665-8938
Hernández Yáñez, Eduard|||0000-0002-5337-6947
Achaerandio Puente, María Isabel|||0000-0002-0387-6118
author Vásquez Castillo, Flor de María|||0000-0002-4665-8938
author_facet Vásquez Castillo, Flor de María|||0000-0002-4665-8938
Hernández Yáñez, Eduard|||0000-0002-5337-6947
Achaerandio Puente, María Isabel|||0000-0002-0387-6118
author_role author
author2 Hernández Yáñez, Eduard|||0000-0002-5337-6947
Achaerandio Puente, María Isabel|||0000-0002-0387-6118
author2_role author
author
dc.subject.none.fl_str_mv Block freeze concentration
Fruit juice
Non-thermal treatment
Bioactive compounds
Punica granatum
Àrees temàtiques de la UPC::Enginyeria agroalimentària::Indústries agroalimentàries::Begudes
topic Block freeze concentration
Fruit juice
Non-thermal treatment
Bioactive compounds
Punica granatum
Àrees temàtiques de la UPC::Enginyeria agroalimentària::Indústries agroalimentàries::Begudes
description Cryoconcentration is a technique in which the concentrate fraction preserves the thermolabile bioactive compounds of fruit juices. Separation of the concentrated juice fraction is a critical step that depends on the concentrate’s operating temperature and freezing point. Some systems use gravity forces for separation, resulting in low efciency. Centrifugation force is also used to separate the concentrate and ice fraction in the frozen juice to improve the process yield. This work aims to investigate a new system where centrifugation and vacuum are combined in successive stages, cryoconcentration in block assisted by centrifugation-vacuum (V-CABC), and compare it with centrifugation-assisted block cryoconcentration (CABC). The conditions evaluated were for CABC: centrifugation speed 40, 750, and 2360 RCF (relative centrifugal force), time of 10 min, 35 min, and 60 min, and for V-CABC: same as for CABC and 20 kPa (absolute pressure) for 10 min. With the CABC, the best concentration index (CI) is obtained with shorter times, while the solute yield (SY) increases with time and centrifugation speed. With the application of additional vacuum (V-CABC) the parameters improved obtaining a concentrated juice with 50.4–54.9°Brix, 3.5–3.8 of CI; 39.3–66.7% of SY, 81.5–90.2% of efciency (Ef, %) and 4763–5665 mg GAE/L of total phenolic compounds (TPC). The best conditions were 2360 RCF for 10 min with 20 kPa for 10 min. V-CABC might be a promising technique for obtaining high-quality concentrated pomegranate juice.
publishDate 2024
dc.date.none.fl_str_mv 2024
2024-06-18
2025
2025-03-21
dc.type.none.fl_str_mv journal article
http://purl.org/coar/resource_type/c_6501
AM
http://purl.org/coar/version/c_ab4af688f83e57aa
dc.type.openaire.fl_str_mv info:eu-repo/semantics/article
format article
dc.identifier.none.fl_str_mv https://hdl.handle.net/2117/426858
https://dx.doi.org/10.1007/s11947-024-03472-3
url https://hdl.handle.net/2117/426858
https://dx.doi.org/10.1007/s11947-024-03472-3
dc.language.none.fl_str_mv Inglés
eng
language_invalid_str_mv Inglés
language eng
dc.rights.none.fl_str_mv open access
http://purl.org/coar/access_right/c_abf2
dc.rights.openaire.fl_str_mv info:eu-repo/semantics/openAccess
rights_invalid_str_mv open access
http://purl.org/coar/access_right/c_abf2
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Springer
publisher.none.fl_str_mv Springer
dc.source.none.fl_str_mv reponame:UPCommons. Portal del coneixement obert de la UPC
instname:Universitat Politècnica de Catalunya (UPC)
instname_str Universitat Politècnica de Catalunya (UPC)
reponame_str UPCommons. Portal del coneixement obert de la UPC
collection UPCommons. Portal del coneixement obert de la UPC
repository.name.fl_str_mv
repository.mail.fl_str_mv
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