Application of thermal analysis and kinetic predictions to YBCO films prepared by chemical solution deposition methods

Fluorine-based chemical solution deposition routes to prepare YBa2Cu3O7-∂ films were characterized with the aid of thermal analysis techniques. Thermogravimetric analysis and X-ray diffraction were applied to characterize the main steps of the fluorine-based route: pyrolysis of the organic material...

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Detalles Bibliográficos
Autores: Rasi, Silvia, Farjas Silva, Jordi, Roura Grabulosa, Pere
Tipo de recurso: artículo
Estado:Versión aceptada para publicación
Fecha de publicación:2020
País:España
Institución:Varias* (Consorci de Biblioteques Universitáries de Catalunya, Centre de Serveis Científics i Acadèmics de Catalunya)
Repositorio:Recercat. Dipósit de la Recerca de Catalunya
OAI Identifier:oai:recercat.cat:10256/18688
Acceso en línea:http://hdl.handle.net/10256/18688
Access Level:acceso abierto
Palabra clave:Cinètica química
Anàlisi tèrmica
Chemical kinetics
Thermal analysis
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spelling Application of thermal analysis and kinetic predictions to YBCO films prepared by chemical solution deposition methodsRasi, SilviaFarjas Silva, JordiRoura Grabulosa, PereCinètica químicaAnàlisi tèrmicaChemical kineticsThermal analysisFluorine-based chemical solution deposition routes to prepare YBa2Cu3O7-∂ films were characterized with the aid of thermal analysis techniques. Thermogravimetric analysis and X-ray diffraction were applied to characterize the main steps of the fluorine-based route: pyrolysis of the organic material and growth of the oxide. The difference between the thermal behaviour of films and powders in fluorine-based chemical solution deposition route is reiterated to justify the importance of the study of films. Finally, the kinetic analysis is used to predict the mass evolution of the pyrolysis for an arbitrary temperature program with the aim to optimize this treatment to minimize film porosity and crack formationThis work was funded by Ministerio de Ciencia, Innovación y Universidades (grant number RTI2018‐095853‐B‐C21); it was also supported by the Generalitat de Catalunya (2017‐SGR‐1519) and the Universitat de Girona (UdG, contract number MPCUdG2016/059)Akadémiai Kiadó, Springer-Verlag2020info:eu-repo/semantics/articleinfo:eu-repo/semantics/acceptedVersionpeer-reviewed10 p.application/pdfhttp://hdl.handle.net/10256/18688http://hdl.handle.net/10256/18688© Journal of Thermal Analysis and Calorimetry, 2020, vol. 142, p. 2077-2086Articles publicats (D-F)Rasi, Silvia Farjas Silva, Jordi Roura Grabulosa, Pere 2020 Application of thermal analysis and kinetic predictions to YBCO films prepared by chemical solution deposition methods Journal of Thermal Analysis and Calorimetry 142 2077 2086reponame:Recercat. Dipósit de la Recerca de Catalunyainstname:Varias* (Consorci de Biblioteques Universitáries de Catalunya, Centre de Serveis Científics i Acadèmics de Catalunya)Inglésinfo:eu-repo/semantics/altIdentifier/doi/10.1007/s10973-020-10103-4info:eu-repo/semantics/altIdentifier/issn/1388-6150info:eu-repo/semantics/altIdentifier/eissn/1588-2926Tots els drets reservatsinfo:eu-repo/semantics/openAccessoai:recercat.cat:10256/186882026-05-29T05:05:01Z
dc.title.none.fl_str_mv Application of thermal analysis and kinetic predictions to YBCO films prepared by chemical solution deposition methods
title Application of thermal analysis and kinetic predictions to YBCO films prepared by chemical solution deposition methods
spellingShingle Application of thermal analysis and kinetic predictions to YBCO films prepared by chemical solution deposition methods
Rasi, Silvia
Cinètica química
Anàlisi tèrmica
Chemical kinetics
Thermal analysis
title_short Application of thermal analysis and kinetic predictions to YBCO films prepared by chemical solution deposition methods
title_full Application of thermal analysis and kinetic predictions to YBCO films prepared by chemical solution deposition methods
title_fullStr Application of thermal analysis and kinetic predictions to YBCO films prepared by chemical solution deposition methods
title_full_unstemmed Application of thermal analysis and kinetic predictions to YBCO films prepared by chemical solution deposition methods
title_sort Application of thermal analysis and kinetic predictions to YBCO films prepared by chemical solution deposition methods
dc.creator.none.fl_str_mv Rasi, Silvia
Farjas Silva, Jordi
Roura Grabulosa, Pere
author Rasi, Silvia
author_facet Rasi, Silvia
Farjas Silva, Jordi
Roura Grabulosa, Pere
author_role author
author2 Farjas Silva, Jordi
Roura Grabulosa, Pere
author2_role author
author
dc.subject.none.fl_str_mv Cinètica química
Anàlisi tèrmica
Chemical kinetics
Thermal analysis
topic Cinètica química
Anàlisi tèrmica
Chemical kinetics
Thermal analysis
description Fluorine-based chemical solution deposition routes to prepare YBa2Cu3O7-∂ films were characterized with the aid of thermal analysis techniques. Thermogravimetric analysis and X-ray diffraction were applied to characterize the main steps of the fluorine-based route: pyrolysis of the organic material and growth of the oxide. The difference between the thermal behaviour of films and powders in fluorine-based chemical solution deposition route is reiterated to justify the importance of the study of films. Finally, the kinetic analysis is used to predict the mass evolution of the pyrolysis for an arbitrary temperature program with the aim to optimize this treatment to minimize film porosity and crack formation
publishDate 2020
dc.date.none.fl_str_mv 2020
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/acceptedVersion
peer-reviewed
format article
status_str acceptedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/10256/18688
http://hdl.handle.net/10256/18688
url http://hdl.handle.net/10256/18688
dc.language.none.fl_str_mv Inglés
language_invalid_str_mv Inglés
dc.relation.none.fl_str_mv info:eu-repo/semantics/altIdentifier/doi/10.1007/s10973-020-10103-4
info:eu-repo/semantics/altIdentifier/issn/1388-6150
info:eu-repo/semantics/altIdentifier/eissn/1588-2926
dc.rights.none.fl_str_mv Tots els drets reservats
info:eu-repo/semantics/openAccess
rights_invalid_str_mv Tots els drets reservats
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv 10 p.
application/pdf
dc.publisher.none.fl_str_mv Akadémiai Kiadó, Springer-Verlag
publisher.none.fl_str_mv Akadémiai Kiadó, Springer-Verlag
dc.source.none.fl_str_mv © Journal of Thermal Analysis and Calorimetry, 2020, vol. 142, p. 2077-2086
Articles publicats (D-F)
Rasi, Silvia Farjas Silva, Jordi Roura Grabulosa, Pere 2020 Application of thermal analysis and kinetic predictions to YBCO films prepared by chemical solution deposition methods Journal of Thermal Analysis and Calorimetry 142 2077 2086
reponame:Recercat. Dipósit de la Recerca de Catalunya
instname:Varias* (Consorci de Biblioteques Universitáries de Catalunya, Centre de Serveis Científics i Acadèmics de Catalunya)
instname_str Varias* (Consorci de Biblioteques Universitáries de Catalunya, Centre de Serveis Científics i Acadèmics de Catalunya)
reponame_str Recercat. Dipósit de la Recerca de Catalunya
collection Recercat. Dipósit de la Recerca de Catalunya
repository.name.fl_str_mv
repository.mail.fl_str_mv
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score 15,812429

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