Influence of 1 and 5 wt% TiC additions on the oxidation behaviour of pure tungsten

The influence of 1 and 5 wt% of TiC nanoparticles on the oxidation behaviour of reinforced tungsten has been evaluated up to 700 °C in dry air. Isothermal thermogravimetric tests prove that the addition of 5 wt% of TiC particles is detrimental, increasing the mass gain of pure tungsten by a factor o...

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Detalles Bibliográficos
Autores: Pérez Zubiaur, Pablo, Monge, M. Ángeles, Muñoz, A., Adeva, Paloma
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2020
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/226032
Acceso en línea:http://hdl.handle.net/10261/226032
Access Level:acceso abierto
Palabra clave:Tungsten
Composites
Oxidation resistance
Reinforced materials
TiC
Titanium carbide
Descripción
Sumario:The influence of 1 and 5 wt% of TiC nanoparticles on the oxidation behaviour of reinforced tungsten has been evaluated up to 700 °C in dry air. Isothermal thermogravimetric tests prove that the addition of 5 wt% of TiC particles is detrimental, increasing the mass gain of pure tungsten by a factor of ten. TiC particles act as stress concentrators, facilitating microcracking events within the scale and promoting decohesion between TiC-free boundaries and TiC-containing regions of the material. Compared to pure tungsten, lowering TiC addition to 1 wt% significantly improves the oxidation resistance at 700 °C by reducing about seven times the mass gain, while at 600 °C both materials exhibit similar resistance. At 700 °C, the presence of 1 wt% of TiC particles inhibits massive microcracking events occurring in the scale formed on pure tungsten, rendering the oxide scale denser and more protective.