Rapid Modified QuEChERS Method for Pesticides Detection in Honey by High-Performance Liquid Chromatography UV-visible

The extensive use of pesticides in agriculture plays an important role in bees die-off and allows the presence of residues in hive products, particularly in honey. An accurate and reliable analytical method, based on QuEChERS extractive technique, has been developed for the quantitative determinatio...

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Autores: Bonerba, Elisabetta, Ceci, Edmondo, Montemurro, Nicola, Tantillo, Giuseppina, Di Pinto, Angela, Celano, Gaetano Vitale, Bozzo, Giancarlo
Tipo de recurso: artículo
Estado:Versión aceptada para publicación
Fecha de publicación:2014
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/414012
Acceso en línea:http://hdl.handle.net/10261/414012
https://api.elsevier.com/content/abstract/scopus_id/84945557114
Access Level:acceso abierto
Palabra clave:QuEChERS
Analytical method
Honey
HPLC UV-Vis
Pesticides
http://metadata.un.org/sdg/3
http://metadata.un.org/sdg/12
http://metadata.un.org/sdg/9
Ensure healthy lives and promote well-being for all at all ages
Build resilient infrastructure, promote inclusive and sustainable industrialization and foster innovation
Ensure sustainable consumption and production patterns
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repository_id_str
spelling Rapid Modified QuEChERS Method for Pesticides Detection in Honey by High-Performance Liquid Chromatography UV-visibleBonerba, ElisabettaCeci, EdmondoMontemurro, NicolaTantillo, GiuseppinaDi Pinto, AngelaCelano, Gaetano VitaleBozzo, GiancarloQuEChERSAnalytical methodHoneyHPLC UV-VisPesticideshttp://metadata.un.org/sdg/3http://metadata.un.org/sdg/12http://metadata.un.org/sdg/9Ensure healthy lives and promote well-being for all at all agesBuild resilient infrastructure, promote inclusive and sustainable industrialization and foster innovationEnsure sustainable consumption and production patternsThe extensive use of pesticides in agriculture plays an important role in bees die-off and allows the presence of residues in hive products, particularly in honey. An accurate and reliable analytical method, based on QuEChERS extractive technique, has been developed for the quantitative determination by high-performance liquid chromatography UV-visible detector of 5 pesticides (Deltamethrin, Dimethoate, Imidacloprid, Acetamiprid, Chlorfenvinphos) in honey. The method, according to Commission Directive 2002/63/EC and Regulation 882/2004/EC, provided excellent results with respect to linearity (correlation coefficient up to 0.993), limits of detection and quantification (0.005 and 0.01 µg/mL for Dimethoate, Deltamethrin and Chlorfenvinphos; 0.02 and 0.05 µg/mL for Acetamiprid and Imidacloprid), recovery values (86.4 to 96.3%), precision and relative expanded uncertainty of a measurement, demonstrating the conformity of the this method with the European directives. The proposed method was applied to 23 samples of Apulian honey. None of the investigated pesticides was detected in these samples.Peer reviewedPAGEPressConsejo Superior de Investigaciones Científicas [https://ror.org/02gfc7t72]202620262014info:eu-repo/semantics/articlehttp://purl.org/coar/resource_type/c_6501Postprintinfo:eu-repo/semantics/acceptedVersionhttp://hdl.handle.net/10261/414012https://api.elsevier.com/content/abstract/scopus_id/84945557114reponame:DIGITAL.CSIC. Repositorio Institucional del CSICinstname:Consejo Superior de Investigaciones Científicas (CSIC)InglésItalian journal of food safety10.4081/ijfs.2014.1647Síinfo:eu-repo/semantics/openAccessoai:digital.csic.es:10261/4140122026-05-22T06:33:51Z
dc.title.none.fl_str_mv Rapid Modified QuEChERS Method for Pesticides Detection in Honey by High-Performance Liquid Chromatography UV-visible
title Rapid Modified QuEChERS Method for Pesticides Detection in Honey by High-Performance Liquid Chromatography UV-visible
spellingShingle Rapid Modified QuEChERS Method for Pesticides Detection in Honey by High-Performance Liquid Chromatography UV-visible
Bonerba, Elisabetta
QuEChERS
Analytical method
Honey
HPLC UV-Vis
Pesticides
http://metadata.un.org/sdg/3
http://metadata.un.org/sdg/12
http://metadata.un.org/sdg/9
Ensure healthy lives and promote well-being for all at all ages
Build resilient infrastructure, promote inclusive and sustainable industrialization and foster innovation
Ensure sustainable consumption and production patterns
title_short Rapid Modified QuEChERS Method for Pesticides Detection in Honey by High-Performance Liquid Chromatography UV-visible
title_full Rapid Modified QuEChERS Method for Pesticides Detection in Honey by High-Performance Liquid Chromatography UV-visible
title_fullStr Rapid Modified QuEChERS Method for Pesticides Detection in Honey by High-Performance Liquid Chromatography UV-visible
title_full_unstemmed Rapid Modified QuEChERS Method for Pesticides Detection in Honey by High-Performance Liquid Chromatography UV-visible
title_sort Rapid Modified QuEChERS Method for Pesticides Detection in Honey by High-Performance Liquid Chromatography UV-visible
dc.creator.none.fl_str_mv Bonerba, Elisabetta
Ceci, Edmondo
Montemurro, Nicola
Tantillo, Giuseppina
Di Pinto, Angela
Celano, Gaetano Vitale
Bozzo, Giancarlo
author Bonerba, Elisabetta
author_facet Bonerba, Elisabetta
Ceci, Edmondo
Montemurro, Nicola
Tantillo, Giuseppina
Di Pinto, Angela
Celano, Gaetano Vitale
Bozzo, Giancarlo
author_role author
author2 Ceci, Edmondo
Montemurro, Nicola
Tantillo, Giuseppina
Di Pinto, Angela
Celano, Gaetano Vitale
Bozzo, Giancarlo
author2_role author
author
author
author
author
author
dc.contributor.none.fl_str_mv Consejo Superior de Investigaciones Científicas [https://ror.org/02gfc7t72]
dc.subject.none.fl_str_mv QuEChERS
Analytical method
Honey
HPLC UV-Vis
Pesticides
http://metadata.un.org/sdg/3
http://metadata.un.org/sdg/12
http://metadata.un.org/sdg/9
Ensure healthy lives and promote well-being for all at all ages
Build resilient infrastructure, promote inclusive and sustainable industrialization and foster innovation
Ensure sustainable consumption and production patterns
topic QuEChERS
Analytical method
Honey
HPLC UV-Vis
Pesticides
http://metadata.un.org/sdg/3
http://metadata.un.org/sdg/12
http://metadata.un.org/sdg/9
Ensure healthy lives and promote well-being for all at all ages
Build resilient infrastructure, promote inclusive and sustainable industrialization and foster innovation
Ensure sustainable consumption and production patterns
description The extensive use of pesticides in agriculture plays an important role in bees die-off and allows the presence of residues in hive products, particularly in honey. An accurate and reliable analytical method, based on QuEChERS extractive technique, has been developed for the quantitative determination by high-performance liquid chromatography UV-visible detector of 5 pesticides (Deltamethrin, Dimethoate, Imidacloprid, Acetamiprid, Chlorfenvinphos) in honey. The method, according to Commission Directive 2002/63/EC and Regulation 882/2004/EC, provided excellent results with respect to linearity (correlation coefficient up to 0.993), limits of detection and quantification (0.005 and 0.01 µg/mL for Dimethoate, Deltamethrin and Chlorfenvinphos; 0.02 and 0.05 µg/mL for Acetamiprid and Imidacloprid), recovery values (86.4 to 96.3%), precision and relative expanded uncertainty of a measurement, demonstrating the conformity of the this method with the European directives. The proposed method was applied to 23 samples of Apulian honey. None of the investigated pesticides was detected in these samples.
publishDate 2014
dc.date.none.fl_str_mv 2014
2026
2026
dc.type.none.fl_str_mv info:eu-repo/semantics/article
http://purl.org/coar/resource_type/c_6501
Postprint
info:eu-repo/semantics/acceptedVersion
format article
status_str acceptedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/10261/414012
https://api.elsevier.com/content/abstract/scopus_id/84945557114
url http://hdl.handle.net/10261/414012
https://api.elsevier.com/content/abstract/scopus_id/84945557114
dc.language.none.fl_str_mv Inglés
language_invalid_str_mv Inglés
dc.relation.none.fl_str_mv Italian journal of food safety
10.4081/ijfs.2014.1647
Sí
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.publisher.none.fl_str_mv PAGEPress
publisher.none.fl_str_mv PAGEPress
dc.source.none.fl_str_mv reponame:DIGITAL.CSIC. Repositorio Institucional del CSIC
instname:Consejo Superior de Investigaciones Científicas (CSIC)
instname_str Consejo Superior de Investigaciones Científicas (CSIC)
reponame_str DIGITAL.CSIC. Repositorio Institucional del CSIC
collection DIGITAL.CSIC. Repositorio Institucional del CSIC
repository.name.fl_str_mv
repository.mail.fl_str_mv
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score 15.812429

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