Modeling of H-2 Permeation through Electroless Pore-Plated Composite Pd Membranes Using Computational Fluid Dynamics

This work focused on the computational fluid dynamics (CFD) modeling of H-2/N-2 separation in a membrane permeator module containing a supported dense Pd-based membrane that was prepared using electroless pore-plating (ELP-PP). An easy-to-implement model was developed based on a source-sink pair for...

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Detalhes bibliográficos
Autores: Fernández Hoya, Alberto, Casado Merino, Cintia, Alique Amor, David, Calles, J.A., Marugán Aguado, Ángel Javier
Formato: artículo
Fecha de publicación:2021
País:España
Recursos:Universidad Rey Juan Carlos
Repositorio:BURJC-Digital. Repositorio Institucional de la Universidad Rey Juan Carlos
OAI Identifier:oai:burjcdigital.urjc.es:10115/130217
Acesso em linha:https://hdl.handle.net/10115/130217
https://doi.org/10.3390/membranes11020123
Access Level:acceso abierto
Palavra-chave:Chemical engineering (miscellaneous)
Chemistry, physical
Engineering, chemical
Filtration and separation
General materials science
Materials science, multidisciplinary
Polymer science
Process chemistry and technology
Química
Composite membrane
Darcy&amp
#8211
Darcy–forcheimer
Electroless plating
Experimental validation
Forcheimer
Gas separation
Hydrogen
Multiphysics modeling
Palladium
Permeation rate
Sink
Source&amp
Source–sink
Descrição
Resumo:This work focused on the computational fluid dynamics (CFD) modeling of H-2/N-2 separation in a membrane permeator module containing a supported dense Pd-based membrane that was prepared using electroless pore-plating (ELP-PP). An easy-to-implement model was developed based on a source-sink pair formulation of the species transport and continuity equations. The model also included the Darcy-Forcheimer formulation for modeling the porous stainless steel (PSS) membrane support and Sieverts' law for computing the H-2 permeation flow through the dense palladium film. Two different reactor configurations were studied, which involved varying the hydrogen flow permeation direction (in-out or out-in). A wide range of experimental data was simulated by considering the impact of the operating conditions on the H-2 separation, such as the feed pressure and the H-2 concentration in the inlet stream. Simulations of the membrane permeator device showed an excellent agreement between the predicted and experimental data (measured as permeate and retentate flows and H-2 separation). Molar fraction profiles inside the permeator device for both configurations showed that concentration polarization near the membrane surface was not a limit for the hydrogen permeation but could be useful information for membrane reactor design, as it showed the optimal length of the reactor.