High Performance of Superconducting YBa2Cu3O7 Thick Films Prepared by Single-Deposition Inkjet Printing

Inkjet printing (IJP) is a very appealing cost-effective deposition technique to achieve large-area solution-derived functional films. For many applications, it is very challenging to increase the film thickness in order to achieve competitive performance, for instance, high critical currents in sup...

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Autores: Villarejo, Bohores, Pino, Flavio, Pop, Cornelia, Ricart, Susagna, Vallés, Ferran, Mundet, Bernat, Palau, Anna, Roura, Pere, Farjas, Jordi, Chamorro, Natalia, Yáñez, Ramón, Granados, Xavier, Puig Molina, Teresa, Obradors, Xavier
Formato: artículo
Estado:Versión aceptada para publicación
Fecha de publicación:2021
País:España
Recursos:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/250843
Acesso em linha:http://hdl.handle.net/10261/250843
Access Level:acceso abierto
Palavra-chave:Superconductor
YBa2Cu3O7
Thin film
Inkjet printing
Nanocomposite
Critical current
Colloidal ink
Chemical solution deposition
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dc.title.none.fl_str_mv High Performance of Superconducting YBa2Cu3O7 Thick Films Prepared by Single-Deposition Inkjet Printing
title High Performance of Superconducting YBa2Cu3O7 Thick Films Prepared by Single-Deposition Inkjet Printing
spellingShingle High Performance of Superconducting YBa2Cu3O7 Thick Films Prepared by Single-Deposition Inkjet Printing
Villarejo, Bohores
Superconductor
YBa2Cu3O7
Thin film
Inkjet printing
Nanocomposite
Critical current
Colloidal ink
Chemical solution deposition
title_short High Performance of Superconducting YBa2Cu3O7 Thick Films Prepared by Single-Deposition Inkjet Printing
title_full High Performance of Superconducting YBa2Cu3O7 Thick Films Prepared by Single-Deposition Inkjet Printing
title_fullStr High Performance of Superconducting YBa2Cu3O7 Thick Films Prepared by Single-Deposition Inkjet Printing
title_full_unstemmed High Performance of Superconducting YBa2Cu3O7 Thick Films Prepared by Single-Deposition Inkjet Printing
title_sort High Performance of Superconducting YBa2Cu3O7 Thick Films Prepared by Single-Deposition Inkjet Printing
dc.creator.none.fl_str_mv Villarejo, Bohores
Pino, Flavio
Pop, Cornelia
Ricart, Susagna
Vallés, Ferran
Mundet, Bernat
Palau, Anna
Roura, Pere
Farjas, Jordi
Chamorro, Natalia
Yáñez, Ramón
Granados, Xavier
Puig Molina, Teresa
Obradors, Xavier
author Villarejo, Bohores
author_facet Villarejo, Bohores
Pino, Flavio
Pop, Cornelia
Ricart, Susagna
Vallés, Ferran
Mundet, Bernat
Palau, Anna
Roura, Pere
Farjas, Jordi
Chamorro, Natalia
Yáñez, Ramón
Granados, Xavier
Puig Molina, Teresa
Obradors, Xavier
author_role author
author2 Pino, Flavio
Pop, Cornelia
Ricart, Susagna
Vallés, Ferran
Mundet, Bernat
Palau, Anna
Roura, Pere
Farjas, Jordi
Chamorro, Natalia
Yáñez, Ramón
Granados, Xavier
Puig Molina, Teresa
Obradors, Xavier
author2_role author
author
author
author
author
author
author
author
author
author
author
author
author
dc.contributor.none.fl_str_mv European Commission
Ministerio de Economía y Competitividad (España)
European Cooperation in Science and Technology
Generalitat de Catalunya
Consejo Superior de Investigaciones Científicas [https://ror.org/02gfc7t72]
dc.subject.none.fl_str_mv Superconductor
YBa2Cu3O7
Thin film
Inkjet printing
Nanocomposite
Critical current
Colloidal ink
Chemical solution deposition
topic Superconductor
YBa2Cu3O7
Thin film
Inkjet printing
Nanocomposite
Critical current
Colloidal ink
Chemical solution deposition
description Inkjet printing (IJP) is a very appealing cost-effective deposition technique to achieve large-area solution-derived functional films. For many applications, it is very challenging to increase the film thickness in order to achieve competitive performance, for instance, high critical currents in superconducting films. In this paper, the preparation of superconducting YBa2Cu3O7 thick films (∼1.1 μm) using a single deposition is reported. Specific rules for ink design, deposition protocols, and pyrolysis processes are provided. The most important aspect is to formulate an ink with a solvent having a high boiling point that keeps the whole film wet during deposition to avoid liquid movement due to coffee-ring effects. An additional success has been to modify the ink with a photocurable polyacrylic ester varnish which after polymerization with a UV LED lamp helps keep homogeneous thickness. This varnish also helped avoid the generation of film instabilities (wrinkling or cracking) during pyrolysis. Homogeneous pyrolyzed thick films are transformed into epitaxial thick films with high critical currents. The IJP process is shown to be valid to prepare nanocomposite films using colloidal inks including pre-prepared BaZrO3 nanoparticles. The nanocomposite thick films display enhanced vortex pinning, thus keeping high critical currents under high magnetic fields.
publishDate 2021
dc.date.none.fl_str_mv 2021
2021
2021
dc.type.none.fl_str_mv info:eu-repo/semantics/article
http://purl.org/coar/resource_type/c_6501
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info:eu-repo/semantics/acceptedVersion
format article
status_str acceptedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/10261/250843
url http://hdl.handle.net/10261/250843
dc.language.none.fl_str_mv Inglés
language_invalid_str_mv Inglés
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info:eu-repo/grantAgreement/EC/FP7/280432
info:eu-repo/grantAgreement/MINECO/Plan Estatal de Investigación Científica y Técnica y de Innovación 2013-2016/MAT2014- 51778-C2-1-R
info:eu-repo/grantAgreement/MINECO/Plan Estatal de Investigación Científica y Técnica y de Innovación 2013-2016/MAT2014-51778-C2-2-R
info:eu-repo/grantAgreement/AEI/Plan Estatal de Investigación Científica y Técnica y de Innovación 2017-2020/RTI2018-095853-BC21
info:eu-repo/grantAgreement/AEI/Plan Estatal de Investigación Científica y Técnica y de Innovación 2017-2020/RTI2018-095853-B-C22
info:eu-repo/grantAgreement/MINECO/Plan Estatal de Investigación Científica y Técnica y de Innovación 2013-2016/RTC-2015-3840-S
info:eu-repo/grantAgreement/AEI/Plan Estatal de Investigación Científica y Técnica y de Innovación 2017-2020/CEX2019-000917-S
http://dx.doi.org/10.1021/acsaelm.1c00513

dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.publisher.none.fl_str_mv American Chemical Society
publisher.none.fl_str_mv American Chemical Society
dc.source.none.fl_str_mv reponame:DIGITAL.CSIC. Repositorio Institucional del CSIC
instname:Consejo Superior de Investigaciones Científicas (CSIC)
instname_str Consejo Superior de Investigaciones Científicas (CSIC)
reponame_str DIGITAL.CSIC. Repositorio Institucional del CSIC
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spelling High Performance of Superconducting YBa2Cu3O7 Thick Films Prepared by Single-Deposition Inkjet PrintingVillarejo, BohoresPino, FlavioPop, CorneliaRicart, SusagnaVallés, FerranMundet, BernatPalau, AnnaRoura, PereFarjas, JordiChamorro, NataliaYáñez, RamónGranados, XavierPuig Molina, TeresaObradors, XavierSuperconductorYBa2Cu3O7Thin filmInkjet printingNanocompositeCritical currentColloidal inkChemical solution depositionInkjet printing (IJP) is a very appealing cost-effective deposition technique to achieve large-area solution-derived functional films. For many applications, it is very challenging to increase the film thickness in order to achieve competitive performance, for instance, high critical currents in superconducting films. In this paper, the preparation of superconducting YBa2Cu3O7 thick films (∼1.1 μm) using a single deposition is reported. Specific rules for ink design, deposition protocols, and pyrolysis processes are provided. The most important aspect is to formulate an ink with a solvent having a high boiling point that keeps the whole film wet during deposition to avoid liquid movement due to coffee-ring effects. An additional success has been to modify the ink with a photocurable polyacrylic ester varnish which after polymerization with a UV LED lamp helps keep homogeneous thickness. This varnish also helped avoid the generation of film instabilities (wrinkling or cracking) during pyrolysis. Homogeneous pyrolyzed thick films are transformed into epitaxial thick films with high critical currents. The IJP process is shown to be valid to prepare nanocomposite films using colloidal inks including pre-prepared BaZrO3 nanoparticles. The nanocomposite thick films display enhanced vortex pinning, thus keeping high critical currents under high magnetic fields.The authors acknowledge the EUROTAPES project (EU-FP7 NMP-LA-2012-280432), COACHSUPENERGY (MAT2014- 51778-C2-1-R and MAT2014-51778-C2-2-R), SUMATE (RTI2018-095853-BC21 and RTI2018-095853-B-C22) cofinanced by the European Regional Development Fund and SUPERINKS (RTC-2015-3840-S) from MINECO (cofinanced by the European Regional Development Fund), 2017-SGR 753 from Generalitat de Catalunya, and COST Action NANOCOHYBRI (CA16218). ICMAB authors acknowledge the Center of Excellence awards Severo Ochoa SEV2015-0496 and CEX2019-000917-S. The authors acknowledge the Scientific Services at ICMAB, ICN2 Electron Microscopy Division, and LMA-INA from Aragon. They also acknowledge KAO Chimigraf for providing varnishes and Bruker HTS for providing metallic substrates.Peer reviewedAmerican Chemical SocietyEuropean CommissionMinisterio de Economía y Competitividad (España)European Cooperation in Science and TechnologyGeneralitat de CatalunyaConsejo Superior de Investigaciones Científicas [https://ror.org/02gfc7t72]202120212021info:eu-repo/semantics/articlehttp://purl.org/coar/resource_type/c_6501Postprintinfo:eu-repo/semantics/acceptedVersionhttp://hdl.handle.net/10261/250843reponame:DIGITAL.CSIC. Repositorio Institucional del CSICinstname:Consejo Superior de Investigaciones Científicas (CSIC)Inglés#PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE#info:eu-repo/grantAgreement/EC/FP7/280432info:eu-repo/grantAgreement/MINECO/Plan Estatal de Investigación Científica y Técnica y de Innovación 2013-2016/MAT2014- 51778-C2-1-Rinfo:eu-repo/grantAgreement/MINECO/Plan Estatal de Investigación Científica y Técnica y de Innovación 2013-2016/MAT2014-51778-C2-2-Rinfo:eu-repo/grantAgreement/AEI/Plan Estatal de Investigación Científica y Técnica y de Innovación 2017-2020/RTI2018-095853-BC21info:eu-repo/grantAgreement/AEI/Plan Estatal de Investigación Científica y Técnica y de Innovación 2017-2020/RTI2018-095853-B-C22info:eu-repo/grantAgreement/MINECO/Plan Estatal de Investigación Científica y Técnica y de Innovación 2013-2016/RTC-2015-3840-Sinfo:eu-repo/grantAgreement/AEI/Plan Estatal de Investigación Científica y Técnica y de Innovación 2017-2020/CEX2019-000917-Shttp://dx.doi.org/10.1021/acsaelm.1c00513Síinfo:eu-repo/semantics/openAccessoai:digital.csic.es:10261/2508432026-05-22T06:33:51Z
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