Production of biodegradable PLGA foams processed with high pressure CO2

Microcellular scaffolds were prepared using high pressure fluids. Solutions of biodegradable material Poly (lactic-co-glycolic) acid (PLGA) in a green solvent such as ethyl lactate was used as the scaffold matrix. To carry out polymer foaming from polymer solutions allows the possibility of reducing...

Descripción completa

Detalles Bibliográficos
Autores: Álvarez, I., Gutiérrez, Cristina, Rodríguez Romero, Juan Francisco, Lucas Martínez, Antonio de, García González, María Teresa
Tipo de recurso: artículo
Fecha de publicación:2020
País:España
Institución:Universidad de Castilla-La Mancha
Repositorio:RUIdeRA. Repositorio Institucional de la UCLM
OAI Identifier:oai:ruidera.uclm.es:10578/29926
Acceso en línea:http://hdl.handle.net/10578/29926
Access Level:acceso abierto
Palabra clave:PLGA
Supercritical CO2 foaming
Ethyl lactate
Tg depression
Espuma de CO2 supercrítico
Lactato de etilo
Tg depresión
Descripción
Sumario:Microcellular scaffolds were prepared using high pressure fluids. Solutions of biodegradable material Poly (lactic-co-glycolic) acid (PLGA) in a green solvent such as ethyl lactate was used as the scaffold matrix. To carry out polymer foaming from polymer solutions allows the possibility of reducing the working temperature. The effect of the ratio lactide to glycolide of the polymer, the working pressure, the initial concentration of the polymer in the solvent and the depressurization time were the variables studied at a temperature of 25 °C. The morphology of the foams obtained was characterized based on the cell diameter and its standard deviation, indicator of the homogeneity of the scaffolds obtained, as well as the density of cells. In addition, a study was performed on how the glass transition temperature (Tg) of a polymer is modified by the plasticizing effect of CO2 pressure.