Improving trade-offs in the figures of merit of gas-phase single-pass continuous CO2 electrocatalytic reduction to formate

The electrochemical conversion of CO2 is gaining increasing attention because it could be considered as an appealing strategy for making value-added products at mild conditions from CO2 captured. In this work, we report a process for the electrocatalytic reduction of CO2 to formate (HCOO-) operating...

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Detalles Bibliográficos
Autores: Díaz Sainz, Guillermo, Álvarez Guerra, Manuel|||0000-0002-3546-584X, Ávila Bolívar, Beatriz, Solla Gullón, José, Montiel Leguey, Vicente, Irabien Gulías, Ángel|||0000-0002-2411-4163
Tipo de recurso: artículo
Fecha de publicación:2021
País:España
Institución:Universidad de Cantabria (UC)
Repositorio:UCrea Repositorio Abierto de la Universidad de Cantabria
Idioma:inglés
OAI Identifier:oai:repositorio.unican.es:10902/19249
Acceso en línea:http://hdl.handle.net/10902/19249
Access Level:acceso abierto
Palabra clave:CO2 electroreduction
Formate
Bismuth electrocatalysts
Gas Diffusion Electrode (GDE)
Membrane electrode assembly (MEA)
Electrochemical filter press reactor
Descripción
Sumario:The electrochemical conversion of CO2 is gaining increasing attention because it could be considered as an appealing strategy for making value-added products at mild conditions from CO2 captured. In this work, we report a process for the electrocatalytic reduction of CO2 to formate (HCOO-) operating in a continuous way, employing a single pass of the reactants through the electrochemical reactor and using Bi carbon supported nanoparticles in the form of a membrane electrode assembly composed by a Gas Diffusion Electrode, a current collector and a cationic exchange membrane. This contribution presents the best trade-off between HCOO- concentration, Faradaic Efficiency and energy consumption in the literature. We also show noteworthy values of energy consumption required of only 180 kWh·kmol-1 of HCOO-, lower than previous approaches, working at current densities that allow achieving formate concentration higher than 300 g·L-1 and simultaneously, a Faradaic Efficiency close to 90%. The results here displayed make the electrochemical approach closer for future implementation at the industrial scale.