Effect of Fe substitution for Cu on microstructure and magnetic properties of laser floating zone (LFZ) grown Bi-2212 rods
In this paper, the laser floating zone (LFZ) technique has been used to fabricate Bi2Sr2Ca1Cu2-x Fe x O (x=0,0.01,0.03,0.05,0.1) superconducting fibers. The effects of Fe substitution on grain alignment and superconducting properties of annealed fibers were studied using SEM/EDX microanalysis in add...
| Autores: | , , , |
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| Tipo de recurso: | artículo |
| Estado: | Versión enviada para evaluación y publicación |
| Fecha de publicación: | 2013 |
| País: | España |
| Institución: | Consejo Superior de Investigaciones Científicas (CSIC) |
| Repositorio: | DIGITAL.CSIC. Repositorio Institucional del CSIC |
| OAI Identifier: | oai:dnet:digitalcsic_::eb748db40bbb66a08f88cac81bd30d07 |
| Acceso en línea: | http://hdl.handle.net/10261/117552 |
| Access Level: | acceso abierto |
| Palabra clave: | Fe substitution Bi-2212 Texture Melt processing LFZ |
| Sumario: | In this paper, the laser floating zone (LFZ) technique has been used to fabricate Bi2Sr2Ca1Cu2-x Fe x O (x=0,0.01,0.03,0.05,0.1) superconducting fibers. The effects of Fe substitution on grain alignment and superconducting properties of annealed fibers were studied using SEM/EDX microanalysis in addition to phase analysis and magnetic measurements realized through XRD, M-T, and M-H loops. In the same growth conditions, higher Fe contents lead to a more compact microstructure with lower porosity but also caused the formation of poor superconducting phases followed by the decrease of T c and J cmag. No evidence of enhanced pinning capability was found in the magnetic measurements. Annealed rods indicated a weakly ferromagnetic-like behavior at relatively high doping levels. |
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