Room temperature synthesis and characterization of novel lead-free double perovskite nanocrystals with a stable and broadband emission

Low-dimensional and lead-free halide perovskites are of great interest for their wide application potential for optoelectronic applications. We report on the successful synthesis of novel lead-free colloidal Cs3BiBr6 nanocrystals (NCs) with an ultra-small size of ∼1.5-3 nm by a room temperature anti...

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Autores: Tang, Yingying, Gomez, Leyre|||0000-0002-2926-5665, Van Der Laan, Marco, Timmerman, Dolf, Sebastian, Víctor|||0000-0002-6873-5244, Huang, Chia-Ching, Gregorkiewicz, Tom|||0000-0003-2092-8378, Schall, Peter
Tipo de recurso: artículo
Fecha de publicación:2021
País:España
Institución:Universitat Autònoma de Barcelona
Repositorio:Dipòsit Digital de Documents de la UAB
Idioma:inglés
OAI Identifier:oai:ddd.uab.cat:237732
Acceso en línea:https://ddd.uab.cat/record/237732
https://dx.doi.org/urn:doi:10.1039/d0tc04394j
Access Level:acceso abierto
Palabra clave:Antisolvent process
Crystallographic characterization
Double perovskites
Halide perovskites
Low temperature photoluminescence
Optoelectronic applications
Room temperature synthesis
Stable blue emission
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spelling Room temperature synthesis and characterization of novel lead-free double perovskite nanocrystals with a stable and broadband emissionTang, YingyingGomez, Leyre|||0000-0002-2926-5665Van Der Laan, MarcoTimmerman, DolfSebastian, Víctor|||0000-0002-6873-5244Huang, Chia-ChingGregorkiewicz, Tom|||0000-0003-2092-8378Schall, PeterAntisolvent processCrystallographic characterizationDouble perovskitesHalide perovskitesLow temperature photoluminescenceOptoelectronic applicationsRoom temperature synthesisStable blue emissionLow-dimensional and lead-free halide perovskites are of great interest for their wide application potential for optoelectronic applications. We report on the successful synthesis of novel lead-free colloidal Cs3BiBr6 nanocrystals (NCs) with an ultra-small size of ∼1.5-3 nm by a room temperature antisolvent process. From crystallographic characterization we show that it is critical to precisely control the ratio of precursors to obtain the pure 3-1-6 phase. The synthesis process is facile and repeatable and results in Cs3BiBr6 NCs that display stable blue emission around 438 nm with a relatively broad linewidth of 92.1 nm. Low-temperature photoluminescence (PL) measurements displayed a red-shift of bandgap with decreasing temperature, which might be attributed to the thermal expansion of the lattice. In addition, the NCs demonstrate high stability at ambient conditions. 22021-01-0120212021-01-01Articlehttp://purl.org/coar/resource_type/c_6501VoRhttp://purl.org/coar/version/c_970fb48d4fbd8a85info:eu-repo/semantics/articleapplication/pdfhttps://ddd.uab.cat/record/237732https://dx.doi.org/urn:doi:10.1039/d0tc04394jreponame:Dipòsit Digital de Documents de la UABinstname:Universitat Autònoma de BarcelonaInglésengopen accesshttp://purl.org/coar/access_right/c_abf2Aquest document està subjecte a una llicència d'ús Creative Commons. Es permet la reproducció total o parcial, la distribució, la comunicació pública de l'obra i la creació d'obres derivades, sempre que no sigui amb finalitats comercials, i sempre que es reconegui l'autoria de l'obra original.https://creativecommons.org/licenses/by-nc/4.0/info:eu-repo/semantics/openAccessoai:ddd.uab.cat:2377322026-06-06T12:50:31Z
dc.title.none.fl_str_mv Room temperature synthesis and characterization of novel lead-free double perovskite nanocrystals with a stable and broadband emission
title Room temperature synthesis and characterization of novel lead-free double perovskite nanocrystals with a stable and broadband emission
spellingShingle Room temperature synthesis and characterization of novel lead-free double perovskite nanocrystals with a stable and broadband emission
Tang, Yingying
Antisolvent process
Crystallographic characterization
Double perovskites
Halide perovskites
Low temperature photoluminescence
Optoelectronic applications
Room temperature synthesis
Stable blue emission
title_short Room temperature synthesis and characterization of novel lead-free double perovskite nanocrystals with a stable and broadband emission
title_full Room temperature synthesis and characterization of novel lead-free double perovskite nanocrystals with a stable and broadband emission
title_fullStr Room temperature synthesis and characterization of novel lead-free double perovskite nanocrystals with a stable and broadband emission
title_full_unstemmed Room temperature synthesis and characterization of novel lead-free double perovskite nanocrystals with a stable and broadband emission
title_sort Room temperature synthesis and characterization of novel lead-free double perovskite nanocrystals with a stable and broadband emission
dc.creator.none.fl_str_mv Tang, Yingying
Gomez, Leyre|||0000-0002-2926-5665
Van Der Laan, Marco
Timmerman, Dolf
Sebastian, Víctor|||0000-0002-6873-5244
Huang, Chia-Ching
Gregorkiewicz, Tom|||0000-0003-2092-8378
Schall, Peter
author Tang, Yingying
author_facet Tang, Yingying
Gomez, Leyre|||0000-0002-2926-5665
Van Der Laan, Marco
Timmerman, Dolf
Sebastian, Víctor|||0000-0002-6873-5244
Huang, Chia-Ching
Gregorkiewicz, Tom|||0000-0003-2092-8378
Schall, Peter
author_role author
author2 Gomez, Leyre|||0000-0002-2926-5665
Van Der Laan, Marco
Timmerman, Dolf
Sebastian, Víctor|||0000-0002-6873-5244
Huang, Chia-Ching
Gregorkiewicz, Tom|||0000-0003-2092-8378
Schall, Peter
author2_role author
author
author
author
author
author
author
dc.subject.none.fl_str_mv Antisolvent process
Crystallographic characterization
Double perovskites
Halide perovskites
Low temperature photoluminescence
Optoelectronic applications
Room temperature synthesis
Stable blue emission
topic Antisolvent process
Crystallographic characterization
Double perovskites
Halide perovskites
Low temperature photoluminescence
Optoelectronic applications
Room temperature synthesis
Stable blue emission
description Low-dimensional and lead-free halide perovskites are of great interest for their wide application potential for optoelectronic applications. We report on the successful synthesis of novel lead-free colloidal Cs3BiBr6 nanocrystals (NCs) with an ultra-small size of ∼1.5-3 nm by a room temperature antisolvent process. From crystallographic characterization we show that it is critical to precisely control the ratio of precursors to obtain the pure 3-1-6 phase. The synthesis process is facile and repeatable and results in Cs3BiBr6 NCs that display stable blue emission around 438 nm with a relatively broad linewidth of 92.1 nm. Low-temperature photoluminescence (PL) measurements displayed a red-shift of bandgap with decreasing temperature, which might be attributed to the thermal expansion of the lattice. In addition, the NCs demonstrate high stability at ambient conditions.
publishDate 2021
dc.date.none.fl_str_mv 2
2021-01-01
2021
2021-01-01
dc.type.none.fl_str_mv Article
http://purl.org/coar/resource_type/c_6501
VoR
http://purl.org/coar/version/c_970fb48d4fbd8a85
dc.type.openaire.fl_str_mv info:eu-repo/semantics/article
format article
dc.identifier.none.fl_str_mv https://ddd.uab.cat/record/237732
https://dx.doi.org/urn:doi:10.1039/d0tc04394j
url https://ddd.uab.cat/record/237732
https://dx.doi.org/urn:doi:10.1039/d0tc04394j
dc.language.none.fl_str_mv Inglés
eng
language_invalid_str_mv Inglés
language eng
dc.rights.none.fl_str_mv open access
http://purl.org/coar/access_right/c_abf2
https://creativecommons.org/licenses/by-nc/4.0/
dc.rights.openaire.fl_str_mv info:eu-repo/semantics/openAccess
rights_invalid_str_mv open access
http://purl.org/coar/access_right/c_abf2
https://creativecommons.org/licenses/by-nc/4.0/
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.source.none.fl_str_mv reponame:Dipòsit Digital de Documents de la UAB
instname:Universitat Autònoma de Barcelona
instname_str Universitat Autònoma de Barcelona
reponame_str Dipòsit Digital de Documents de la UAB
collection Dipòsit Digital de Documents de la UAB
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repository.mail.fl_str_mv
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