Controlled oxygen doping in highly dispersed Ni-loaded g-C3N4 nanotubes for efficient photocatalytic H2O2 production

Hydrogen peroxide (HO) is both a key component in several industrial processes and a promising liquid fuel. The production of HO by solar photocatalysis is a suitable strategy to convert and store solar energy into chemical energy. Here we report an oxygen-doped tubular g-CN with uniformly dispersed...

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Detalles Bibliográficos
Autores: Du, Ruifeng, Xiao, Ke, Li, Baoying, Han, Xu, Zhang, Chaoqi, Wang, Xiang, Zuo, Yong, Guardia, Pablo, Li, Junshan, Chen, Jianbin, Arbiol, Jordi, Cabot, Andreu
Tipo de recurso: artículo
Estado:Versión aceptada para publicación
Fecha de publicación:2022
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/280524
Acceso en línea:http://hdl.handle.net/10261/280524
Access Level:acceso abierto
Palabra clave:Carbon nitrides
Nanotubes
Nickel nanoparticles
Photocatalysis
H2O2
Descripción
Sumario:Hydrogen peroxide (HO) is both a key component in several industrial processes and a promising liquid fuel. The production of HO by solar photocatalysis is a suitable strategy to convert and store solar energy into chemical energy. Here we report an oxygen-doped tubular g-CN with uniformly dispersed nickel nanoparticles for efficient photocatalytic HO generation. The hollow structure of the tubular g-CN provides a large surface with a high density of reactive sites and efficient visible light absorption during the photocatalytic reaction. The oxygen doping and Ni loading enable a fast separation of photogenerated charge carriers and a high selectivity toward the two-electron process during the oxygen reduction reaction (ORR). The optimized composition, Ni/OtCN, displays an HO production rate of 2464 μmol g·h, which is eightfold higher than that of bulk g-CN under visible light irradiation (λ > 420 nm), and achieves an apparent quantum yield (AQY) of 28.2% at 380 nm and 14.9% at 420 nm.