Residues of b-lactams and quinolones in tissues and milk samples. Confirmatory analysis by liquid chromatography-mass spectrometry

The aim of this work is to optimize and validate methods for the multiresidue determination of series of families of antibiotics as quinolones, penicillins and cephalosporins included in European regulation in food samples using LC-MS/MS. Different extraction techniques and clean-up applied to antib...

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Detalhes bibliográficos
Autores: Junza Martínez, Alexandra, Amatya, Rameshwari, Pérez-Burgos, Rafael, Gokce, Gultekin, Grzelak, Edyta, Barrón Bueno, Dolores, Barbosa Torralbo, José
Formato: artículo
Estado:Versión publicada
Fecha de publicación:2010
País:España
Recursos:Varias* (Consorci de Biblioteques Universitáries de Catalunya, Centre de Serveis Científics i Acadèmics de Catalunya)
Repositorio:Recercat. Dipósit de la Recerca de Catalunya
OAI Identifier:oai:recercat.cat:2445/44669
Acesso em linha:https://hdl.handle.net/2445/44669
Access Level:acceso abierto
Palavra-chave:Quinolones
Penicil·lina
Teixits (Histologia)
Llet
Cefalosporines
Quinolone antibacterial agents
Penicillin
Tissues
Milk
Cephalosporines
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spelling Residues of b-lactams and quinolones in tissues and milk samples. Confirmatory analysis by liquid chromatography-mass spectrometryJunza Martínez, AlexandraAmatya, RameshwariPérez-Burgos, RafaelGokce, GultekinGrzelak, EdytaBarrón Bueno, DoloresBarbosa Torralbo, JoséQuinolonesPenicil·linaTeixits (Histologia)LletCefalosporinesQuinolone antibacterial agentsPenicillinTissuesMilkCephalosporinesThe aim of this work is to optimize and validate methods for the multiresidue determination of series of families of antibiotics as quinolones, penicillins and cephalosporins included in European regulation in food samples using LC-MS/MS. Different extraction techniques and clean-up applied to antibiotics in meat were compared. The quality parameters were established according with EU guideline. The developed method was applied to 49 positive raw milk samples from animal medicated with different antibiotics; the 63% of the analyzed samples were found to be compliant. ___________________________________________________________________________________________Universitatea Ovidius2013201320102013info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersion14 p.application/pdfhttps://hdl.handle.net/2445/44669Articles publicats en revistes (Enginyeria Química i Química Analítica)reponame:Recercat. Dipósit de la Recerca de Catalunyainstname:Varias* (Consorci de Biblioteques Universitáries de Catalunya, Centre de Serveis Científics i Acadèmics de Catalunya)InglésOvidius University Annals of Chemistry, 2010, vol. 21, num. 2, p. 109-122(c) Universitatea Ovidius, 2010info:eu-repo/semantics/openAccessoai:recercat.cat:2445/446692026-05-29T05:05:01Z
dc.title.none.fl_str_mv Residues of b-lactams and quinolones in tissues and milk samples. Confirmatory analysis by liquid chromatography-mass spectrometry
title Residues of b-lactams and quinolones in tissues and milk samples. Confirmatory analysis by liquid chromatography-mass spectrometry
spellingShingle Residues of b-lactams and quinolones in tissues and milk samples. Confirmatory analysis by liquid chromatography-mass spectrometry
Junza Martínez, Alexandra
Quinolones
Penicil·lina
Teixits (Histologia)
Llet
Cefalosporines
Quinolone antibacterial agents
Penicillin
Tissues
Milk
Cephalosporines
title_short Residues of b-lactams and quinolones in tissues and milk samples. Confirmatory analysis by liquid chromatography-mass spectrometry
title_full Residues of b-lactams and quinolones in tissues and milk samples. Confirmatory analysis by liquid chromatography-mass spectrometry
title_fullStr Residues of b-lactams and quinolones in tissues and milk samples. Confirmatory analysis by liquid chromatography-mass spectrometry
title_full_unstemmed Residues of b-lactams and quinolones in tissues and milk samples. Confirmatory analysis by liquid chromatography-mass spectrometry
title_sort Residues of b-lactams and quinolones in tissues and milk samples. Confirmatory analysis by liquid chromatography-mass spectrometry
dc.creator.none.fl_str_mv Junza Martínez, Alexandra
Amatya, Rameshwari
Pérez-Burgos, Rafael
Gokce, Gultekin
Grzelak, Edyta
Barrón Bueno, Dolores
Barbosa Torralbo, José
author Junza Martínez, Alexandra
author_facet Junza Martínez, Alexandra
Amatya, Rameshwari
Pérez-Burgos, Rafael
Gokce, Gultekin
Grzelak, Edyta
Barrón Bueno, Dolores
Barbosa Torralbo, José
author_role author
author2 Amatya, Rameshwari
Pérez-Burgos, Rafael
Gokce, Gultekin
Grzelak, Edyta
Barrón Bueno, Dolores
Barbosa Torralbo, José
author2_role author
author
author
author
author
author
dc.subject.none.fl_str_mv Quinolones
Penicil·lina
Teixits (Histologia)
Llet
Cefalosporines
Quinolone antibacterial agents
Penicillin
Tissues
Milk
Cephalosporines
topic Quinolones
Penicil·lina
Teixits (Histologia)
Llet
Cefalosporines
Quinolone antibacterial agents
Penicillin
Tissues
Milk
Cephalosporines
description The aim of this work is to optimize and validate methods for the multiresidue determination of series of families of antibiotics as quinolones, penicillins and cephalosporins included in European regulation in food samples using LC-MS/MS. Different extraction techniques and clean-up applied to antibiotics in meat were compared. The quality parameters were established according with EU guideline. The developed method was applied to 49 positive raw milk samples from animal medicated with different antibiotics; the 63% of the analyzed samples were found to be compliant. ___________________________________________________________________________________________
publishDate 2010
dc.date.none.fl_str_mv 2010
2013
2013
2013
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv https://hdl.handle.net/2445/44669
url https://hdl.handle.net/2445/44669
dc.language.none.fl_str_mv Inglés
language_invalid_str_mv Inglés
dc.relation.none.fl_str_mv Ovidius University Annals of Chemistry, 2010, vol. 21, num. 2, p. 109-122
dc.rights.none.fl_str_mv (c) Universitatea Ovidius, 2010
info:eu-repo/semantics/openAccess
rights_invalid_str_mv (c) Universitatea Ovidius, 2010
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv 14 p.
application/pdf
dc.publisher.none.fl_str_mv Universitatea Ovidius
publisher.none.fl_str_mv Universitatea Ovidius
dc.source.none.fl_str_mv Articles publicats en revistes (Enginyeria Química i Química Analítica)
reponame:Recercat. Dipósit de la Recerca de Catalunya
instname:Varias* (Consorci de Biblioteques Universitáries de Catalunya, Centre de Serveis Científics i Acadèmics de Catalunya)
instname_str Varias* (Consorci de Biblioteques Universitáries de Catalunya, Centre de Serveis Científics i Acadèmics de Catalunya)
reponame_str Recercat. Dipósit de la Recerca de Catalunya
collection Recercat. Dipósit de la Recerca de Catalunya
repository.name.fl_str_mv
repository.mail.fl_str_mv
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score 15,198674

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