Stereoselective synthesis on fullerenes: properties and photoelectrochemical applications

After the discovery of fullerenes, carbon nanotubes and graphene, the classical allotropes of carbon were enriched with new structures and new potential applications. C60, with its singular spherical shape, its size (~1nm) and its remarkable electronic and photophysical properties, has emerged as a...

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Detalles Bibliográficos
Autor: Girón Rubio, Rosa María
Tipo de recurso: tesis doctoral
Fecha de publicación:2019
País:España
Institución:Universidad Complutense de Madrid (UCM)
Repositorio:Docta Complutense
Idioma:inglés
OAI Identifier:oai:docta.ucm.es:20.500.14352/17334
Acceso en línea:https://hdl.handle.net/20.500.14352/17334
Access Level:acceso abierto
Palabra clave:547.1(043.2)
Fullerenos
Fullerenes
Química orgánica (Química)
2306 Química Orgánica
Descripción
Sumario:After the discovery of fullerenes, carbon nanotubes and graphene, the classical allotropes of carbon were enriched with new structures and new potential applications. C60, with its singular spherical shape, its size (~1nm) and its remarkable electronic and photophysical properties, has emerged as a promising material for many potential applications in materials, nanotechnology and biomedical sciences. Objectives 1. Synthesis and electronic properties of fullerenes-fused unsaturated carbocyclesWe will extend the scope of asymmetric phosphine-catalysed cycloaddition of allenoates onto fullerenes through the variation of all the elements involved in the reaction. In addition, the intrinsic electronic mobility of these fullerenic derivatives will be measured with the objective of evaluating the influence of the optical purity on this property. 2. Reversible stereodivergent cycloaddition of a helicene derivative onto [60]fullerene: a chiral resolution strategyWe will try to take advantage of the stereoselective and reversible covalent fullerene chemistry as a tool for the resolution of racemates. For this purpose, enantioselective pyrrolidino[60]fullerenes will be prepared from a racemic iminoester derived from [6]helicene...