Scaffold electrodes based on thioctic acid-capped gold nanoparticles coordinated Alcohol Dehydrogenase and Azure A films for high performance biosensor

Nanometric size gold nanoparticles capped with thiotic acid are used to coordinate with the Zn (II) present in the catalytic center of Alcohol Dehydrogenase (ADH). In combination with the NADH oxidation molecular catalyst Azure A, electrografted onto carbon screen-printed electrodes, they are used a...

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Detalhes bibliográficos
Autores: Gómez-Anquela, C., García-Mendiola, Tania, Abad, José M., Pita, Marcos, Pariente, Félix, Lorenzo, Encarnación
Formato: artículo
Estado:Versión aceptada para publicación
Fecha de publicación:2015
País:España
Recursos:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/163637
Acesso em linha:http://hdl.handle.net/10261/163637
Access Level:acceso abierto
Palavra-chave:Alcohol dehydrogenases
Biosensors
Gold nanoparticles
Electrografting
Descrição
Resumo:Nanometric size gold nanoparticles capped with thiotic acid are used to coordinate with the Zn (II) present in the catalytic center of Alcohol Dehydrogenase (ADH). In combination with the NADH oxidation molecular catalyst Azure A, electrografted onto carbon screen-printed electrodes, they are used as scaffold electrodes for the construction of a very efficient ethanol biosensor. The final biosensing device exhibits a highly efficient ethanol oxidation with low overpotential of − 0.25 V besides a very good analytical performance with a detection limit of 0.14 ± 0.01 μM and a stable response for more than one month.