NMR study of manganese(II) binding by a new versatile peroxidase from the white-rot fungus Pleurotus eryngii

Nuclear magnetic resonance spectroscopy has been used to characterize the versatile peroxidase from Pleurotus eryngii, both in the resting state and in the cyanide-inhibited form. The assignment of most of the hyperfine-shifted resonances has been achieved by two-dimensional NMR, allowing the compar...

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Detalles Bibliográficos
Autores: Banci, Lucia, Camarero, Susana, Martínez, Ángel T., Martínez, María Jesús, Pérez-Boada, Marta, Pierattelli, Roberta, Ruiz-Dueñas, F. J.
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2003
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:dnet:digitalcsic_::57b36302a1e29427550df373dc84f3b2
Acceso en línea:http://hdl.handle.net/10261/429071
https://api.elsevier.com/content/abstract/scopus_id/0141790930
Access Level:acceso abierto
Palabra clave:Heme protein
Lignin biodegradation
Manganese-oxidizing enzyme
Site-directed mutagenesis
Substrate interaction
Descripción
Sumario:Nuclear magnetic resonance spectroscopy has been used to characterize the versatile peroxidase from Pleurotus eryngii, both in the resting state and in the cyanide-inhibited form. The assignment of most of the hyperfine-shifted resonances has been achieved by two-dimensional NMR, allowing the comparison of the present system with other ligninolytic peroxidases. This information has enabled a detailed analysis of the interaction of the enzyme with one of its reducing substrates, Mn(II). Furthermore, comparison with the data collected on a mutant in the putative Mn(II) binding site, and an analysis of the enzyme kinetic properties, shed light on the factors affecting the function of this novel peroxidase.