Facile synthesis of nanoparticles of the molecule-based superconductor κ-(BEDT-TTF)2Cu(NCS)2

[EN]: Well-dispersed roughly spherical nano-objects of the molecule-based superconductor κ-(BEDT-TTF)2Cu(NCS)2 have been prepared in an organic solution by using an easy synthetic route. Long alkyl-chain aconitate esters have been used as growth controlling agents. Nano-objects exhibiting sizes in t...

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Detalhes bibliográficos
Autores: Cormary, Benoît, Faulmann, Christophe, Caro, Dominique de, Valade, Lydie, Caro, Pascale de, Ballesteros, Belén, Fraxedas, J.
Formato: artículo
Estado:Versión publicada
Fecha de publicación:2018
País:España
Recursos:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/199194
Acesso em linha:http://hdl.handle.net/10261/199194
Access Level:acceso abierto
Palavra-chave:Nanostructures
Donor–acceptor systems
Systèmes donneur–accepteur
Supraconducteurs
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spelling Facile synthesis of nanoparticles of the molecule-based superconductor κ-(BEDT-TTF)2Cu(NCS)2Synthèse aisée de nanoparticules du supraconducteur moléculaire κ-(BEDT-TTF)2Cu(NCS)2Cormary, BenoîtFaulmann, ChristopheCaro, Dominique deValade, LydieCaro, Pascale deBallesteros, BelénFraxedas, J.NanostructuresDonor–acceptor systemsSystèmes donneur–accepteurSupraconducteurs[EN]: Well-dispersed roughly spherical nano-objects of the molecule-based superconductor κ-(BEDT-TTF)2Cu(NCS)2 have been prepared in an organic solution by using an easy synthetic route. Long alkyl-chain aconitate esters have been used as growth controlling agents. Nano-objects exhibiting sizes in the 35–120 nm range are made of aggregated individual smaller nanoparticles ranging from 3 to 10 nm. Nanoparticle powders have been studied by X-ray diffraction, high resolution electron microscopy and atomic force microscopy in the conductivity mode.[FR]: Des nano-objets sphériques et bien dispersés du supraconducteur moléculaire κ-(BEDT-TTF)2Cu(NCS)2 ont été préparés en solution organique à l'aide d'une méthode de synthèse relativement aisée. Des aconitates à longue chaîne alkyle ont été utilisés comme régulateurs de croissance. Ces nano-objets de taille comprise entre 35 et 120 nm sont constitués de petites particules dont le diamètre individuel est de l'ordre de 3 à 10 nm. Les poudres nanoparticulaires ont été étudiées par diffraction des rayons X, par microscopie électronique à haute résolution et enfin par microscopie à force atomique en mode conducteur.B. Cormary thanks the Centre National de la Recherche Scientifique (CNRS) for a post-doctoral fellowship. The authors thank S. Ladeira for XRD characterization and M. Tassé for AFM and IV curves. The authors also thank the GDRI HC3A (Heteroelements and Coordination Chemistry: from Concepts to Applications). The ICN2 is funded by the CERCA programme/Generalitat de Catalunya. The ICN2 is supported by the Severo Ochoa programme of the Spanish Ministry of Economy, Industry and Competitiveness (MINECO, grant no. SEV-2013-0295).Peer reviewedElsevierCentre National de la Recherche Scientifique (France)Generalitat de CatalunyaMinisterio de Economía y Competitividad (España)Ministerio de Economía, Industria y Competitividad (España)Consejo Superior de Investigaciones Científicas [https://ror.org/02gfc7t72]202020202018info:eu-repo/semantics/articlehttp://purl.org/coar/resource_type/c_6501Publisher's versioninfo:eu-repo/semantics/publishedVersionhttp://hdl.handle.net/10261/199194reponame:DIGITAL.CSIC. Repositorio Institucional del CSICinstname:Consejo Superior de Investigaciones Científicas (CSIC)Inglés#PLACEHOLDER_PARENT_METADATA_VALUE#info:eu-repo/grantAgreement/MINECO/Plan Estatal de Investigación Científica y Técnica y de Innovación 2013-2016/SEV-2013-0295https://doi.org/10.1016/j.crci.2018.07.006Síinfo:eu-repo/semantics/openAccessoai:digital.csic.es:10261/1991942026-05-22T06:33:51Z
dc.title.none.fl_str_mv Facile synthesis of nanoparticles of the molecule-based superconductor κ-(BEDT-TTF)2Cu(NCS)2
Synthèse aisée de nanoparticules du supraconducteur moléculaire κ-(BEDT-TTF)2Cu(NCS)2
title Facile synthesis of nanoparticles of the molecule-based superconductor κ-(BEDT-TTF)2Cu(NCS)2
spellingShingle Facile synthesis of nanoparticles of the molecule-based superconductor κ-(BEDT-TTF)2Cu(NCS)2
Cormary, Benoît
Nanostructures
Donor–acceptor systems
Systèmes donneur–accepteur
Supraconducteurs
title_short Facile synthesis of nanoparticles of the molecule-based superconductor κ-(BEDT-TTF)2Cu(NCS)2
title_full Facile synthesis of nanoparticles of the molecule-based superconductor κ-(BEDT-TTF)2Cu(NCS)2
title_fullStr Facile synthesis of nanoparticles of the molecule-based superconductor κ-(BEDT-TTF)2Cu(NCS)2
title_full_unstemmed Facile synthesis of nanoparticles of the molecule-based superconductor κ-(BEDT-TTF)2Cu(NCS)2
title_sort Facile synthesis of nanoparticles of the molecule-based superconductor κ-(BEDT-TTF)2Cu(NCS)2
dc.creator.none.fl_str_mv Cormary, Benoît
Faulmann, Christophe
Caro, Dominique de
Valade, Lydie
Caro, Pascale de
Ballesteros, Belén
Fraxedas, J.
author Cormary, Benoît
author_facet Cormary, Benoît
Faulmann, Christophe
Caro, Dominique de
Valade, Lydie
Caro, Pascale de
Ballesteros, Belén
Fraxedas, J.
author_role author
author2 Faulmann, Christophe
Caro, Dominique de
Valade, Lydie
Caro, Pascale de
Ballesteros, Belén
Fraxedas, J.
author2_role author
author
author
author
author
author
dc.contributor.none.fl_str_mv Centre National de la Recherche Scientifique (France)
Generalitat de Catalunya
Ministerio de Economía y Competitividad (España)
Ministerio de Economía, Industria y Competitividad (España)
Consejo Superior de Investigaciones Científicas [https://ror.org/02gfc7t72]
dc.subject.none.fl_str_mv Nanostructures
Donor–acceptor systems
Systèmes donneur–accepteur
Supraconducteurs
topic Nanostructures
Donor–acceptor systems
Systèmes donneur–accepteur
Supraconducteurs
description [EN]: Well-dispersed roughly spherical nano-objects of the molecule-based superconductor κ-(BEDT-TTF)2Cu(NCS)2 have been prepared in an organic solution by using an easy synthetic route. Long alkyl-chain aconitate esters have been used as growth controlling agents. Nano-objects exhibiting sizes in the 35–120 nm range are made of aggregated individual smaller nanoparticles ranging from 3 to 10 nm. Nanoparticle powders have been studied by X-ray diffraction, high resolution electron microscopy and atomic force microscopy in the conductivity mode.
publishDate 2018
dc.date.none.fl_str_mv 2018
2020
2020
dc.type.none.fl_str_mv info:eu-repo/semantics/article
http://purl.org/coar/resource_type/c_6501
Publisher's version
info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/10261/199194
url http://hdl.handle.net/10261/199194
dc.language.none.fl_str_mv Inglés
language_invalid_str_mv Inglés
dc.relation.none.fl_str_mv #PLACEHOLDER_PARENT_METADATA_VALUE#
info:eu-repo/grantAgreement/MINECO/Plan Estatal de Investigación Científica y Técnica y de Innovación 2013-2016/SEV-2013-0295
https://doi.org/10.1016/j.crci.2018.07.006
Sí
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.publisher.none.fl_str_mv Elsevier
publisher.none.fl_str_mv Elsevier
dc.source.none.fl_str_mv reponame:DIGITAL.CSIC. Repositorio Institucional del CSIC
instname:Consejo Superior de Investigaciones Científicas (CSIC)
instname_str Consejo Superior de Investigaciones Científicas (CSIC)
reponame_str DIGITAL.CSIC. Repositorio Institucional del CSIC
collection DIGITAL.CSIC. Repositorio Institucional del CSIC
repository.name.fl_str_mv
repository.mail.fl_str_mv
_version_ 1869403854718631936
score 15.812429

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