Optimization and characterization of reinforced biodegradable cellulose-based aerogels via polylactic acid/polyhydroxybutyrate coating

Vine shoots (VS) and waste eucalyptus paperboard (EP) have been used as cellulose sources (in the form of cellulose nanocrystals -CNCs- and cellulosic fibers respectively) for developing cellulose-based aerogels. Two different parameters including cellulose concentration (0.5 % and 2 % w/v) and free...

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Detalles Bibliográficos
Autores: Reyes, Alcira, Calleja, Alberto, Gil-Guillén, Irene, Benito González, Isaac
Tipo de recurso: artículo
Estado:Versión aceptada para publicación
Fecha de publicación:2023
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/338722
Acceso en línea:http://hdl.handle.net/10261/338722
https://api.elsevier.com/content/abstract/scopus_id/85173137633
Access Level:acceso abierto
Palabra clave:Biodegradability
Cellulosic aerogels
PHB
PLA
Water resistance
Descripción
Sumario:Vine shoots (VS) and waste eucalyptus paperboard (EP) have been used as cellulose sources (in the form of cellulose nanocrystals -CNCs- and cellulosic fibers respectively) for developing cellulose-based aerogels. Two different parameters including cellulose concentration (0.5 % and 2 % w/v) and freezing temperatures (-20 °C and -80 °C) were tested to evaluate differences in the porosity of the aerogels via Brunauer-Emmett-Teller (BET) and thermal conductivity analyses. In addition, a supplementary coating was applied to the raw aerogels by means of dipping the materials in either polylactic acid (PLA) or polyhydroxybutyrate (PHB) solutions (1 % w/v). Their microstructure was observed via SEM and the reinforcing capacity provided by the coating was measured by means of mechanical compressive tests (~10-fold improvement) and water resistance (contact angle >100°). Finally, aerogels' biodegradability was also confirmed according to the standard ISO 20200 thus providing a sustainable and high-performance alternative to conventional materials also following circular economy principles.