Novel Binders for Aqueous Electrode Processing of Electrochemical Capacitors

This work studies the use of epoxy and polyurethane formulations as binders for the aqueous processing of activated carbon (AC) electrodes used as positive and negative electrodes in Electrochemical Double Layer Capacitors (EDLCs). The use of amine and carbodiimide as crosslinkers is also evaluated....

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Detalles Bibliográficos
Autores: Arnaiz, María, Fernandez, Marcial, Suty, Antoine, Martin-Fuentes, Silvia, Carriazo, Daniel, Bouvet-Marchand, Agathe, Villaverde, Aitor, Morant-Miñana, Maria C.
Tipo de recurso: artículo
Fecha de publicación:2025
País:España
Institución:TECNALIA Research & Innovation
Repositorio:TECNALIA Publications
Idioma:inglés
OAI Identifier:oai:dsp.tecnalia.com:11556/5652
Acceso en línea:https://hdl.handle.net/11556/5652
Access Level:acceso abierto
Palabra clave:Aqueous processing
Epoxy-amine
Flexible supercapacitor
Polyurethane
Waterborne polymer
Environmental Chemistry
General Chemical Engineering
General Materials Science
General Energy
Descripción
Sumario:This work studies the use of epoxy and polyurethane formulations as binders for the aqueous processing of activated carbon (AC) electrodes used as positive and negative electrodes in Electrochemical Double Layer Capacitors (EDLCs). The use of amine and carbodiimide as crosslinkers is also evaluated. The mechanical properties of those different binders have been investigated, looking towards aqueous processable and flexible electrodes. Microstructural analysis of the fabricated AC electrodes has been carried out to understand the pore-blocking effect exhibited by certain polymers. Furthermore, electrochemical characterization of all the systems has been performed by cyclic voltammetry, electrochemical impedance spectroscopy, and constant current charge/discharge measurements at different current densities. The obtained results show that polyurethane (PU) outperforms in terms of energy and power density the carboxymethyl cellulose:styrene butadiene rubber (CMC : SBR) reference system. Moreover, the studied polyurethanes maintain close to 100 % of their initial capacitance after 2500 cycles under a current density of 5 A g−1 and a discharge time of 20 s.