Improving the water resistance of Bi-based perovskite-inspired materials for vapor-phase photocatalytic overall water splitting

[EN] Lead halide perovskites are well known for their exceptional photophysical and electronic properties, which have placed them at the forefront of challenging optoelectronic applications and solar-to-fuel conversion. However, their air/water instability, combined with their toxicity, is still a c...

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Detalhes bibliográficos
Autores: Chacón-García, Antonio J., Pols, Mike, Tao, Shuxia, Calero, Sofía, Vitorica-Yrezabal, Iñigo J., Rodríguez-Diéguez, Antonio, Horcajada, Patricia, Pérez, Yolanda, Garcia-Baldovi, Hermenegildo, Navalón Oltra, Sergio|||0000-0001-8423-0759, García Gómez, Hermenegildo|||0000-0002-9664-493X
Tipo de documento: artigo
Data de publicação:2024
País:España
Recursos:Universitat Politècnica de València (UPV)
Repositório:RiuNet. Repositorio Institucional de la Universitat Politécnica de Valéncia
Idioma:inglês
OAI Identifier:oai:riunet.upv.es:10251/221725
Acesso em linha:https://riunet.upv.es/handle/10251/221725
Access Level:Acceso aberto
Palavra-chave:Lead halide perovskites
Photophysical properties
Electronic properties
Optoelectronic applications
Solar-to-fuel conversion
Descrição
Resumo:[EN] Lead halide perovskites are well known for their exceptional photophysical and electronic properties, which have placed them at the forefront of challenging optoelectronic applications and solar-to-fuel conversion. However, their air/water instability, combined with their toxicity, is still a critical problem that has slowed down their commercialization. In this sense, bismuth-based halide derivatives attract much interest as a potentially safer, air-stable alternative. Herein, a novel Bi-based perovskite-inspired material, IEF-19 (IEF stands for IMDEA Energy Framework), which contains a bulky aromatic cation (1,5-diammonium naphthalene), is prepared. Additionally, an N-alkylation strategy is successfully employed to achieve four water-stable perovskite-inspired materials, which contains diammonium naphthalene cations that are tetra-alkylated by methyl, ethyl, propyl, and butyl groups. Moreover, computational studies are performed to gain a deeper understanding of the intrinsic structural stability and affinity of water molecules for Bi-based perovskite-inspired materials. Importantly, the air- and water-stable IEF-19-Et (i.e., stable at least 12 months under ambient conditions and 3 weeks in contact with water) is found to be an active photocatalyst for vapor-phase overall water splitting in the absence of any sacrificial agent under both ultraviolet-visible or simulated sunlight irradiation. This material exhibits an estimated apparent quantum yield of 0.08% at 400 nm, partially explained by its adequate energy band level diagram.