Multiresidue determination of quinolones regulated by the European Union in bovine and porcine plasma. Application of chromatographic and capillary electrophoretic methodologies

This paper presents the multiresidue determination of the series of quinolones regulated by the European Union (marbofloxacin, ciprofloxacin, danofloxacin, enrofloxacin, sarafloxacin, difloxacin, oxolinic acid and flumequine) in bovine and porcine plasma using capillary electrophoresis and liquid ch...

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Autores: Hermo Outeiral, Ma. del Pilar, Nemutlu, E., Barbosa Torralbo, José, Barrón Bueno, Dolores
Tipo de documento: artigo
Estado:Versión aceptada para publicación
Data de publicação:2011
País:España
Recursos:Varias* (Consorci de Biblioteques Universitáries de Catalunya, Centre de Serveis Científics i Acadèmics de Catalunya)
Repositório:Recercat. Dipósit de la Recerca de Catalunya
OAI Identifier:oai:recercat.cat:2445/158646
Acesso em linha:https://hdl.handle.net/2445/158646
Access Level:Acceso aberto
Palavra-chave:Antibiòtics
Electroforesi capil·lar
Quinolones
Cromatografia de líquids
Antibiotics
Capillary electrophoresis
Quinolone antibacterial agents
Liquid chromatography
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spelling Multiresidue determination of quinolones regulated by the European Union in bovine and porcine plasma. Application of chromatographic and capillary electrophoretic methodologiesHermo Outeiral, Ma. del PilarNemutlu, E.Barbosa Torralbo, JoséBarrón Bueno, DoloresAntibiòticsElectroforesi capil·larQuinolonesCromatografia de líquidsAntibioticsCapillary electrophoresisQuinolone antibacterial agentsLiquid chromatographyThis paper presents the multiresidue determination of the series of quinolones regulated by the European Union (marbofloxacin, ciprofloxacin, danofloxacin, enrofloxacin, sarafloxacin, difloxacin, oxolinic acid and flumequine) in bovine and porcine plasma using capillary electrophoresis and liquid chromatography with ultraviolet detection (CE-UV, LC-UV), liquid chromatography-mass spectrometry and -tandem mass spectrometry (LC-MS, LC-MS/MS) methods. These procedures involve a sample preparation by solid-phase extraction for clean-up and preconcentration of the analytes before their injection into the separation system. All methods give satisfactory results in terms of linearity, precision, accuracy and limits of quantification. The suitability of the methods to determine quinolones was evaluated by determining the concentration of enrofloxacin and ciprofloxacin in real samples from pig plasma and cow plasmaWiley2020202020112020info:eu-repo/semantics/articleinfo:eu-repo/semantics/acceptedVersion15 p.application/pdfhttps://hdl.handle.net/2445/158646Articles publicats en revistes (Nutrició, Ciències de l'Alimentació i Gastronomia)reponame:Recercat. Dipósit de la Recerca de Catalunyainstname:Varias* (Consorci de Biblioteques Universitáries de Catalunya, Centre de Serveis Científics i Acadèmics de Catalunya)InglésVersió postprint del document publicat a: https://doi.org/10.1002/bmc.1483Biomedical Chromatography, 2011, vol. 25, num. 5, p. 555-569https://doi.org/10.1002/bmc.1483(c) Wiley, 2011info:eu-repo/semantics/openAccessoai:recercat.cat:2445/1586462026-05-29T05:05:01Z
dc.title.none.fl_str_mv Multiresidue determination of quinolones regulated by the European Union in bovine and porcine plasma. Application of chromatographic and capillary electrophoretic methodologies
title Multiresidue determination of quinolones regulated by the European Union in bovine and porcine plasma. Application of chromatographic and capillary electrophoretic methodologies
spellingShingle Multiresidue determination of quinolones regulated by the European Union in bovine and porcine plasma. Application of chromatographic and capillary electrophoretic methodologies
Hermo Outeiral, Ma. del Pilar
Antibiòtics
Electroforesi capil·lar
Quinolones
Cromatografia de líquids
Antibiotics
Capillary electrophoresis
Quinolone antibacterial agents
Liquid chromatography
title_short Multiresidue determination of quinolones regulated by the European Union in bovine and porcine plasma. Application of chromatographic and capillary electrophoretic methodologies
title_full Multiresidue determination of quinolones regulated by the European Union in bovine and porcine plasma. Application of chromatographic and capillary electrophoretic methodologies
title_fullStr Multiresidue determination of quinolones regulated by the European Union in bovine and porcine plasma. Application of chromatographic and capillary electrophoretic methodologies
title_full_unstemmed Multiresidue determination of quinolones regulated by the European Union in bovine and porcine plasma. Application of chromatographic and capillary electrophoretic methodologies
title_sort Multiresidue determination of quinolones regulated by the European Union in bovine and porcine plasma. Application of chromatographic and capillary electrophoretic methodologies
dc.creator.none.fl_str_mv Hermo Outeiral, Ma. del Pilar
Nemutlu, E.
Barbosa Torralbo, José
Barrón Bueno, Dolores
author Hermo Outeiral, Ma. del Pilar
author_facet Hermo Outeiral, Ma. del Pilar
Nemutlu, E.
Barbosa Torralbo, José
Barrón Bueno, Dolores
author_role author
author2 Nemutlu, E.
Barbosa Torralbo, José
Barrón Bueno, Dolores
author2_role author
author
author
dc.subject.none.fl_str_mv Antibiòtics
Electroforesi capil·lar
Quinolones
Cromatografia de líquids
Antibiotics
Capillary electrophoresis
Quinolone antibacterial agents
Liquid chromatography
topic Antibiòtics
Electroforesi capil·lar
Quinolones
Cromatografia de líquids
Antibiotics
Capillary electrophoresis
Quinolone antibacterial agents
Liquid chromatography
description This paper presents the multiresidue determination of the series of quinolones regulated by the European Union (marbofloxacin, ciprofloxacin, danofloxacin, enrofloxacin, sarafloxacin, difloxacin, oxolinic acid and flumequine) in bovine and porcine plasma using capillary electrophoresis and liquid chromatography with ultraviolet detection (CE-UV, LC-UV), liquid chromatography-mass spectrometry and -tandem mass spectrometry (LC-MS, LC-MS/MS) methods. These procedures involve a sample preparation by solid-phase extraction for clean-up and preconcentration of the analytes before their injection into the separation system. All methods give satisfactory results in terms of linearity, precision, accuracy and limits of quantification. The suitability of the methods to determine quinolones was evaluated by determining the concentration of enrofloxacin and ciprofloxacin in real samples from pig plasma and cow plasma
publishDate 2011
dc.date.none.fl_str_mv 2011
2020
2020
2020
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/acceptedVersion
format article
status_str acceptedVersion
dc.identifier.none.fl_str_mv https://hdl.handle.net/2445/158646
url https://hdl.handle.net/2445/158646
dc.language.none.fl_str_mv Inglés
language_invalid_str_mv Inglés
dc.relation.none.fl_str_mv Versió postprint del document publicat a: https://doi.org/10.1002/bmc.1483
Biomedical Chromatography, 2011, vol. 25, num. 5, p. 555-569
https://doi.org/10.1002/bmc.1483
dc.rights.none.fl_str_mv (c) Wiley, 2011
info:eu-repo/semantics/openAccess
rights_invalid_str_mv (c) Wiley, 2011
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv 15 p.
application/pdf
dc.publisher.none.fl_str_mv Wiley
publisher.none.fl_str_mv Wiley
dc.source.none.fl_str_mv Articles publicats en revistes (Nutrició, Ciències de l'Alimentació i Gastronomia)
reponame:Recercat. Dipósit de la Recerca de Catalunya
instname:Varias* (Consorci de Biblioteques Universitáries de Catalunya, Centre de Serveis Científics i Acadèmics de Catalunya)
instname_str Varias* (Consorci de Biblioteques Universitáries de Catalunya, Centre de Serveis Científics i Acadèmics de Catalunya)
reponame_str Recercat. Dipósit de la Recerca de Catalunya
collection Recercat. Dipósit de la Recerca de Catalunya
repository.name.fl_str_mv
repository.mail.fl_str_mv
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score 15.812455

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