Germanium recovery from zinc calcines using a hydrometallurgical procedure

[EN] In the final stage of zinc calcines processing, zinc is recovered by zinc electrowinning. However, he presence of germanium in the electrolyte seriously affects the current density in the electrowinning step. Since germanium is a critical and strategic material for the European Union according...

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Detalles Bibliográficos
Autores: Alguacil, Francisco José, Alonso Gámez, Manuel, Lozano-Blanco, Luis J., Robla, J. I.
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2025
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/417564
Acceso en línea:http://hdl.handle.net/10261/417564
Access Level:acceso abierto
Palabra clave:Germanium
Germanium(IV) oxide
Ionic liquid
Leaching
Precipitation
Solvent extraction
Zinc calcines
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Descripción
Sumario:[EN] In the final stage of zinc calcines processing, zinc is recovered by zinc electrowinning. However, he presence of germanium in the electrolyte seriously affects the current density in the electrowinning step. Since germanium is a critical and strategic material for the European Union according to the most recent foresight studies, this research has focused on an alternative route for the treatment of germanium concentrates (0.1 wt Ge) obtained after the roasting step in conventional zinc processes. The results showed that this concentrate can be treated by leaching in mild acidic medium (90% germanium efficiency)-solvent extraction with an ionic liquid and alkaline stripping (99% germanium recovery), followed by neutralization and precipitation steps to yield GeO2 as end-product. The overall germanium recovery was around 85%.