Potentiometric analytical microsystem based on the integration of a gas-diffusion step for on-line ammonium determination in water recycling processes in manned space missions

The design, construction and evaluation of a versatile cyclic olefin copolymer (COC)-based continuous flow potentiometric microanalyzer to monitor the presence of ammonium ion in recycling water processes for future manned space missions is presented. The microsystem integrates microfluidics, a gas-...

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Detalles Bibliográficos
Autores: Calvo-López, Antonio|||0000-0003-2728-8676, Ymbern Llorens, Oriol|||0000-0003-1997-6794, Puyol, Mar|||0000-0002-9274-2284, Casalta, Joan Manel, Alonso-Chamarro, Julián|||0000-0002-6804-6027
Tipo de recurso: artículo
Fecha de publicación:2015
País:España
Institución:Universitat Autònoma de Barcelona
Repositorio:Dipòsit Digital de Documents de la UAB
Idioma:inglés
OAI Identifier:oai:ddd.uab.cat:287977
Acceso en línea:https://ddd.uab.cat/record/287977
https://dx.doi.org/urn:doi:10.1016/j.aca.2014.12.038
Access Level:acceso abierto
Palabra clave:Ammonium ion
Gas-diffusion
Lab on a chip
Miniaturization
Polymer technology
Potentiometric detection
Descripción
Sumario:The design, construction and evaluation of a versatile cyclic olefin copolymer (COC)-based continuous flow potentiometric microanalyzer to monitor the presence of ammonium ion in recycling water processes for future manned space missions is presented. The microsystem integrates microfluidics, a gas-diffusion module and a detection system in a single substrate. The gas-diffusion module was integrated by a hydrophobic polyvinylidene fluoride (PVDF) membrane. The potentiometric detection system is based on an all-solid state ammonium selective electrode and a screen-printed Ag/AgCl reference electrode. The analytical features provided by the analytical microsystem after the optimization process were a linear range from 0.15 to 500mgL-1 and a detection limit of 0.07±0.01mgL-1. Nevertheless, the operational features can be easily adapted to other applications through the modification of the hydrodynamic variables of the microfluidic platform.