Semiconducting Polymer Nanoparticles Enable Light-Controlled Bidirectional Modulation of Nitric Oxide in Endothelial Cells

Endothelial-derived nitric oxide (·NO) is a key signaling molecule in the vascular system, exerting concentration-dependent control over critical cellular functions such as angiogenesis, vascular tone, and endothelial barrier integrity. Tools for achieving reversible, spatiotemporally resolved modul...

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Detalles Bibliográficos
Autores: Marzuoli, Camilla, Pianetti, Andrea, Mancinelli, Elena, Villano, Anthea, Vailati, Matteo, Lagonegro, Paola, Criado-González, Miryam, Climent, Montserrat, Comas-Rojas, Hansel, Elia, Leonardo, Moccia, Francesco, Tullii, Gabriele, Antognazza, Maria Rosa
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2026
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/421754
Acceso en línea:http://hdl.handle.net/10261/421754
https://api.elsevier.com/content/abstract/scopus_id/105030679630
Access Level:acceso abierto
Palabra clave:Conjugated polymer
Endothelial cells
Light
Nitric oxide
Organic bioelectronics
Photo‐redox modulation
Semiconducting polymer nanoparticles
Descripción
Sumario:Endothelial-derived nitric oxide (·NO) is a key signaling molecule in the vascular system, exerting concentration-dependent control over critical cellular functions such as angiogenesis, vascular tone, and endothelial barrier integrity. Tools for achieving reversible, spatiotemporally resolved modulation of intracellular ·NO, without pharmacological or genetic manipulation, are currently lacking. Here, we present a light-activated, nanoparticle (NP)-based strategy enabling bidirectional control of endogenous ·NO in endothelial cells. Composite NPs, based on poly(3-hexylthiophene), P3HT, and poly(3,4-ethylene-dioxythiophene):poly(styrenesulfonate), PEDOT:PSS polymers, are efficiently internalized in human (HUVEC) and murine (H5V) endothelial cells. In dark, NP uptake induces a ROS-dependent, intracellular ·NO increase (+50% and +100% in HUVEC and H5V, respectively, vs. controls), a metabolic shift toward glycolysis and upregulation of both endothelial nitric oxide synthase (eNOS, +50%) and induced nitric oxide synthase (iNOS, +40%). NP photostimulation reverses this response, decreasing ·NO below basal levels, up to -40% in HUVEC and H5V, via ROS-mediated scavenging and iNOS downregulation (-40%), partially restoring oxidative phosphorylation metabolism. Importantly, the photoexcitation protocol is compatible with perspective in vivo use, in terms of source type (LEDs) and power density (6 mW/cm2). Our approach represents an innovative strategy for bidirectional endothelial ·NO modulation, providing new opportunities in the emerging field of photo-redox medicine.