Electrochemical Study of Self-assembled Monolayer of Cysteamine Functionalized with 6-methyl-2-pirydincarboxaldehyde

This paper presents a systematic study of the Self-Assembled Monolayer (SAM) of Cisteamine (CA) on gold electrodes functionalized with 6-Methyl-2 Pyridinecarboxaldehyde (MPC) in order to quantitate its binding capacity with metal ions in aqueous solution. The electrochemical properties of gold surfa...

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Detalles Bibliográficos
Autores: Rendón Enríquez, Ibeth, Aguilar Cordero, Julio César
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2011
País:Ecuador
Institución:Universidad Central del Ecuador
Repositorio:Revista Química central
Idioma:español
OAI Identifier:oai:revistadigital.uce.edu.ec:article/548
Acceso en línea:https://revistadigital.uce.edu.ec/index.php/QUIMICA/article/view/548
Access Level:acceso abierto
Palabra clave:Monocapas Autoensambladas (MAEs)
Voltamperometría Cíclica (VC)
Espectroscopía Electroquímica de Impedancia (EIS)
Microscopía Electroquímica de Barrido (SECM)
Self-Assembled Monolayers (SAMs)
Ciclic Voltammetry (CV)
Electrochemical Impedance Spectroscopy (EIS)
Scanning Electrochemical Microscopy (SECM)
Descripción
Sumario:This paper presents a systematic study of the Self-Assembled Monolayer (SAM) of Cisteamine (CA) on gold electrodes functionalized with 6-Methyl-2 Pyridinecarboxaldehyde (MPC) in order to quantitate its binding capacity with metal ions in aqueous solution. The electrochemical properties of gold surfaces modified in the presence of a redox mediator were studied with Cyclic Voltamperommetry (CV) and Electrochemical Impedance Spectroscopy (EIS). The effect of the analyte (CA, MPC or metal ions) and the buffer solution was also evaluated. The Schiff base formed with MPC can not stabilize in the buffer solution, and it is not posible to use the modified electrode as an impedimetric sensor.