Adsorption of the rare earth elements cerium, lanthanum, and neodymium onto ZSM-5 zeolite: A statistical physics approach

The recovery of rare earth elements (REE) is essential to meet the growing demand for these resources and promote the reuse of available resources. This study investigated the potential of ZSM-5 zeolite in the recovery of trivalent ions of cerium, lanthanum and neodymium under conditions of pH 6 and...

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Authors: Piazzi Fuhr, Ana Carolina Ferreira, Pinto, Diana, Silva Oliveira, Luis Felipe, Hessien, Mahmoud M., Alshammari, Dalal A., El-Bahy, Zeinhom M., Dotto, Guilherme Luiz
Format: article
Status:Published version
Publication Date:2024
Country:Colombia
Institution:Corporación Universidad de la Costa
Repository:Repositorio REDICUC
Language:English
OAI Identifier:oai:repositorio.cuc.edu.co:11323/13313
Online Access:https://hdl.handle.net/11323/13313
https://repositorio.cuc.edu.co/
Access Level:Embargoed access
Keyword:Rare earth elements
Adsorption
Isotherms
Statistical physic models
Mechanism
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dc.title.none.fl_str_mv Adsorption of the rare earth elements cerium, lanthanum, and neodymium onto ZSM-5 zeolite: A statistical physics approach
title Adsorption of the rare earth elements cerium, lanthanum, and neodymium onto ZSM-5 zeolite: A statistical physics approach
spellingShingle Adsorption of the rare earth elements cerium, lanthanum, and neodymium onto ZSM-5 zeolite: A statistical physics approach
Piazzi Fuhr, Ana Carolina Ferreira
Rare earth elements
Adsorption
Isotherms
Statistical physic models
Mechanism
title_short Adsorption of the rare earth elements cerium, lanthanum, and neodymium onto ZSM-5 zeolite: A statistical physics approach
title_full Adsorption of the rare earth elements cerium, lanthanum, and neodymium onto ZSM-5 zeolite: A statistical physics approach
title_fullStr Adsorption of the rare earth elements cerium, lanthanum, and neodymium onto ZSM-5 zeolite: A statistical physics approach
title_full_unstemmed Adsorption of the rare earth elements cerium, lanthanum, and neodymium onto ZSM-5 zeolite: A statistical physics approach
title_sort Adsorption of the rare earth elements cerium, lanthanum, and neodymium onto ZSM-5 zeolite: A statistical physics approach
dc.creator.none.fl_str_mv Piazzi Fuhr, Ana Carolina Ferreira
Pinto, Diana
Silva Oliveira, Luis Felipe
Hessien, Mahmoud M.
Alshammari, Dalal A.
El-Bahy, Zeinhom M.
Dotto, Guilherme Luiz
author Piazzi Fuhr, Ana Carolina Ferreira
author_facet Piazzi Fuhr, Ana Carolina Ferreira
Pinto, Diana
Silva Oliveira, Luis Felipe
Hessien, Mahmoud M.
Alshammari, Dalal A.
El-Bahy, Zeinhom M.
Dotto, Guilherme Luiz
author_role author
author2 Pinto, Diana
Silva Oliveira, Luis Felipe
Hessien, Mahmoud M.
Alshammari, Dalal A.
El-Bahy, Zeinhom M.
Dotto, Guilherme Luiz
author2_role author
author
author
author
author
author
dc.subject.none.fl_str_mv Rare earth elements
Adsorption
Isotherms
Statistical physic models
Mechanism
topic Rare earth elements
Adsorption
Isotherms
Statistical physic models
Mechanism
description The recovery of rare earth elements (REE) is essential to meet the growing demand for these resources and promote the reuse of available resources. This study investigated the potential of ZSM-5 zeolite in the recovery of trivalent ions of cerium, lanthanum and neodymium under conditions of pH 6 and temperatures between 298 and 328 K. REE equilibrium isotherms were analyzed using five statistical physics models. The results indicate that removing all REE occurs predominantly in monolayers, as these models showed better prediction performance (coefficient of determination > 0.97 and mean squared error < 18.0). The best model determined that lanthanum and neodymium have one adsorption energy, while cerium has two adsorption energies involved in the process. The predominant functional groups are those containing silicon. Increasing temperature causes an increase in the number of REE ions captured per functional group, which reduces the adsorption space available on the surface. The model parameters indicate that the adsorption of these ions implies a multi-ionic mechanism (number of ions adsorbed per site greater than 1) and is an exothermic process. Based on the calculated adsorption capacities at saturation, the order of preference in adsorption can be established: neodymium > cerium > lanthanum. The adsorption energies indicate that the process occurred mainly due to physical forces since all energy values are below 40 kJ mol−1. The study’s results led to the proposal of a mechanism for the adsorption of REE on ZSM-5 zeolite, which highlights the predominance of electrostatic interactions and complex formation, which result in the formation of a monolayer on the adsorbent’s surface.
publishDate 2024
dc.date.none.fl_str_mv 2024-09-12T19:14:43Z
2024-09-12T19:14:43Z
2024-07-01
2026-07-01
dc.type.none.fl_str_mv Artículo de revista
http://purl.org/coar/resource_type/c_2df8fbb1
Text
info:eu-repo/semantics/article
http://purl.org/redcol/resource_type/ART
info:eu-repo/semantics/publishedVersion
http://purl.org/coar/version/c_970fb48d4fbd8a85
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv Ana Carolina Ferreira Piazzi Fuhr, Diana Pinto, Luis Felipe Oliveira Silva, Mahmoud M. Hessien, Dalal A. Alshammari, Zeinhom M. El-Bahy, Guilherme Luiz Dotto, Adsorption of the rare earth elements cerium, lanthanum, and neodymium onto ZSM-5 zeolite: A statistical physics approach, Journal of Molecular Liquids, Volume 405, 2024, 125035, ISSN 0167-7322, https://doi.org/10.1016/j.molliq.2024.125035.
0167-7322
https://hdl.handle.net/11323/13313
10.1016/j.molliq.2024.125035
1873-3166
Corporación Universidad de la Costa
REDICUC - Repositorio CUC
https://repositorio.cuc.edu.co/
identifier_str_mv Ana Carolina Ferreira Piazzi Fuhr, Diana Pinto, Luis Felipe Oliveira Silva, Mahmoud M. Hessien, Dalal A. Alshammari, Zeinhom M. El-Bahy, Guilherme Luiz Dotto, Adsorption of the rare earth elements cerium, lanthanum, and neodymium onto ZSM-5 zeolite: A statistical physics approach, Journal of Molecular Liquids, Volume 405, 2024, 125035, ISSN 0167-7322, https://doi.org/10.1016/j.molliq.2024.125035.
0167-7322
10.1016/j.molliq.2024.125035
1873-3166
Corporación Universidad de la Costa
REDICUC - Repositorio CUC
url https://hdl.handle.net/11323/13313
https://repositorio.cuc.edu.co/
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv Journal of Molecular Liquids
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dc.publisher.none.fl_str_mv Elsevier B.V.
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publisher.none.fl_str_mv Elsevier B.V.
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spelling Adsorption of the rare earth elements cerium, lanthanum, and neodymium onto ZSM-5 zeolite: A statistical physics approachPiazzi Fuhr, Ana Carolina FerreiraPinto, DianaSilva Oliveira, Luis FelipeHessien, Mahmoud M.Alshammari, Dalal A.El-Bahy, Zeinhom M.Dotto, Guilherme LuizRare earth elementsAdsorptionIsothermsStatistical physic modelsMechanismThe recovery of rare earth elements (REE) is essential to meet the growing demand for these resources and promote the reuse of available resources. This study investigated the potential of ZSM-5 zeolite in the recovery of trivalent ions of cerium, lanthanum and neodymium under conditions of pH 6 and temperatures between 298 and 328 K. REE equilibrium isotherms were analyzed using five statistical physics models. The results indicate that removing all REE occurs predominantly in monolayers, as these models showed better prediction performance (coefficient of determination > 0.97 and mean squared error < 18.0). The best model determined that lanthanum and neodymium have one adsorption energy, while cerium has two adsorption energies involved in the process. The predominant functional groups are those containing silicon. Increasing temperature causes an increase in the number of REE ions captured per functional group, which reduces the adsorption space available on the surface. The model parameters indicate that the adsorption of these ions implies a multi-ionic mechanism (number of ions adsorbed per site greater than 1) and is an exothermic process. Based on the calculated adsorption capacities at saturation, the order of preference in adsorption can be established: neodymium > cerium > lanthanum. The adsorption energies indicate that the process occurred mainly due to physical forces since all energy values are below 40 kJ mol−1. The study’s results led to the proposal of a mechanism for the adsorption of REE on ZSM-5 zeolite, which highlights the predominance of electrostatic interactions and complex formation, which result in the formation of a monolayer on the adsorbent’s surface.Elsevier B.V.Netherlands2024-09-12T19:14:43Z2026-07-012024-09-12T19:14:43Z2024-07-01Artículo de revistahttp://purl.org/coar/resource_type/c_2df8fbb1Textinfo:eu-repo/semantics/articlehttp://purl.org/redcol/resource_type/ARTinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/version/c_970fb48d4fbd8a8512 páginasapplication/pdfapplication/pdfAna Carolina Ferreira Piazzi Fuhr, Diana Pinto, Luis Felipe Oliveira Silva, Mahmoud M. Hessien, Dalal A. Alshammari, Zeinhom M. El-Bahy, Guilherme Luiz Dotto, Adsorption of the rare earth elements cerium, lanthanum, and neodymium onto ZSM-5 zeolite: A statistical physics approach, Journal of Molecular Liquids, Volume 405, 2024, 125035, ISSN 0167-7322, https://doi.org/10.1016/j.molliq.2024.125035.0167-7322https://hdl.handle.net/11323/1331310.1016/j.molliq.2024.1250351873-3166Corporación Universidad de la CostaREDICUC - Repositorio CUChttps://repositorio.cuc.edu.co/https://www.sciencedirect.com/science/article/pii/S0167732224010912?pes=vorreponame:Repositorio REDICUCinstname:Corporación Universidad de la Costainstacron:Corporación Universidad de la CostaengJournal of Molecular Liquids[1] Executive summary – The Role of Critical Minerals in Clean Energy Transitions – Analysis, IEA (n.d.). https://www.iea.org/reports/the-role-of-critical-minerals-inclean-energy-transitions/executive-summary (accessed February 21, 2024).[2] The race to produce rare earth elements, MIT Technology Review (n.d.). https:// www.technologyreview.com/2024/01/05/1084791/rare-earth-materialsclean-energy/ (accessed February 21, 2024).[3] Global Rare Earth Metals Market Size & Forecast, [Latest], MarketsandMarkets (n. d.). https://www.marketsandmarkets.com/Market-Reports/rare-earth-metals-ma rket-121495310.html (accessed February 21, 2024).[4] F. 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Res. 27 (2020) 36052–36074, https://doi.org/10.1007/s11356-020-09630-2.[8] T. Kegl, A. Koˇsak, A. Lobnik, Z. Novak, A.K. Kralj, I. Ban, Adsorption of rare earth metals from wastewater by nanomaterials: A review, J. Hazard. Mater. 386 (2020) 121632, https://doi.org/10.1016/j.jhazmat.2019.121632.[9] T.B.D. Costa, M.G.C.D. Silva, M.G.A. Vieira, Recovery of rare-earth metals from aqueous solutions by bio/adsorption using non-conventional materials: A review with recent studies and promising approaches in column applications, J. Rare Earths 38 (2020) 339–355, https://doi.org/10.1016/j.jre.2019.06.001.[10] S. Iftekhar, G. Heidari, N. Amanat, E.N. Zare, M.B. Asif, M. Hassanpour, V.P. Lehto, M. Sillanpaa, Porous materials for the recovery of rare earth elements, platinum group metals, and other valuable metals: A review, Environ. Chem. Lett. 20 (2022) 3697–3746, https://doi.org/10.1007/s10311-022-01486-x.[11] O. Artiushenko, R.F. Da Silva, V. 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