Mössbauer and X-ray study of the Fe 65 Ni 35 invar alloy obtained by mechanical alloying

Fe65Ni35 samples were prepared by mechanical alloying (MA) with milling times of 5, 6, 7, 10 and 11 h, using a ball mass to powder mass ratio of 20:1 and at 280 rpm. The samples were characterized by X-ray diffraction (XRD) and transmission 57Fe Mössbauer spectrometry. The X-ray diffraction pattern...

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Detalhes bibliográficos
Autores: Rodríguez Jacobo, Ruby Rocío, Valenzuela, J. L, Tabares Giraldo, Jesús Anselmo, Pérez Alcázar, German Antonio
Formato: artículo
Estado:Versión publicada
Fecha de publicación:2013
País:Colombia
Recursos:Universidad Autónoma de Occidente
Repositorio:RED: Repositorio Educativo Digital UAO
Idioma:español
OAI Identifier:oai:red.uao.edu.co:10614/11848
Acesso em linha:http://hdl.handle.net/10614/11848
Access Level:acceso abierto
Palavra-chave:Aleación mecánica
FeNi
Mechanical alloying
Invar composition
Mössbauer spectrometry
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spelling Mössbauer and X-ray study of the Fe 65 Ni 35 invar alloy obtained by mechanical alloyingRodríguez Jacobo, Ruby RocíoValenzuela, J. LTabares Giraldo, Jesús AnselmoPérez Alcázar, German AntonioAleación mecánicaFeNiMechanical alloyingInvar compositionMössbauer spectrometryFe65Ni35 samples were prepared by mechanical alloying (MA) with milling times of 5, 6, 7, 10 and 11 h, using a ball mass to powder mass ratio of 20:1 and at 280 rpm. The samples were characterized by X-ray diffraction (XRD) and transmission 57Fe Mössbauer spectrometry. The X-ray diffraction pattern showed the coexistence of one body centered cubic (BCC) and two face centered cubic (FCC1 and FCC2) structural phases. The lattice parameters of these phases did not change significantly with the milling time (2.866 Å, 3.597 Å and 3.538 Å, respectively). After 10 h of milling, the X-ray diffraction pattern showed clearly the coexistence of these three phases. Hence, Mössbauer spectrometry measurements at low temperatures from 20 to 300 K of this sample were also carried out. The Mössbauer spectra were fitted using a model with three components: the first one is a hyperfine magnetic field distributions at high fields, related to the BCC phase; the second one is a hyperfine magnetic field distribution involving low hyperfine fields related to a FCC phase rich in Ni, and the third one is a singlet related to a FCC phase rich in Fe, with paramagnetic behavior. As proposed by some authors, the last phase is related with the antitaenite phaseUniversidad Autónoma de Occidente2020-02-10T14:46:47Z2020-02-10T14:46:47Z2013-03-13Artículo de revistahttp://purl.org/coar/resource_type/c_6501Textinfo:eu-repo/semantics/articlehttp://purl.org/redcol/resource_type/ARTREFinfo:eu-repo/semantics/publishedVersionapplication/pdf8 páginashttp://hdl.handle.net/10614/1184810.1007/s10751-013-0834-5spa330323224Hyperfine InteractionsTcherdyntsev, V.V., Kaloshkin, S.D., Tomilin, I.A., Shelekhov, E.V., Baldokhin, Yu.V.: Nanostruct. Mater. 12, 139–142 (1999)Hellstern, E., Schultz, L.: J. Appl. Phys. 63, 1408 (1988)Suryanarayana, C.: Prog. Mater. Sci. 46, 1–184 (2001)Hellstern, E., Fecht, H.J., Fu, Z., Johnson, W.L.: J. Appl. Phys. 65, 305 (1989)Djekoun, A., Otmani, A., Bouzabata, B., Bechiri, L., Randrianantoandro, N., Greneche, J.M.: Catal. Today 113, 235–239 (2006)Valderruten, J.F., Pérez Alcázar, G.A., Greneche, J.M.: J. Phys. Condens. Matter 20, 485204 (2008)Scorzelli, R.B.: Hyperfine Interact. 110, 143–150 (1997)Valderruten, J.F., Pérez Alcázar, G.A., Greneche, J.M.: Hyperfine Interact. 195, 219–226 (2010)Rancourt, D.G., Scorzelli, R.B.: J. Magn. Magn. Mater. 150, 30 (1995)Larson, A.C., Von Dreele, R.B.: General structure analysis system (GSAS). Los Alamos Natl. Lab. Rep. No. LAUR 86–748 (2004)Teillet, J., Varret, F.: Mosfit Programm, University du Maine, France (unpublished)Petrov, Yu.I., Shafranovsky, E.A., Baldokhin, Yu.V., Kochetov, G.A.: J. Appl. Phys. 86(12), 7001 (1999)Rancourt, D.G., Lagarec, K., Densmore, A., Dunlap, R.A., Goldstein, J.I., Reisener, R.J., Scorzelli, R.B.: J. Magn. Magn. Mater. 191, L255–L260 (1999)Restrepo, J., Pérez Alcázar, G.A., Bohórquez, A.: J. Appl. Phys. 81(8), 4101 (1997)Derechos Reservados - Universidad Autónoma de Occidentehttps://creativecommons.org/licenses/by-nc-nd/4.0/info:eu-repo/semantics/openAccessAtribución-NoComercial-SinDerivadas 4.0 Internacional (CC BY-NC-ND 4.0)reponame:RED: Repositorio Educativo Digital UAOinstname:Universidad Autónoma de Occidenteinstacron:Universidad Autónoma de Occidente2024-03-14T13:47:17Z
dc.title.none.fl_str_mv Mössbauer and X-ray study of the Fe 65 Ni 35 invar alloy obtained by mechanical alloying
title Mössbauer and X-ray study of the Fe 65 Ni 35 invar alloy obtained by mechanical alloying
spellingShingle Mössbauer and X-ray study of the Fe 65 Ni 35 invar alloy obtained by mechanical alloying
Rodríguez Jacobo, Ruby Rocío
Aleación mecánica
FeNi
Mechanical alloying
Invar composition
Mössbauer spectrometry
title_short Mössbauer and X-ray study of the Fe 65 Ni 35 invar alloy obtained by mechanical alloying
title_full Mössbauer and X-ray study of the Fe 65 Ni 35 invar alloy obtained by mechanical alloying
title_fullStr Mössbauer and X-ray study of the Fe 65 Ni 35 invar alloy obtained by mechanical alloying
title_full_unstemmed Mössbauer and X-ray study of the Fe 65 Ni 35 invar alloy obtained by mechanical alloying
title_sort Mössbauer and X-ray study of the Fe 65 Ni 35 invar alloy obtained by mechanical alloying
dc.creator.none.fl_str_mv Rodríguez Jacobo, Ruby Rocío
Valenzuela, J. L
Tabares Giraldo, Jesús Anselmo
Pérez Alcázar, German Antonio
author Rodríguez Jacobo, Ruby Rocío
author_facet Rodríguez Jacobo, Ruby Rocío
Valenzuela, J. L
Tabares Giraldo, Jesús Anselmo
Pérez Alcázar, German Antonio
author_role author
author2 Valenzuela, J. L
Tabares Giraldo, Jesús Anselmo
Pérez Alcázar, German Antonio
author2_role author
author
author
dc.subject.none.fl_str_mv Aleación mecánica
FeNi
Mechanical alloying
Invar composition
Mössbauer spectrometry
topic Aleación mecánica
FeNi
Mechanical alloying
Invar composition
Mössbauer spectrometry
description Fe65Ni35 samples were prepared by mechanical alloying (MA) with milling times of 5, 6, 7, 10 and 11 h, using a ball mass to powder mass ratio of 20:1 and at 280 rpm. The samples were characterized by X-ray diffraction (XRD) and transmission 57Fe Mössbauer spectrometry. The X-ray diffraction pattern showed the coexistence of one body centered cubic (BCC) and two face centered cubic (FCC1 and FCC2) structural phases. The lattice parameters of these phases did not change significantly with the milling time (2.866 Å, 3.597 Å and 3.538 Å, respectively). After 10 h of milling, the X-ray diffraction pattern showed clearly the coexistence of these three phases. Hence, Mössbauer spectrometry measurements at low temperatures from 20 to 300 K of this sample were also carried out. The Mössbauer spectra were fitted using a model with three components: the first one is a hyperfine magnetic field distributions at high fields, related to the BCC phase; the second one is a hyperfine magnetic field distribution involving low hyperfine fields related to a FCC phase rich in Ni, and the third one is a singlet related to a FCC phase rich in Fe, with paramagnetic behavior. As proposed by some authors, the last phase is related with the antitaenite phase
publishDate 2013
dc.date.none.fl_str_mv 2013-03-13
2020-02-10T14:46:47Z
2020-02-10T14:46:47Z
dc.type.none.fl_str_mv Artículo de revista
http://purl.org/coar/resource_type/c_6501
Text
info:eu-repo/semantics/article
http://purl.org/redcol/resource_type/ARTREF
info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/10614/11848
10.1007/s10751-013-0834-5
url http://hdl.handle.net/10614/11848
identifier_str_mv 10.1007/s10751-013-0834-5
dc.language.none.fl_str_mv spa
language spa
dc.relation.none.fl_str_mv 330
323
224
Hyperfine Interactions
Tcherdyntsev, V.V., Kaloshkin, S.D., Tomilin, I.A., Shelekhov, E.V., Baldokhin, Yu.V.: Nanostruct. Mater. 12, 139–142 (1999)
Hellstern, E., Schultz, L.: J. Appl. Phys. 63, 1408 (1988)
Suryanarayana, C.: Prog. Mater. Sci. 46, 1–184 (2001)
Hellstern, E., Fecht, H.J., Fu, Z., Johnson, W.L.: J. Appl. Phys. 65, 305 (1989)
Djekoun, A., Otmani, A., Bouzabata, B., Bechiri, L., Randrianantoandro, N., Greneche, J.M.: Catal. Today 113, 235–239 (2006)
Valderruten, J.F., Pérez Alcázar, G.A., Greneche, J.M.: J. Phys. Condens. Matter 20, 485204 (2008)
Scorzelli, R.B.: Hyperfine Interact. 110, 143–150 (1997)
Valderruten, J.F., Pérez Alcázar, G.A., Greneche, J.M.: Hyperfine Interact. 195, 219–226 (2010)
Rancourt, D.G., Scorzelli, R.B.: J. Magn. Magn. Mater. 150, 30 (1995)
Larson, A.C., Von Dreele, R.B.: General structure analysis system (GSAS). Los Alamos Natl. Lab. Rep. No. LAUR 86–748 (2004)
Teillet, J., Varret, F.: Mosfit Programm, University du Maine, France (unpublished)
Petrov, Yu.I., Shafranovsky, E.A., Baldokhin, Yu.V., Kochetov, G.A.: J. Appl. Phys. 86(12), 7001 (1999)
Rancourt, D.G., Lagarec, K., Densmore, A., Dunlap, R.A., Goldstein, J.I., Reisener, R.J., Scorzelli, R.B.: J. Magn. Magn. Mater. 191, L255–L260 (1999)
Restrepo, J., Pérez Alcázar, G.A., Bohórquez, A.: J. Appl. Phys. 81(8), 4101 (1997)
dc.rights.none.fl_str_mv Derechos Reservados - Universidad Autónoma de Occidente
https://creativecommons.org/licenses/by-nc-nd/4.0/
info:eu-repo/semantics/openAccess
Atribución-NoComercial-SinDerivadas 4.0 Internacional (CC BY-NC-ND 4.0)
rights_invalid_str_mv Derechos Reservados - Universidad Autónoma de Occidente
https://creativecommons.org/licenses/by-nc-nd/4.0/
Atribución-NoComercial-SinDerivadas 4.0 Internacional (CC BY-NC-ND 4.0)
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
8 páginas
dc.publisher.none.fl_str_mv Universidad Autónoma de Occidente
publisher.none.fl_str_mv Universidad Autónoma de Occidente
dc.source.none.fl_str_mv reponame:RED: Repositorio Educativo Digital UAO
instname:Universidad Autónoma de Occidente
instacron:Universidad Autónoma de Occidente
instname_str Universidad Autónoma de Occidente
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reponame_str RED: Repositorio Educativo Digital UAO
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