Chromatography-Independent Fractionation and Newly Identified Molecular Features of the Adzuki Bean (Vigna angularis Willd.) beta-vignin Protein

Adzuki seed beta-vignin, a vicilin-like globulin, has proven to exert various health-promoting biological activities, notably in cardiovascular health. A simple scalable enrichment procedure of this protein for further nutritional and functional studies is crucial. In this study, a simplified chroma...

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Detalles Bibliográficos
Autores: Philadelpho, Biane, Souza, Victoria, Souza, Fabiani, Santos, Johnnie, Batista, Fabiana, Silva, Mariana [UNESP], Capraro, Jessica, De Benedetti, Stefano, Heinzl, Giuditta C., Cilli, Eduardo [UNESP], Scarafoni, Alessio, Magni, Chiara, Ferreira, Ederlan
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2021
País:Brasil
Institución:Universidade Estadual Paulista (UNESP)
Repositorio:Repositório Institucional da UNESP
Idioma:inglés
OAI Identifier:oai:repositorio.unesp.br:11449/210774
Acceso en línea:http://dx.doi.org/10.3390/ijms22063018
http://hdl.handle.net/11449/210774
Access Level:acceso abierto
Palabra clave:protein vicilin-type
protein fractionation
biological activities
in vitro digestibility
amino acid sequencing
glycosylated polypeptides
metal binding capacity
Descripción
Sumario:Adzuki seed beta-vignin, a vicilin-like globulin, has proven to exert various health-promoting biological activities, notably in cardiovascular health. A simple scalable enrichment procedure of this protein for further nutritional and functional studies is crucial. In this study, a simplified chromatography-independent protein fractionation procedure has been optimized and described. The electrophoretic analysis showed a high degree of homogeneity of beta-vignin isolate. Furthermore, the molecular features of the purified protein were investigated. The adzuki bean beta-vignin was found to have a native size of 146 kDa, and the molecular weight determined was consistent with a trimeric structure. These were identified in two main polypeptide chains (masses of 56-54 kDa) that are glycosylated polypeptides with metal binding capacity, and one minor polypeptide chain with a mass 37 kDa, wherein these features are absent. The in vitro analysis showed a high degree of digestibility of the protein (92%) and potential anti-inflammatory capacity. The results lay the basis not only for further investigation of the health-promoting properties of the adzuki bean beta-vignin protein, but also for a possible application as nutraceutical molecule.