Influence of curing protocols on water sorption and solubility of a self-adhesive resin-cement

Aim: To evaluate the effect of different activation protocols on the polymerization of a self-adhesive dual cured resin-based cement. Methods: Thirty disc-shaped specimens were prepared with the resin cement RelyX U200 (3M ESPE) and divided according to three protocols: immediate light-activation fo...

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Detalles Bibliográficos
Autores: Dziedzic, Dilcele Silva Moreira, Prohny, João Paulo Stanislovicz, Picharski, Gledson Luiz, Furuse, Adilson Yoshio
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2017
País:Brasil
Institución:Universidade Estadual de Campinas (UNICAMP)
Repositorio:Brazilian journal of oral sciences (Online)
Idioma:inglés
OAI Identifier:oai:ojs.periodicos.sbu.unicamp.br:article/8648766
Acceso en línea:https://periodicos.sbu.unicamp.br/ojs/index.php/bjos/article/view/8648766
Access Level:acceso abierto
Palabra clave:Resin cements. Solubility. Polymerization.
Polimerização
Descripción
Sumario:Aim: To evaluate the effect of different activation protocols on the polymerization of a self-adhesive dual cured resin-based cement. Methods: Thirty disc-shaped specimens were prepared with the resin cement RelyX U200 (3M ESPE) and divided according to three protocols: immediate light-activation for 40 s, delayed light-activation (10 min after manipulation, for 40 s) or self-curing without light-activation. The specimens were desiccated, kept in water at 37 °C for 7 days and desiccated again to calculate water sorption, solubility and mass variation. Data were analyzed by Shapiro-Wilk Test and Wilcoxon tests (α=0.05). Images after the specimens’ final desiccation were also made. Results: The Wilcoxon test revealed a significant difference for sorption and mass variation (p<0.05) and the highest value was observed in self-curing or chemical activation group (CA), followed by delayed light-activation (DL) and immediate light-activation (IL). Besides the water sorption parameters, there were also microvoids on the discs from the delayed and no light-activation groups. Conclusions: The light-activation immediately after manipulation is recommended for the evaluated resin cement.