Synthesis and electrochemical characterization of Si/TiO2/Au composite anode: Efficient oxygen evolution and hydroxyl radicals generation

This paper describes the photoelectrochemical properties of a novel composite anode composed of a 200 nm Au-Sb ohmic contact/300 μm n-Si wafer/20 nm TiO2 /120 nm Au grid. By connecting the Au ohmic contact to the gold grid via a power supply, holes thermally or photochemically generated in the Si ar...

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Detalles Bibliográficos
Autores: Bessegato, G. G. [UNESP], Cooke, M. D., Christensen, P. A., Wood, D., Zanoni, M. V.B. [UNESP]
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2021
País:Brasil
Institución:Universidade Estadual Paulista (UNESP)
Repositorio:Repositório Institucional da UNESP
Idioma:inglés
OAI Identifier:oai:repositorio.unesp.br:11449/205739
Acceso en línea:http://dx.doi.org/10.1016/j.electacta.2021.137742
http://hdl.handle.net/11449/205739
Access Level:acceso abierto
Palabra clave:Dye degradation
Oxygen generation
Photoelectrochemistry
Titanium dioxide
Descripción
Sumario:This paper describes the photoelectrochemical properties of a novel composite anode composed of a 200 nm Au-Sb ohmic contact/300 μm n-Si wafer/20 nm TiO2 /120 nm Au grid. By connecting the Au ohmic contact to the gold grid via a power supply, holes thermally or photochemically generated in the Si are launched to the TiO2 surface where they are converted to •OH radicals. We show that the Si/TiO2/Au composite anode can be efficiently employed in the oxygen evolution reaction and prove that the anode generates hydroxyl radicals (using p-nitrosodimethylaniline as a probe). Potential applications include the photoelectrocatalytic oxidation of organic contaminants, water splitting, and organic electro-synthesis.