Efeito da adição de fluoreto de lítio na sinterização da alumina

The incorporation of additives in the sintering of alumina (Al2O3) has the aim of improvement the ceramic processing and, consequently, the physicochemical properties of bulk ceramics. In the present study, the influence of litium fluoride (LiF) additive into Al2O3 sintering using a weight concentra...

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Detalles Bibliográficos
Autores: Lopes, Camila Cristine, Gomes, Alaelson Vieira, Marçal, Rubens Lincoln Santana Blazutti
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2018
País:Brasil
Institución:Instituto Militar de Engenharia (IME)
Repositorio:C&T (Rio de Janeiro. Online)
Idioma:portugués
OAI Identifier:oai:meiramattos.eceme.ensino.eb.br:article/1947
Acceso en línea:https://ebrevistas.eb.mil.br/CT/article/view/1947
Access Level:acceso abierto
Palabra clave:Alumina
additive
Litium fluoride
sintering
aditivo
Fluoreto de lítio
sinterização
Descripción
Sumario:The incorporation of additives in the sintering of alumina (Al2O3) has the aim of improvement the ceramic processing and, consequently, the physicochemical properties of bulk ceramics. In the present study, the influence of litium fluoride (LiF) additive into Al2O3 sintering using a weight concentration of 0.30% LiF at1400 oC /3h was studied. The particle size characterization indicated that the addition of LiF reduced the average particle size after milling the powders. The densification of bulk ceramics revealed higher values in the presence of LiF additive sintering. The superficial morphology of sintered Al2O3-LiF bulk ceramics were characterized by scanning electron microscopy (SEM), which revealed the formation of second phase in the grain boundary. X-ray diffraction (XRD) analysis identified this second phase as: LiAl5O