Evaluation of blood compatibility of plasma deposited heparin-like films and SF6 plasma treated surfaces

In devices used in open-heart surgery and dialysis, blood must be continuously processed using extracorporeal circuits composed of peristaltic pumps and active components such as specifc flters and oxygenators. Several procedures have been employed to avoid blood coagulation induced by contact with...

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Detalhes bibliográficos
Autores: Perrenoud, Ivanira Antunes [UNESP], Rangel, Elidiane Cipriano [UNESP], Mota, Rogério Pinto [UNESP], Durrant, Steven Frederick [UNESP], Da Cruz, Nilson Cristino [UNESP]
Formato: artículo
Estado:Versión publicada
Fecha de publicación:2010
País:Brasil
Recursos:Universidade Estadual Paulista (UNESP)
Repositorio:Repositório Institucional da UNESP
Idioma:inglés
OAI Identifier:oai:repositorio.unesp.br:11449/71530
Acesso em linha:http://dx.doi.org/10.1590/S1516-14392010000100019
http://hdl.handle.net/11449/71530
Access Level:acceso abierto
Palavra-chave:Biomaterials
Blood compatibility
Heparin
PECVD
Plasma treatment
Active components
Bioactive proteins
Blood coagulation
Clot formation
Coagulation time
Gas plasma
Glass substrates
Glass surfaces
Human bloods
Open-heart surgery
Peristaltic pump
Radio-frequency plasma enhanced chemical vapor deposition
Surface energy measurements
Biological materials
Blood substitutes
Coagulation
Contact angle
Dialysis
Glass
Infrared spectroscopy
Oxygenators
Plasma deposition
Plasma enhanced chemical vapor deposition
Plasmas
Polysaccharides
Polyvinyl chlorides
Substrates
Surface chemistry
Surface tension
Blood
Descrição
Resumo:In devices used in open-heart surgery and dialysis, blood must be continuously processed using extracorporeal circuits composed of peristaltic pumps and active components such as specifc flters and oxygenators. Several procedures have been employed to avoid blood coagulation induced by contact with the artifcial surfaces of such devices. Often heparin, a bioactive protein able to prevent clot formation, is employed. In this work, we have used heparin-containing gas plasmas to evaluate the possibility of depositing adherent anticoagulant flms onto PVC and glass surfaces. The flms were produced by radiofrequency plasma enhanced chemical vapor deposition from heparin/isopropanol and heparin/hexamethyldisiloxane solutions. In addition, the effects of exposure to SF6 plasmas on the compatibility of such surfaces have also been investigated. The blood compatibility was evaluated through the determination of the density of platelets and fbrinogen and activated partial thromboplastin (APTT) and prothrombin times (PT) of human blood freshly collected and after contact for 2.5 hours with different surfaces. The deposited flms were also characterized by infrared spectroscopy, contact angle and surface energy measurements. The coagulation time of blood, placed in contact with glass substrates coated by PECVD flms of heparin/isopropanol mixtures, and in contact with SF6 plasma-treated PVC, increased by about 60 and 20%, respectively, compared to the values measured with untreated samples.