Adequacy of isotherm adsorption of black 5 reactive dye for crosslinked chitosan microspheres

Chitosan microspheres with average diameter 1.03 ± 0.06 mm and degree of deacetylation of 72.5% were employed as adsorbent for reactive dye black 5. Chitosan was characterized through infrared spectroscopy (IR), 13C NMR spectrum and deacetylation degree (DD%), and crosslinked with glutara...

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Detalles Bibliográficos
Autores: Kimura, Irene Yukiko, Favere, Valfredo Tadeu, Martins, Amarildo Otavio, Spinelli, Viviane Aparecida, Josué, Atche
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2008
País:Brasil
Institución:Universidade Estadual de Maringá (UEM)
Repositorio:Acta scientiarum. Technology (Online)
Idioma:portugués
OAI Identifier:oai:periodicos.uem.br/ojs:article/2753
Acceso en línea:http://www.periodicos.uem.br/ojs/index.php/ActaSciTechnol/article/view/2753
Access Level:acceso abierto
Palabra clave:adsorção
microesfera de quitosana
corante reativo
1.06.00.00-0 Química
Descripción
Sumario:Chitosan microspheres with average diameter 1.03 ± 0.06 mm and degree of deacetylation of 72.5% were employed as adsorbent for reactive dye black 5. Chitosan was characterized through infrared spectroscopy (IR), 13C NMR spectrum and deacetylation degree (DD%), and crosslinked with glutaraldehyde 2.5% (w/v) to increase its resistance in acid medium. Corresponding isotherms were obtained in acid and alkaline solutions. Experimental data were fitted by Langmuir’s, extended Freundlich’s and Nernst’s isotherms. Adsorption was more effective in acid medium and adjusted better the Langmuir’s isotherm