Synthesis of beta-AgVO3 nanowires by hydrothermal and precipitation routes: a comparative study

Silver vanadate, especially beta-AgVO3, have a wide range of technological applications due to remarkable biological, optical, and electrical features. The structure, morphology, and properties of beta-AgVO3 are directly affected by synthesis conditions. A comparative study between two different syn...

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Detalles Bibliográficos
Autores: Canuto de Menezes, Beatriz Rossi, Ribas, Renata Guimaraes, Schatkoski, Vanessa Modelski, Amaral Montanheiro, Thais Larissa do, Koga-Ito, Cristiane Yumi [UNESP], Thim, Gilmar Patrocinio
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2019
País:Brasil
Institución:Universidade Estadual Paulista (UNESP)
Repositorio:Repositório Institucional da UNESP
Idioma:inglés
OAI Identifier:oai:repositorio.unesp.br:11449/197503
Acceso en línea:http://dx.doi.org/10.1007/s42452-019-1396-1
http://hdl.handle.net/11449/197503
Access Level:acceso abierto
Palabra clave:Silver vanadate
beta-AgVO3
Precipitation synthesis
Hydrothermal method
Descripción
Sumario:Silver vanadate, especially beta-AgVO3, have a wide range of technological applications due to remarkable biological, optical, and electrical features. The structure, morphology, and properties of beta-AgVO3 are directly affected by synthesis conditions. A comparative study between two different synthesis routes (precipitation and hydrothermal) of beta-AgVO3 was systematically investigated in this work. X-ray diffraction, Raman spectroscopy, scanning electron microscopy, zeta potential, and UV-visible spectrometry results showed that the hydrothermal method produced more homogeneous samples of beta-AgVO3, with elevated purity and crystallinity. In addition, the sample of beta-AgVO3 obtained by hydrothermal method had a wire-like morphology while that obtained by precipitation had irregular shape. Finally, the hydrothermal procedure showed more elevated reproducibility.