Influence of substrate, cement and aging on the biaxial flexural strength of lithium disilicate

Objective: To evaluate the biaxial flexural strength (BFS) of lithium disilicate (L), cemented on different substrates (epoxy resin-E and metal-M) with dual-cure resin cement (Rc) and zinc phosphate cement (Zc), not aged, thermally aged (TC) or thermo-mechanical aged (TC/MC). Material and Methods: D...

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Autores: de LIMA, Leonardo Custódio, Miranda, Jean Soares, de CARVALHO, Ronaldo Luis Almeida, Barcellos, Aline Serrado de Pinho [UNESP], Amaral, Marina, Kimpara, Estevão Tomomitsu [UNESP]
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2023
País:Brasil
Institución:Universidade Estadual Paulista (UNESP)
Repositorio:Repositório Institucional da UNESP
Idioma:inglés
OAI Identifier:oai:repositorio.unesp.br:11449/307237
Acceso en línea:http://dx.doi.org/10.4322/bds.2023.e3923
https://hdl.handle.net/11449/307237
Access Level:acceso abierto
Palabra clave:Aging
Cementation
Ceramics
Flexural strength
Lithium disilicate
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spelling Influence of substrate, cement and aging on the biaxial flexural strength of lithium disilicateInfluência do substrato, cimento e envelhecimento na resistência a flexão biaxial do dissilicato de lítioAgingCementationCeramicsFlexural strengthLithium disilicateObjective: To evaluate the biaxial flexural strength (BFS) of lithium disilicate (L), cemented on different substrates (epoxy resin-E and metal-M) with dual-cure resin cement (Rc) and zinc phosphate cement (Zc), not aged, thermally aged (TC) or thermo-mechanical aged (TC/MC). Material and Methods: Disks of L, E, and M were fabricated, and the cementation was performed according to the following groups: ERc (L+E+Rc); MRc (L+M+Rc); MZc (L+M+Zc); EZc (L+E+Zc). Ten samples from each described group were tested in BFS, ten more samples were subjected to TC (1×104 cycles between 5 ºC and 55 ºC water), and the last 10 samples were subjected to TC/MC (MC: 1.2×106 cycles, 50 N, 3.8 Hz). The BFS test was performed and scanning electron microscopy (SEM) was performed to evaluate the failure mode. The effect of the cementation strategy (cement/substrate) was compared in each aging method and the effect of the aging method was evaluated for each cementation strategy by one-way ANOVA and Tukey post-hoc test (α=0.05). Results: The strength values were highest to M (237.8 ~ 463.9 MPa), in comparison to the E (41.03 ~ 66.76 MPa), despite aging and luting agent. Flexural strength data decreased after TC and TC/MC in groups cemented with Zc, but was stable when cemented with Rc. SEM analysis indicated that failure origins were located at the tensile surface of the L. Conclusion: Lithium disilicate discs cemented to the metallic substrate presented the highest biaxial flexural strength. The cementation with dual-cure resin cement did not decrease BFS after aging.Departamento de Odontologia Restauradora Faculdade de Odontologia Universidade de São Paulo, SPDepartamento de Odontologia Universidade Federal de Juiz de Fora, MGDepartamento de Odontologia Universidade Braz Cubas, SPDepartamento de Materiais e Dentários e Prótese Instituto de Ciência e Tecnologia Unesp, SPDepartamento de Odontologia Universidade de Taubaté, SPDepartamento de Materiais e Dentários e Prótese Instituto de Ciência e Tecnologia Unesp, SPUniversidade de São Paulo (USP)Universidade Federal de Juiz de ForaUniversidade Braz CubasUniversidade Estadual Paulista (UNESP)Universidade de Taubaté2025-04-29T20:08:48Z2023-10-01info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articlehttp://dx.doi.org/10.4322/bds.2023.e3923Brazilian Dental Science, v. 26, n. 4, 2023.2178-6011https://hdl.handle.net/11449/30723710.4322/bds.2023.e39232-s2.0-85174919374Scopusreponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESPengBrazilian Dental Scienceinfo:eu-repo/semantics/openAccessde LIMA, Leonardo CustódioMiranda, Jean Soaresde CARVALHO, Ronaldo Luis AlmeidaBarcellos, Aline Serrado de Pinho [UNESP]Amaral, MarinaKimpara, Estevão Tomomitsu [UNESP]2025-04-30T13:56:09Zoai:repositorio.unesp.br:11449/307237Repositório InstitucionalPUBhttp://repositorio.unesp.br/oai/requestrepositoriounesp@unesp.bropendoar:29462025-04-30T13:56:09Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)false
dc.title.none.fl_str_mv Influence of substrate, cement and aging on the biaxial flexural strength of lithium disilicate
Influência do substrato, cimento e envelhecimento na resistência a flexão biaxial do dissilicato de lítio
title Influence of substrate, cement and aging on the biaxial flexural strength of lithium disilicate
spellingShingle Influence of substrate, cement and aging on the biaxial flexural strength of lithium disilicate
de LIMA, Leonardo Custódio
Aging
Cementation
Ceramics
Flexural strength
Lithium disilicate
title_short Influence of substrate, cement and aging on the biaxial flexural strength of lithium disilicate
title_full Influence of substrate, cement and aging on the biaxial flexural strength of lithium disilicate
title_fullStr Influence of substrate, cement and aging on the biaxial flexural strength of lithium disilicate
title_full_unstemmed Influence of substrate, cement and aging on the biaxial flexural strength of lithium disilicate
title_sort Influence of substrate, cement and aging on the biaxial flexural strength of lithium disilicate
dc.creator.none.fl_str_mv de LIMA, Leonardo Custódio
Miranda, Jean Soares
de CARVALHO, Ronaldo Luis Almeida
Barcellos, Aline Serrado de Pinho [UNESP]
Amaral, Marina
Kimpara, Estevão Tomomitsu [UNESP]
author de LIMA, Leonardo Custódio
author_facet de LIMA, Leonardo Custódio
Miranda, Jean Soares
de CARVALHO, Ronaldo Luis Almeida
Barcellos, Aline Serrado de Pinho [UNESP]
Amaral, Marina
Kimpara, Estevão Tomomitsu [UNESP]
author_role author
author2 Miranda, Jean Soares
de CARVALHO, Ronaldo Luis Almeida
Barcellos, Aline Serrado de Pinho [UNESP]
Amaral, Marina
Kimpara, Estevão Tomomitsu [UNESP]
author2_role author
author
author
author
author
dc.contributor.none.fl_str_mv Universidade de São Paulo (USP)
Universidade Federal de Juiz de Fora
Universidade Braz Cubas
Universidade Estadual Paulista (UNESP)
Universidade de Taubaté
dc.subject.por.fl_str_mv Aging
Cementation
Ceramics
Flexural strength
Lithium disilicate
topic Aging
Cementation
Ceramics
Flexural strength
Lithium disilicate
description Objective: To evaluate the biaxial flexural strength (BFS) of lithium disilicate (L), cemented on different substrates (epoxy resin-E and metal-M) with dual-cure resin cement (Rc) and zinc phosphate cement (Zc), not aged, thermally aged (TC) or thermo-mechanical aged (TC/MC). Material and Methods: Disks of L, E, and M were fabricated, and the cementation was performed according to the following groups: ERc (L+E+Rc); MRc (L+M+Rc); MZc (L+M+Zc); EZc (L+E+Zc). Ten samples from each described group were tested in BFS, ten more samples were subjected to TC (1×104 cycles between 5 ºC and 55 ºC water), and the last 10 samples were subjected to TC/MC (MC: 1.2×106 cycles, 50 N, 3.8 Hz). The BFS test was performed and scanning electron microscopy (SEM) was performed to evaluate the failure mode. The effect of the cementation strategy (cement/substrate) was compared in each aging method and the effect of the aging method was evaluated for each cementation strategy by one-way ANOVA and Tukey post-hoc test (α=0.05). Results: The strength values were highest to M (237.8 ~ 463.9 MPa), in comparison to the E (41.03 ~ 66.76 MPa), despite aging and luting agent. Flexural strength data decreased after TC and TC/MC in groups cemented with Zc, but was stable when cemented with Rc. SEM analysis indicated that failure origins were located at the tensile surface of the L. Conclusion: Lithium disilicate discs cemented to the metallic substrate presented the highest biaxial flexural strength. The cementation with dual-cure resin cement did not decrease BFS after aging.
publishDate 2023
dc.date.none.fl_str_mv 2023-10-01
2025-04-29T20:08:48Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://dx.doi.org/10.4322/bds.2023.e3923
Brazilian Dental Science, v. 26, n. 4, 2023.
2178-6011
https://hdl.handle.net/11449/307237
10.4322/bds.2023.e3923
2-s2.0-85174919374
url http://dx.doi.org/10.4322/bds.2023.e3923
https://hdl.handle.net/11449/307237
identifier_str_mv Brazilian Dental Science, v. 26, n. 4, 2023.
2178-6011
10.4322/bds.2023.e3923
2-s2.0-85174919374
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv Brazilian Dental Science
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.source.none.fl_str_mv Scopus
reponame:Repositório Institucional da UNESP
instname:Universidade Estadual Paulista (UNESP)
instacron:UNESP
instname_str Universidade Estadual Paulista (UNESP)
instacron_str UNESP
institution UNESP
reponame_str Repositório Institucional da UNESP
collection Repositório Institucional da UNESP
repository.name.fl_str_mv Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)
repository.mail.fl_str_mv repositoriounesp@unesp.br
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score 15,127371